ChemicalBook > CAS DataBase List > 6-Bromo-1H-indol-4-amine

6-Bromo-1H-indol-4-amine

Product Name
6-Bromo-1H-indol-4-amine
CAS No.
350800-81-6
Chemical Name
6-Bromo-1H-indol-4-amine
Synonyms
4-AMINO-6-BROMOINDOLE;6-BROMO-4-AMINOINDOLE;6-BROMOINDOL-4-YLAMINE;6-bromo-1H-indol-4-amine;4-Amino-6-bromo-1H-indole;1H-Indol-4-aMine, 6-broMo-
CBNumber
CB0277482
Molecular Formula
C8H7BrN2
Formula Weight
211.06
MOL File
350800-81-6.mol
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6-Bromo-1H-indol-4-amine Property

storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
A607818
Product name
4-Amino-6-bromoindole
Packaging
10mg
Price
$45
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0012844
Product name
4-AMINO-6-BROMOINDOLE
Purity
95.00%
Packaging
1G
Price
$1431.05
Updated
2021/12/16
Alichem
Product number
350800816
Product name
6-Bromo-1H-indol-4-amine
Packaging
5g
Price
$1735.22
Updated
2021/12/16
Ambeed
Product number
A127841
Product name
6-Bromo-1H-indol-4-amine
Purity
95%
Packaging
100mg
Price
$70
Updated
2021/12/16
Ambeed
Product number
A127841
Product name
6-Bromo-1H-indol-4-amine
Purity
95%
Packaging
250mg
Price
$104
Updated
2021/12/16
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6-Bromo-1H-indol-4-amine Chemical Properties,Usage,Production

Synthesis

350800-78-1

350800-81-6

To 6-bromo-1H-indol-4-amine (3 g, 9.49 mmol) was added HCl solution (61.20 g, 167.86 mmol) of TiCl3 (7.32 g, 47.45 mmol). The reaction mixture was stirred at 25 °C for 16 hours. After completion of the reaction, the mixture was slowly poured into 2N aqueous NaOH solution (150 mL) and extracted with EtOAc (150 mL). The organic phase was dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (eluent: petroleum ether to petroleum ether/ethyl acetate = 5/1) to afford 6-bromo-1H-indol-4-amine (2 g, 36% yield) as a gray solid.1H NMR (CDCl3, 400 MHz) δ 8.10 (br s, 1H), 7.09-7.08 (m, 1H), 7.02 (d, J = 1.4Hz , 1H), 6.54 (d, J = 1.4Hz, 1H), 6.44-6.43 (m, 1H), 3.98 (br s, 2H).

References

[1] Patent: WO2016/168682, 2016, A2. Location in patent: Paragraph 0256
[2] European Journal of Medicinal Chemistry, 2001, vol. 36, # 2, p. 165 - 178

6-Bromo-1H-indol-4-amine Preparation Products And Raw materials

Raw materials

Preparation Products

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6-Bromo-1H-indol-4-amine Suppliers

China 59 India 1 Switzerland 2 United Kingdom 4 United States 11 Global 77
Molekula Ltd
Tel
--
Fax
--
Email
info@molekula.com
Country
United Kingdom
ProdList
4060
Advantage
50
Leancare Ltd.
Tel
--
Fax
--
Email
enquiry@leancare.co.uk
Country
United Kingdom
ProdList
6446
Advantage
42
MOLEKULA Ltd.
Tel
--
Fax
--
Email
kevinbanks@molekula.com
Country
United Kingdom
ProdList
6140
Advantage
66
Fulcrum Scientific Ltd.
Tel
--
Fax
--
Country
United Kingdom
ProdList
6565
Advantage
38
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View Lastest Price from 6-Bromo-1H-indol-4-amine manufacturers

Career Henan Chemical Co
Product
4-AMINO-6-BROMOINDOLE 350800-81-6
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2020-01-09

350800-81-6, 6-Bromo-1H-indol-4-amineRelated Search:

Indole 1H-Indole, 4-broMo-6-(trifluoroMethyl)- 1H-Indole, 6-broMo-4-(phenylMethoxy)- 4-BROMO-6-AMINOINDOLE 1H-Indole, 6-broMo-4-nitro- 6-Chloro-4-methoxyindole 6-BROMO-4-FLUORO INDOLE 1H-Indol-4-amine,6-iodo-(9CI) 3-AMINO-5-BROMOINDOLE 7-AMINO-5-BROMOINDOLE,7-Amino-5-bromoindole,97% 6-Bromo-1H-indole 6-Bromo-1H-indol-4-amine 6-BROMO-3-METHYL-4-NITROINDOLE 6-BROMO-4-NITRO INDOLE

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  • 6-BROMO-4-AMINOINDOLE
  • 1H-Indol-4-aMine, 6-broMo-
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  • 6-bromo-1H-indol-4-amine
  • 350800-81-6