N-phenyl-3-(trifluoromethyl)aniline
- Product Name
- N-phenyl-3-(trifluoromethyl)aniline
- CAS No.
- 101-23-5
- Chemical Name
- N-phenyl-3-(trifluoromethyl)aniline
- Synonyms
- NSC 50453;Etofenamate EP Impurity C;m-Trifluoromethyldiphenylamine;3-Trifluoromethyl diphenylamine;N-Phenyl-a,a,a-tri-fluorotoluidine;N-phenyl-3-(trifluoromethyl)aniline;Phenyl(m-trifluoromethylphenyl)amine;3-Trifluoromethyl-N-phenylbenzenamine;N-(3-Trifluoromethylphenyl)-phenylamine;N-Phenyl-3-(trifluoromethyl)benzenamine
- CBNumber
- CB0929035
- Molecular Formula
- C13H10F3N
- Formula Weight
- 237.22
- MOL File
- 101-23-5.mol
N-phenyl-3-(trifluoromethyl)aniline Property
- Boiling point:
- 108-110 °C(Press: 0.3 Torr)
- Density
- 1?+-.0.06 g/cm3(Predicted)
- refractive index
- 1.5655 (589.3 nm 25℃)
- storage temp.
- 2-8°C(protect from light)
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- form
- Oil
- pka
- -0.36±0.30(Predicted)
- color
- Colourless
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- P399710
- Product name
- N-Phenyl-3-(trifluoromethyl)aniline
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- IT58090
- Product name
- N-(3-Trifluoromethylphenyl)-phenylamine
- Packaging
- 250mg
- Price
- $77.5
- Updated
- 2021/12/16
- Product number
- IT58090
- Product name
- N-(3-Trifluoromethylphenyl)-phenylamine
- Packaging
- 1g
- Price
- $250
- Updated
- 2021/12/16
- Product number
- HCH0107926
- Product name
- N-PHENYL-ALPHA,ALPHA,ALPHA-TRIFLUORO-META-TOLUIDINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $315
- Updated
- 2021/12/16
- Product number
- IT58090
- Product name
- N-(3-Trifluoromethylphenyl)-phenylamine
- Packaging
- 2g
- Price
- $420
- Updated
- 2021/12/16
N-phenyl-3-(trifluoromethyl)aniline Chemical Properties,Usage,Production
Chemical Properties
Liquid. Boiling point 140-146°C/2.04-2.72kPa.
Uses
N-Phenyl-3-(trifluoromethyl)aniline can be used as fungicides.
Synthesis
62-53-3
1423-26-3
101-23-5
To a stirred solution of deionized water (10 mL) containing aniline (1.0 mmol), 3-(trifluoromethyl)phenylboronic acid (1.0 mmol), and K2CO3 (2.0 mmol) was added an aqueous suspension of FePd nanowires (3.0 mol%, dissolved in 3 mL H2O) at room temperature. The reaction mixture was stirred continuously for 5 h at room temperature. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, 2 M HCl solution was added and the catalyst was separated using an external magnet. Subsequently, the catalyst was washed with ethyl acetate (EtOAc). The reaction mixture was extracted with ethyl acetate (2 × 20 mL), and the organic phases were combined, dried over anhydrous sodium sulfate and concentrated. Finally, the residue was purified by gel permeation chromatography to afford the target product N-phenyl-3-(trifluoromethyl)aniline.
References
[1] Tetrahedron Letters, 2014, vol. 55, # 17, p. 2813 - 2817
N-phenyl-3-(trifluoromethyl)aniline Preparation Products And Raw materials
Raw materials
Preparation Products
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