ChemicalBook > CAS DataBase List > 1-Boc-5-hydroxyindole

1-Boc-5-hydroxyindole

Product Name: 1-Boc-5-hydroxyindole
CAS No.: 434958-85-7
Chemical Name: 1-Boc-5-hydroxyindole
Synonyms: 1-Boc-1H-indol-5-ol;5-AMINOPHTHALIC ACID;1-BOC-5-HYDROXYINDOLE;N-BOC-5-HYDROXYINDOLE;5-hydroxy-1-indolecarboxylate;5-hydroxy-1H-indole-1-carboxylate;tert-butyl 5-hydroxyindole-1-carboxylate;tert-butyl 5-hydroxy-1H-indole-1-carboxylate;1H-Indole-1-carboxylic acid, 5-hydroxy-,1,1-diMethylethyl ester
CBNumber: CB0275347
Molecular Formula: C13H15NO3
Formula Weight: 233.26
MOL File: 434958-85-7.mol

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1-Boc-5-hydroxyindole Property

Boiling point:: 374.5±34.0 °C(Predicted)
Density: 1.16±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 9.55±0.40(Predicted)
Appearance: White to off-white Solid
CAS DataBase Reference: 434958-85-7(CAS DataBase Reference)

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B656693
Product name: N-Boc-5-Hydroxyindole
Packaging: 500mg
Price: $130
Updated: 2021/12/16

Matrix Scientific

Product number: 072860
Product name: N-Boc-5-Hydroxyindole
Purity: 95+%
Packaging: 1g
Price: $163
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140244
Product name: tert-Butyl 5-hydroxy-1H-indole-1-carboxylate
Packaging: 5G
Price: $363
Updated: 2021/12/16

AK Scientific

Product number: W6280
Product name: N-Boc-5-Hydroxyindole
Packaging: 10g
Price: $537
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140244
Product name: tert-Butyl 5-hydroxy-1H-indole-1-carboxylate
Packaging: 10g
Price: $631.3
Updated: 2021/12/16

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1-Boc-5-hydroxyindole Chemical Properties,Usage,Production

Synthesis

170147-29-2

434958-85-7

General procedure for the synthesis of N-Boc-5-hydroxyindole from tert-butyl 5-(benzyloxy)-1H-indole-1-carboxylate: the product of Example 93A (680 mg, 2.103 mmol) was dissolved in ethanol (20 mL) under nitrogen protection, and 10% palladium carbon (68 mg) and ammonium formate (265 mg, 4.205 mmol) were added. After stirring the reaction for 1 h at room temperature, the reaction mixture was filtered through a 0.45 μm PTFE membrane and the catalyst was washed with methanol. The filtrate was concentrated by rotary evaporator and the resulting residue was dissolved in ethyl acetate (50 mL) and washed sequentially with water (2 × 25 mL) and saturated saline (25 mL). The organic phase was dried over anhydrous sodium sulfate, filtered and concentrated in vacuum to give N-Boc-5-hydroxyindole (475 mg, 96% yield) as a white solid.

References

[1] Patent: WO2007/76034, 2007, A2. Location in patent: Page/Page column 127
[2] Patent: WO2005/51957, 2005, A1. Location in patent: Page/Page column 57

1-Boc-5-hydroxyindole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-Boc-5-hydroxyindole manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 1-Boc-5-hydroxyindole 434958-85-7
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: 1-Boc-5-hydroxyindole 434958-85-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%
Supply Ability: 500kg
Release date: 2018-08-19

434958-85-7, 1-Boc-5-hydroxyindoleRelated Search:

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434958-85-7