ChemicalBook > CAS DataBase List > 1-(2'-BROMOPHENYL)ETHYLAMINE

1-(2'-BROMOPHENYL)ETHYLAMINE

Product Name
1-(2'-BROMOPHENYL)ETHYLAMINE
CAS No.
113899-55-1
Chemical Name
1-(2'-BROMOPHENYL)ETHYLAMINE
Synonyms
1-(2-BROMOPHENYL)ETHANAMINE;1-(2'-BROMOPHENYL)ETHYLAMINE;2-bromo-α-methylBenzenemethanamine;Benzenemethanamine, 2-bromo-α-methyl-;2-Bromo-alpha-methylbenzenemethanamine;Benzenemethanamine, 2-bromo-.alpha.-methyl-
CBNumber
CB0699897
Molecular Formula
C8H10BrN
Formula Weight
200.08
MOL File
113899-55-1.mol
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1-(2'-BROMOPHENYL)ETHYLAMINE Property

Boiling point:
248.5±15.0 °C(Predicted)
Density 
1.400±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
8.50±0.10(Predicted)
Appearance
Colorless to yellow Liquid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B679543
Product name
1-(2-Bromophenyl)ethylamine
Packaging
500mg
Price
$220
Updated
2021/12/16
AK Scientific
Product number
Z7493
Product name
1-(2-Bromophenyl)ethylamine
Packaging
1g
Price
$304
Updated
2021/12/16
Matrix Scientific
Product number
132428
Product name
1-(2-Bromophenyl)ethanamine
Purity
97%
Packaging
5g
Price
$900
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0029151
Product name
2-BROMO-ALPHA-METHYL-BENZENEMETHANAMINE
Purity
95.00%
Packaging
1G
Price
$983.52
Updated
2021/12/16
Matrix Scientific
Product number
132428
Product name
1-(2-Bromophenyl)ethanamine
Purity
97%
Packaging
10g
Price
$1437
Updated
2021/12/16
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1-(2'-BROMOPHENYL)ETHYLAMINE Chemical Properties,Usage,Production

Synthesis

27760-49-2

113899-55-1

Under nitrogen protection, sodium borohydride (3.1 g, 86 mmol) and titanium tetrachloride (1 M in toluene, 43 mL, 43 mmol) were dissolved in 40 mL of anhydrous 1,2-dimethoxyethane and the solution was cooled to 0 °C. Subsequently, 1-(2-bromophenyl)ethanone oxime (4.6 g, 21.5 mmol) was slowly added dropwise to the above cooled solution. After the dropwise addition was completed, the reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the reaction was quenched with 200 mL of water and the mixture was adjusted to alkaline with ammonium hydroxide. The crude product was extracted with a solvent mixture of toluene and ethyl acetate to separate the organic and aqueous layers. The organic layer was dried with anhydrous sodium sulfate and subsequently concentrated under reduced pressure to give the crude product 1-(2-bromophenyl)ethylamine (4.0 g, 100% yield). Mass spectrum (electrospray ionization) m/z 200/202 [M + 1]+.

References

[1] Patent: WO2008/144223, 2008, A2. Location in patent: Page/Page column 11

1-(2'-BROMOPHENYL)ETHYLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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113899-55-1, 1-(2'-BROMOPHENYL)ETHYLAMINERelated Search:

BOC-(R)-3-AMINO-3-(2-BROMO-PHENYL)-PROPIONIC ACID FMOC-(S)-3-AMINO-3-(2-BROMO-PHENYL)-PROPIONIC ACID BOC-(S)-3-AMINO-3-(2-BROMO-PHENYL)-PROPIONIC ACID 2-(2-Bromophenyl)pyrrolidine (S)-(-)-4-Bromo-alpha-phenylethylamine 2-(4-BROMOPHENYL)ETHYLAMINE 2-(2,5-Dimethoxy-4-bromophenyl)ethylamine Hydrochloride (R)-1-(3-BROMOPHENYL)ETHYLAMINE,(R)-1-(3-Bromophenyl)ethylamine, ChiPros 99%, ee 98+% (R)-(+)-1-(4-BROMOPHENYL)ETHYLAMINE 1-(4-Bromophenyl)ethylamine hydrochloride (R)-(+)-1-(4-BROMOPHENYL)ETHYLAMINE HYDROCHLORIDE 4-Bromo-alpha-phenethylamine (S)-1-(3-Bromophenyl)ethylamine, ChiPros 99%, ee 98+%,(S)-1-(3-BROMOPHENYL)ETHYLAMINE (S)-(-)-1-(2-Bromophenyl)ethylamine N-FMOC-3-AMINO-3-(2-BROMO-PHENYL)-PROPIONIC ACID AMINO-(1-BROMO-NAPHTHALEN-2-YL)-ACETIC ACID 3-(2-BROMO-4-CHLOROPHENYL)-BETA-ALANINE 2-AMINO-3-METHYLQUINOLINE HYDROCHLORIDE

  • Benzenemethanamine, 2-bromo-.alpha.-methyl-
  • 1-(2-BROMOPHENYL)ETHANAMINE
  • 1-(2'-BROMOPHENYL)ETHYLAMINE
  • 2-Bromo-alpha-methylbenzenemethanamine
  • 2-bromo-α-methylBenzenemethanamine
  • Benzenemethanamine, 2-bromo-α-methyl-
  • 113899-55-1
  • Anilines, Amides & Amines
  • Bromine Compounds