ChemicalBook > CAS DataBase List > 1H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI)

1H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI)

Product Name: 1H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI)
CAS No.: 340702-10-5
Chemical Name: 1H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI)
Synonyms: 6-fluoroisoindolin-one;6-Fluoro-1-isoindolinone;6-fluoroisoindolin-1-one;6-Fluoro-2,3-dihydro-isoindol-1-one;6-Fluoro-2,3-dihydro-1H-isoindol-1-one;1H-Isoindol-1-one,6-fluoro-2,3-dihydro-;H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI);1H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI);TERT-BUTYL4-(2-(2-HYDROXYETHOXY)ETHYL)PIPERAZINE-4-CARBOXYLATE
CBNumber: CB11293523
Molecular Formula: C8H6FNO
Formula Weight: 151.14
MOL File: 340702-10-5.mol

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1H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI) Property

storage temp.: 2-8°C
form: Solid
Appearance: White to light yellow Solid
InChI: InChI=1S/C8H6FNO/c9-6-2-1-5-4-10-8(11)7(5)3-6/h1-3H,4H2,(H,10,11)
InChIKey: TWGFYAUQRMVTSI-UHFFFAOYSA-N
SMILES: C1(=O)C2=C(C=CC(F)=C2)CN1
CAS DataBase Reference: 340702-10-5

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: F402395
Product name: 6-Fluoroisoindolin-1-one
Packaging: 250mg
Price: $110
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-3-88
Product name: 6-Fluoro-2,3-dihydro-1H-isoindol-1-one
Purity: 96%
Packaging: 250mg
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: PC450035
Product name: 6-Fluoro-2,3-dihydro-1H-isoindol-1-one
Packaging: 250mg
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: PC450035
Product name: 6-Fluoro-2,3-dihydro-1H-isoindol-1-one
Packaging: 1g
Price: $195
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H48-3-88
Product name: 6-Fluoro-2,3-dihydro-1H-isoindol-1-one
Purity: 96%
Packaging: 1g
Price: $195
Updated: 2021/12/16

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1H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI) Chemical Properties,Usage,Production

Synthesis

606080-43-7

340702-10-5

The general procedure for the synthesis of 6-fluoroisoindolin-1-one from methyl 2-cyano-5-fluorobenzoate was as follows: methyl 2-cyano-5-fluorobenzoate (10 g, 56 mmol) was dissolved in methanol (200 mL) at room temperature, followed by the addition of 10% palladium carbon catalyst (1.0 g). The reaction mixture was placed in a hydrogen (50 psi) atmosphere and the reaction was stirred overnight. Upon completion of the reaction, the catalyst was removed by diatomaceous earth filtration and the filtrate was concentrated under reduced pressure to afford the target product 6-fluoroisoindolin-1-one as a colorless solid (8.0 g, 90% yield). Mass spectrometry (electrospray ionization): m/z calculated value C8H7FNO [M+H]+ 152, measured value 152.

References

[1] Patent: US2017/144996, 2017, A1. Location in patent: Paragraph 0141; 0144;l 0145
[2] Patent: WO2017/87607, 2017, A1. Location in patent: Paragraph 0190
[3] Patent: WO2017/87610, 2017, A1. Location in patent: Paragraph 0127

1H-Isoindol-1-one,6-fluoro-2,3-dihydro-(9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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