ChemicalBook > CAS DataBase List > 6-(Trifluoromethyl)-1-indanone

6-(Trifluoromethyl)-1-indanone

Product Name: 6-(Trifluoromethyl)-1-indanone
CAS No.: 68755-37-3
Chemical Name: 6-(Trifluoromethyl)-1-indanone
Synonyms: 6-(trifluoromethyl)indan-1-one;6-(Trifluoromethyl)-1-indanone;6-(Trifluoromethyl)-1-indanone 97%;6-(Trifluoromethyl)-2,3-dihydro-1-indenone;6-(trifluoromethyl)-2,3-dihydroinden-1-one;2,3-Dihydro-6-(trifluoromethyl)-1H-inden-1-one;6-(trifluoroMethyl)-2,3-dihydro-1H-inden-1-one;1H-Inden-1-one, 2,3-dihydro-6-(trifluoroMethyl)-
CBNumber: CB0966203
Molecular Formula: C10H7F3O
Formula Weight: 200.16
MOL File: 68755-37-3.mol

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6-(Trifluoromethyl)-1-indanone Property

Boiling point:: 76-78 °C/0.2 mmHg
Density: 1.321 g/mL at 25 °C
refractive index: n20/D 1.496
Flash point:: 110 °C
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Light yellow to brown Solid-Liquid Mixture

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Safety

Hazard Codes: Xn
Risk Statements: 22-43
Safety Statements: 36/37
WGK Germany: 3
HS Code: 2914790090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H334May cause allergy or asthma symptoms or breathing difficulties if inhaled

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P342+P311IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 681652
Product name: 6-(Trifluoromethyl)-1-indanone
Purity: 97%
Packaging: 1g
Price: $115
Updated: 2022/05/15

TRC

Product number: T899628
Product name: 6-(Trifluoromethyl)-1-indanone
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: PC906472
Product name: 6-(Trifluoromethyl)-1-indanone
Purity: 98%
Packaging: 250mg
Price: $116
Updated: 2021/12/16

Apolloscientific

Product number: PC906472
Product name: 6-(Trifluoromethyl)-1-indanone
Purity: 98%
Packaging: 1g
Price: $212
Updated: 2021/12/16

AK Scientific

Product number: 0618AC
Product name: 6-(Trifluoromethyl)-1-indanone
Packaging: 5g
Price: $397
Updated: 2021/12/16

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6-(Trifluoromethyl)-1-indanone Chemical Properties,Usage,Production

Uses

6-(Trifluoromethyl)-1-indanone is a useful research chemical compound used as a reactant in the enantioselective synthesis of homoallylic azides and nitriles.

Synthesis

68755-36-2

68755-37-3

Step D: Synthesis of 6-(trifluoromethyl)-1-indanone To a mixed solution of 3-(2-bromo-4-(trifluoromethyl)phenyl)propanoic acid (6.40 g, 21.5 mmol) in THF (300 mL) and hexane (80 mL) was slowly added a 2.5 M n-butyllithium hexane solution (19 mL) at -78°C. The reaction mixture was stirred at this temperature for 15 minutes and then carefully poured into 2N HCl solution (150 mL) to terminate the reaction. The organic and aqueous layers were separated and the aqueous layer was extracted with ether. All organic layers were combined, washed sequentially with NaHCO3 solution, water and brine, dried over anhydrous MgSO4 and concentrated. Purification by silica gel column chromatography (eluent: 10-20% ethyl acetate in hexane solution) afforded 6-(trifluoromethyl)-1-indanone (2.2 g, yield 51%) as an oil.MS (ESI) calculated value of C10H7F3O(M+H)+: 201.0; measured value: 201.0.

References

[1] Patent: US2005/261310, 2005, A1. Location in patent: Page/Page column 22
[2] Patent: US4132737, 1979, A

6-(Trifluoromethyl)-1-indanone Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-(Trifluoromethyl)-1-indanone manufacturers

Career Henan Chemical Co

Product: 6-(Trifluoromethyl)-1-indanone 68755-37-3
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-09

68755-37-3, 6-(Trifluoromethyl)-1-indanoneRelated Search:

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68755-37-3