ChemicalBook > CAS DataBase List > 1-Fluoro-3-iodobenzene

1-Fluoro-3-iodobenzene

Product Name: 1-Fluoro-3-iodobenzene
CAS No.: 1121-86-4
Chemical Name: 1-Fluoro-3-iodobenzene
Synonyms: 3-FLUOROIODOBENZENE;m-Fluorobenzene;M-FLUOROIODOBENZENE;3-Iodofluorobenzene;m-Iodofluorobenzene;3- Fluoriodobenzene;1-fluoro-3-iodo-benzen;3-Fluoro-1-iodobenzene;1-Iodo-3-fluorobenzene;1-FLUORO-3-IODOBENZENE
CBNumber: CB0284196
Molecular Formula: C6H4FI
Formula Weight: 222
MOL File: 1121-86-4.mol

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1-Fluoro-3-iodobenzene Property

Melting point:: -42°C
Boiling point:: 77-78 °C/19 mmHg (lit.)
Density: 1.89 g/mL at 25 °C (lit.)
refractive index: n20/D 1.584(lit.)
Flash point:: 153 °F
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: Liquid
Specific Gravity: 1.890
color: Clear yellow or pink
Sensitive: Light Sensitive
BRN: 2039305
InChIKey: VSKSBSORLCDRHS-UHFFFAOYSA-N
CAS DataBase Reference: 1121-86-4(CAS DataBase Reference)
NIST Chemistry Reference: Benzene, 1-fluoro-3-iodo-(1121-86-4)
EPA Substance Registry System: m-Fluoroiodobenzene (1121-86-4)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36-37/39
WGK Germany: 3
TSCA: T
HazardClass: IRRITANT
HS Code: 29039990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 219398
Product name: 3-Fluoroiodobenzene
Purity: 99%
Packaging: 25g
Price: $73.22
Updated: 2025/07/31

TCI Chemical

Product number: F0260
Product name: 1-Fluoro-3-iodobenzene (stabilized with Copper chip)
Purity: >99.0%(GC)
Packaging: 25g
Price: $103
Updated: 2025/07/31

TRC

Product number: B434808
Product name: 1-fluoro-3-iodobenzene
Packaging: 2.5g
Price: $65
Updated: 2021/12/16

Usbiological

Product number: 409780
Product name: 1-fluoro-3-iodobenzene
Packaging: 500mg
Price: $305
Updated: 2021/12/16

Usbiological

Product number: 278213
Product name: 1-Fluoro-3-iodobenzene
Packaging: 25g
Price: $350
Updated: 2021/12/16

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1-Fluoro-3-iodobenzene Chemical Properties,Usage,Production

Chemical Properties

clear yellow or pink liquid

Uses

3-Fluoroiodobenzene was used to prepare methyl 4-iodobenzo[b]thiophene-2-carboxylate, key intermediate for the synthesis of 4-substituted benzo[b]thiophene-2-carboxamidines.

General Description

3-Fluoroiodobenzene participates in palladium-catalyzed hydroarylation of arylpropiolamides.

Synthesis

372-19-0

1121-86-4

The general procedure for the synthesis of m-fluoroiodobenzene from 3-fluoroaniline was as follows: an aqueous solution (20 mL) of NaNO2 (6.4 g, 92.75 mmol) was slowly added dropwise at 0 °C to a solution of 3-fluoroaniline (10 g, 90.09 mmol) dissolved in 32% H2SO4 (179 g). The reaction mixture was stirred continuously at 0 °C for 1 hour. Subsequently, an aqueous solution (30 mL) of KI (22.4 g, 134.94 mmol) was added while maintaining 0 °C and stirring was continued at 0 °C for 1 hour. After completion of the reaction, the aqueous phase was extracted with EtOAc (2 x 250 mL). The organic phases were combined and washed sequentially with water (5×200mL) and 10% NaHSO3 solution (3×200mL), dried over Na2SO4 and concentrated under reduced pressure to remove the solvent, yielding 17.7 g of 1-fluoro-3-iodobenzene as a yellow solid in 82% yield.

References

[1] Patent: WO2008/103615, 2008, A1. Location in patent: Page/Page column 40
[2] Journal of the American Chemical Society, 1963, vol. 85, p. 709 - 724

1-Fluoro-3-iodobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Fluoro-3-iodobenzene Suppliers

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View Lastest Price from 1-Fluoro-3-iodobenzene manufacturers

Hebei Fengjia New Material Co., Ltd

Product: 1-Fluoro-3-iodobenzene 1121-86-4
Price: US $4.00/kg
Min. Order: 1kg
Purity: 0.99
Supply Ability: 10000
Release date: 2024-09-06

Hebei Chuanghai Biotechnology Co., Ltd

Product: 1-Fluoro-3-iodobenzene 1121-86-4
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2024-12-02

Speranza Chemical Co., Ltd.

Product: 3-iodofluorobenzene 1121-86-4
Price: US $250.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 20 tons
Release date: 2019-12-24

1121-86-4, 1-Fluoro-3-iodobenzeneRelated Search:

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3-Fluoroiodobenzene (stabilized with Copper chip)

1-Fluoro-3-iodobenzene, 98+%

Benzene, 1-fluoro-3-iodo-

1-Iodo-3-fluorobenzene

3-Fluoro-1-iodobenzene

1-Fluoro-3-iodobenzene,99%

1-Fluoro-3-iodobenzene,97%

3-Fluoroiodobenzene, 97+%

M-FLUOROIODOBENZENE

1-fluoro-3-iodo-benzen

3-Iodofluorobenzene

m-Fluorobenzene

m-Iodofluorobenzene

3-FLUOROIODOBENZENE

1-Fluoro-3-iodobenzene (stabilized with Copper chip)

1-FLUORO-3-IODOBENZENE

3-Fluoroiodobenzene 99%

3-Fluoroiodobenzene99%

1-Fluoro-3-iodobenzene(stabilizedwithCopperchip)&gt

3- Fluoriodobenzene

1-Fluoro-3-iodobenzene ISO 9001：2015 REACH

1121-86-4

1121-88-4

Building Blocks

HALOGEN

Aryl

Halogenated Hydrocarbons

Organic Building Blocks

Fluorinated benzene series

Aryl

Halogenated Hydrocarbons

Aromatic Hydrocarbons (substituted) & Derivatives

Benzene series

Miscellaneous

Fluorine Compounds

Iodine Compounds