ChemicalBook > CAS DataBase List > 4-IODOBUTYL ACETATE

4-IODOBUTYL ACETATE

Product Name
4-IODOBUTYL ACETATE
CAS No.
40596-44-9
Chemical Name
4-IODOBUTYL ACETATE
Synonyms
4-IODOBUTYL ACETATE;1-ACETOXY-4-IODOBUTANE;4-iodobutyl acetate 96%;4-ACETOXY-BUTAN-1-IODIDE;4-iodo-1-butanol acetate;1-Butanol, 4-iodo-, 1-acetate;4-Iodobutylacetate, 85%, tech.;4-Iodobutyl acetate, 97%, stab;ACETIC ACID 4-IODO-BUTYL ESTER;4-IODOBUTYL ACETATE, TECH., 85%
CBNumber
CB1210301
Molecular Formula
C6H11IO2
Formula Weight
242.05
MOL File
40596-44-9.mol
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4-IODOBUTYL ACETATE Property

Boiling point:
94-95 °C5.5 mm Hg(lit.)
Density 
1.61 g/mL at 25 °C(lit.)
refractive index 
n20/D 1.497(lit.)
Flash point:
195 °F
solubility 
Difficult to mix.
form 
liquid
color 
Light green turbid
Sensitive 
Light Sensitive
CAS DataBase Reference
40596-44-9(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36/37/39
WGK Germany 
3
HS Code 
29153900
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H227Combustible liquid

Precautionary statements

P403+P235Store in a well-ventilated place. Keep cool.

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N-Bromosuccinimide Price

Alfa Aesar
Product number
H31826
Product name
4-Iodobutyl acetate, 96%, stab. with copper
Packaging
10g
Price
$63.65
Updated
2024/03/01
Alfa Aesar
Product number
H31826
Product name
4-Iodobutyl acetate, 96%, stab. with copper
Packaging
50g
Price
$196.65
Updated
2024/03/01
SynQuest Laboratories
Product number
2123-H-02
Product name
4-Iodobutyl acetate
Packaging
50g
Price
$312
Updated
2021/12/16
SynQuest Laboratories
Product number
2123-H-02
Product name
4-Iodobutyl acetate
Packaging
10g
Price
$141
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0023951
Product name
4-IODOBUTYLACETATE
Purity
95.00%
Packaging
10G
Price
$166.32
Updated
2021/12/16
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4-IODOBUTYL ACETATE Chemical Properties,Usage,Production

Chemical Properties

CLEAR DARK BROWN LIQUID

Uses

4-Iodobutyl acetate is used in the preparation of tricyclohexyl(acetoxybutyl))phosphonium iodide, tri-n-hexyl(acetoxybutyl))phosphonium iodide

Synthesis Reference(s)

Synthetic Communications, 24, p. 951, 1994 DOI: 10.1080/00397919408020770

Synthesis

The synthesis of 4-IODOBUTYL ACETATE is as follows:Acetic acid (0.30mmol, 1.0 equivalent), CuI (0.03mmol, 10.0mol%, 5.7mg) and NaI (0.60mmol, 2.0 equivalent, 89.9mg) were added to a 10mL Schlenk tube equipped with a magnetic stirring device. Vacuum the flask with a pump and backfill it three times with nitrogen. Then, 1.0 mL tetrahydrofuran (12.30 mmol, 41.0 equivalence, 1 mL, c=0.30 M), deionized water (0.45 mmol, 1.5 equivalence) and TMSCF3 (0.36 mmol, 1.2 equivalence) were added under N2 atmosphere. The mixture is stirred at 150°C (thermostatic oil bath pot) for 12 hours. After cooling to room temperature, dilute the mixture with ethyl acetate (15 mL), wash with water and brine, and dry on anhydrousNa2SO4. After Extraction by EtOAc (5 mL x 3), the combined organic layer was dehydrated with anhydrousNa2SO4 and concentrated under reduced pressure. The crude product is purified by rapid chromatography on silica gel to obtain alkyl iodide.

4-IODOBUTYL ACETATE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-IODOBUTYL ACETATE Suppliers

Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44688
Advantage
61
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42958
Advantage
64
Jingjiang Connect Chemical Manufacture Co., Ltd
Tel
0523-80501690 15252623102
Fax
0523-84506952
Email
andy@katchemical.com
Country
China
ProdList
164
Advantage
62
Mashilabs (Shanghai) Co.,Ltd.
Tel
19916721580
Fax
QQ:3154870176
Email
mafarm@126.com
Country
China
ProdList
4296
Advantage
58
Shanghai HuanChuan Industry Co.,Ltd.
Tel
021-61478794
Fax
021-61478794
Email
sales@hcshhai.com
Country
China
ProdList
9793
Advantage
50
Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
Email
sales@amadischem.com
Country
China
ProdList
131957
Advantage
58
Yantai ShengKailun Chemical Technology Co., Ltd.
Tel
13356901049
Fax
QQ:1025383091
Email
3119594100@qq.com
Country
China
ProdList
7964
Advantage
55
Zhengzhou Huiju Chemical Co., Ltd.
Tel
0371-55900031 18137872243
Fax
QQ:2853979815
Email
2853979815@qq.com
Country
China
ProdList
10009
Advantage
55
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View Lastest Price from 4-IODOBUTYL ACETATE manufacturers

Hebei Mojin Biotechnology Co., Ltd
Product
4-IODOBUTYL ACETATE 40596-44-9
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
50000KG/month
Release date
2023-07-27
Zhuozhou Wenxi import and Export Co., Ltd
Product
4-IODOBUTYL ACETATE 40596-44-9
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-08-11

40596-44-9, 4-IODOBUTYL ACETATERelated Search:


  • 1-ACETOXY-4-IODOBUTANE
  • 4-ACETOXY-BUTAN-1-IODIDE
  • 4-IODOBUTYL ACETATE
  • 4-IODOBUTYL ACETATE, TECH., 85%
  • ACETIC ACID 4-IODO-BUTYL ESTER
  • 4-iodo-1-butanol acetate
  • 4-Iodobutylacetate, 85%, tech.
  • 4-Iodobutylacetate1-Acetoxy-4-iodobutane
  • 4-Iodobutyl acetate, 97%, stab
  • 4-Iodobutyl acetate, 97%, stab. with copper
  • 4-Iodobutyl acetate, stabilized with copper
  • 4-Iodobutyl acetate, 96%, stab. with copper
  • 4-Iodobutyl acetate,stab. with copper
  • 4-iodobutyl acetate 96%
  • 1-Butanol, 4-iodo-, 1-acetate
  • 40596-44-9
  • C6H11IO2
  • CH3CO2CH24I
  • Carbonyl Compounds
  • C6 to C7
  • Building Blocks
  • Esters
  • Organic Building Blocks
  • Building Blocks
  • C6 to C7
  • Carbonyl Compounds
  • Chemical Synthesis
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