4,7-Dichloroisatin

ChemicalBook > CAS DataBase List > 4,7-Dichloroisatin

Product Name: 4,7-Dichloroisatin
CAS No.: 18711-13-2
Chemical Name: 4,7-Dichloroisatin
Synonyms: BUTTPARK 50\07-81;4,7-DICHLOROISATIN;4,7-Dichloroisatin>4,7-Dichloroisatin,99%;4,7-DICHLOROISATIN 98%;4,7-Dichloroindole-2,3-dione;4,7-DICHLOROINDOLINE-2,3-DIONE;4,7-Dichloro-2,3-indolinedione;4,7-dichloro-1H-indole-2,3-dione;1H-Indole-2,3-dione, 4,7-dichloro-
CBNumber: CB0350512
Molecular Formula: C8H3Cl2NO2
Formula Weight: 216.02
MOL File: 18711-13-2.mol

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4,7-Dichloroisatin Property

Melting point:: 250-252 °C(lit.)
Density: 1.643±0.06 g/cm3 (20 ºC 760 Torr)
storage temp.: Inert atmosphere,Room Temperature
solubility: soluble in Methanol
form: powder to crystal
pka: 8.38±0.20(Predicted)
color: Light yellow to Brown
BRN: 168731
InChI: InChI=1S/C8H3Cl2NO2/c9-3-1-2-4(10)6-5(3)7(12)8(13)11-6/h1-2H,(H,11,12,13)
InChIKey: NUXYYWOWNFEMNH-UHFFFAOYSA-N
SMILES: N1C2=C(C(Cl)=CC=C2Cl)C(=O)C1=O
CAS DataBase Reference: 18711-13-2(CAS DataBase Reference)

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Safety

Hazard Codes: Xn
Risk Statements: 22-36
Safety Statements: 26-36
WGK Germany: 3
HS Code: 29337900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 597813
Product name: 4,7-Dichloroisatin
Purity: 97%
Packaging: 1g
Price: $111
Updated: 2023/06/20

TCI Chemical

Product number: D4039
Product name: 4,7-Dichloroisatin
Purity: >97.0%(T)
Packaging: 1g
Price: $58
Updated: 2024/03/01

TCI Chemical

Product number: D4039
Product name: 4,7-Dichloroisatin
Purity: >97.0%(T)
Packaging: 5g
Price: $229
Updated: 2024/03/01

Alfa Aesar

Product number: A14853
Product name: 4,7-Dichloroisatin, 98%
Packaging: 1g
Price: $50.65
Updated: 2024/03/01

Alfa Aesar

Product number: A14853
Product name: 4,7-Dichloroisatin, 98%
Packaging: 5g
Price: $162.65
Updated: 2024/03/01

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4,7-Dichloroisatin Chemical Properties,Usage,Production

Chemical Properties

orange flakes

Uses

Used as an intermediate in organic synthesis.

Synthesis

To a mixture of 2，5-Dichloroaniline (1.02 g, 7.84 mmol), anhydrous sodium sulfate (8.94 g, 62.71 mmol), hydroxylamine hydrochloride (2.24 g, 31.35 mmol) and 1M hydrochloric acid (8.0 mL) in water (60 mL) is added chloral hydrate (1.58 g, 9.41 mmol) at room temperature. The resulting mixture is warmed to 55 °C and stirred for 6 hours. While the mixture is cooling to room temperature, solid precipitate is formed and collected by filtration, washed with water and dried under vacuum to yield the hydroxyliminoacetanilide intermediate, which is added in small portions to concentrated sulfuric acid (5.0 mL) that is preheated to 55 °C. The temperature of the reaction mixture is maintained at below 58 °C throughout the addition. After the addition is completed, the dark-colored mixture is heated to 80 °C for 10 minutes before cooling down to room temperature. The mixture is then poured into crushed ice, swirled, and left to stand for 30 minutes. 4,7-Dichloroisatin formed is collected by filtration, washed with water and dried under vacuum.

4,7-Dichloroisatin Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4,7-Dichloroisatin manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 4,7-DICHLOROISATIN 18711-13-2
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: 4,7-DICHLOROISATIN 18711-13-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10000KGS
Release date: 2019-12-30

18711-13-2, 4,7-DichloroisatinRelated Search:

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18711-13-2

C8H3CI2NO2

Building Blocks

Indoles

Heterocyclic Building Blocks

Halogenated Heterocycles

Indoles and derivatives

Halogenated Heterocycles

Heterocyclic Building Blocks

Indoles

IndolesBuilding Blocks