2-Bromo-5-methoxybenzonitrile

ChemicalBook > CAS DataBase List > 2-Bromo-5-methoxybenzonitrile

2-Bromo-5-methoxybenzonitrile

Product Name: 2-Bromo-5-methoxybenzonitrile
CAS No.: 138642-47-4
Chemical Name: 2-Bromo-5-methoxybenzonitrile
Synonyms: KML-45;4-Bromo-3-cyanoanisole;2-BROMO-5-METHOXYBENZONITRILE;Benzonitrile, 2-bromo-5-methoxy-;2-BroMo-5-Methoxybenzonitrile 97%;4-Bromo-3-cyanoanisole, 6-Bromo-m-anisonitrile
CBNumber: CB11484530
Molecular Formula: C8H6BrNO
Formula Weight: 212.04
MOL File: 138642-47-4.mol

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2-Bromo-5-methoxybenzonitrile Property

Melting point:: 99-102 °C
Boiling point:: 292.8±30.0 °C(Predicted)
Density: 1.56±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
form: solid
color: peachy
CAS DataBase Reference: 138642-47-4

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Safety

Hazard Codes: Xn
Risk Statements: 22
Safety Statements: 36/37
RIDADR: UN3439
WGK Germany: 3
HazardClass: 6.1
PackingGroup: III
HS Code: 29269090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H312Harmful in contact with skin

H315Causes skin irritation

H319Causes serious eye irritation

H331Toxic if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 701149
Product name: 2-Bromo-5-methoxybenzonitrile
Purity: 97%
Packaging: 1g
Price: $37.8
Updated: 2021/12/16

Sigma-Aldrich

Product number: 701149
Product name: 2-Bromo-5-methoxybenzonitrile
Purity: 97%
Packaging: 5g
Price: $130
Updated: 2021/12/16

Alfa Aesar

Product number: H50608
Product name: 2-Bromo-5-methoxybenzonitrile, 98%
Packaging: 250mg
Price: $56.65
Updated: 2024/03/01

Alfa Aesar

Product number: H50608
Product name: 2-Bromo-5-methoxybenzonitrile, 98%
Packaging: 1g
Price: $171
Updated: 2021/12/16

TRC

Product number: B696600
Product name: 2-Bromo-5-methoxybenzonitrile
Packaging: 1g
Price: $75
Updated: 2021/12/16

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2-Bromo-5-methoxybenzonitrile Chemical Properties,Usage,Production

Uses

2-Bromo-5-methoxybenzonitrile (10.0 g, 47.2 mmol) was dissolved in dry tetrahydrofuran (100 mL) in a flame-dried flask and cooled in an ice bath. A solution of borane in tetrahydrofuran (75 mL, 75 mmol, 1.0 M) was added dropwise over 30 minutes. The reaction mixture was stirred overnight at rt, then quenched slowly with ice water and Na2CO3 (saturated aqueous solution). After removing THF, the residue was extracted with large amounts of EtOAc three times. The combined organic layers were washed with water, dried, and concentrated to give the crude, which was purified by silica gel column chromatography to give 1-(2-Bromo-5-methoxyphenyl)methanamine as a white powder (3.65 g, 36%).

2-Bromo-5-methoxybenzonitrile Preparation Products And Raw materials

Raw materials

Preparation Products

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