1-(2'-BROMOPHENYL)ETHYLAMINE
- Product Name
- 1-(2'-BROMOPHENYL)ETHYLAMINE
- CAS No.
- 113899-55-1
- Chemical Name
- 1-(2'-BROMOPHENYL)ETHYLAMINE
- Synonyms
- 1-(2-BROMOPHENYL)ETHANAMINE;1-(2'-BROMOPHENYL)ETHYLAMINE;2-bromo-α-methylBenzenemethanamine;Benzenemethanamine, 2-bromo-α-methyl-;2-Bromo-alpha-methylbenzenemethanamine;Benzenemethanamine, 2-bromo-.alpha.-methyl-
- CBNumber
- CB0699897
- Molecular Formula
- C8H10BrN
- Formula Weight
- 200.08
- MOL File
- 113899-55-1.mol
1-(2'-BROMOPHENYL)ETHYLAMINE Property
- Boiling point:
- 248.5±15.0 °C(Predicted)
- Density
- 1.400±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 8.50±0.10(Predicted)
- Appearance
- Colorless to yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B679543
- Product name
- 1-(2-Bromophenyl)ethylamine
- Packaging
- 500mg
- Price
- $220
- Updated
- 2021/12/16
- Product number
- Z7493
- Product name
- 1-(2-Bromophenyl)ethylamine
- Packaging
- 1g
- Price
- $304
- Updated
- 2021/12/16
- Product number
- 132428
- Product name
- 1-(2-Bromophenyl)ethanamine
- Purity
- 97%
- Packaging
- 5g
- Price
- $900
- Updated
- 2021/12/16
- Product number
- HCH0029151
- Product name
- 2-BROMO-ALPHA-METHYL-BENZENEMETHANAMINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $983.52
- Updated
- 2021/12/16
- Product number
- 132428
- Product name
- 1-(2-Bromophenyl)ethanamine
- Purity
- 97%
- Packaging
- 10g
- Price
- $1437
- Updated
- 2021/12/16
1-(2'-BROMOPHENYL)ETHYLAMINE Chemical Properties,Usage,Production
Synthesis
27760-49-2
113899-55-1
Under nitrogen protection, sodium borohydride (3.1 g, 86 mmol) and titanium tetrachloride (1 M in toluene, 43 mL, 43 mmol) were dissolved in 40 mL of anhydrous 1,2-dimethoxyethane and the solution was cooled to 0 °C. Subsequently, 1-(2-bromophenyl)ethanone oxime (4.6 g, 21.5 mmol) was slowly added dropwise to the above cooled solution. After the dropwise addition was completed, the reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, the reaction was quenched with 200 mL of water and the mixture was adjusted to alkaline with ammonium hydroxide. The crude product was extracted with a solvent mixture of toluene and ethyl acetate to separate the organic and aqueous layers. The organic layer was dried with anhydrous sodium sulfate and subsequently concentrated under reduced pressure to give the crude product 1-(2-bromophenyl)ethylamine (4.0 g, 100% yield). Mass spectrum (electrospray ionization) m/z 200/202 [M + 1]+.
References
[1] Patent: WO2008/144223, 2008, A2. Location in patent: Page/Page column 11
1-(2'-BROMOPHENYL)ETHYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
1-(2'-BROMOPHENYL)ETHYLAMINE Suppliers
- Tel
- 021-31261262/ 49 (0)17662837245
- Fax
- (0)21-33250524
- sales@novochemy.com
- Country
- Germany
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- 6328
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