4-IODOBUTYL ACETATE

Product Name: 4-IODOBUTYL ACETATE
CAS No.: 40596-44-9
Chemical Name: 4-IODOBUTYL ACETATE
Synonyms: 4-IODOBUTYL ACETATE;1-ACETOXY-4-IODOBUTANE;4-iodobutyl acetate 96%;4-ACETOXY-BUTAN-1-IODIDE;4-iodo-1-butanol acetate;1-Butanol, 4-iodo-, 1-acetate;4-Iodobutylacetate, 85%, tech.;4-Iodobutyl acetate, 97%, stab;ACETIC ACID 4-IODO-BUTYL ESTER;4-IODOBUTYL ACETATE, TECH., 85%
CBNumber: CB1210301
Molecular Formula: C6H11IO2
Formula Weight: 242.05
MOL File: 40596-44-9.mol

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4-IODOBUTYL ACETATE Property

Boiling point:: 94-95 °C5.5 mm Hg(lit.)
Density: 1.61 g/mL at 25 °C(lit.)
refractive index: n20/D 1.497(lit.)
Flash point:: 195 °F
solubility: Difficult to mix.
form: liquid
color: Light green turbid
Sensitive: Light Sensitive
CAS DataBase Reference: 40596-44-9(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
WGK Germany: 3
HS Code: 29153900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H227Combustible liquid
Precautionary statements: P403+P235Store in a well-ventilated place. Keep cool.

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N-Bromosuccinimide Price

Alfa Aesar

Product number: H31826
Product name: 4-Iodobutyl acetate, 96%, stab. with copper
Packaging: 10g
Price: $63.65
Updated: 2024/03/01

Alfa Aesar

Product number: H31826
Product name: 4-Iodobutyl acetate, 96%, stab. with copper
Packaging: 50g
Price: $196.65
Updated: 2024/03/01

SynQuest Laboratories

Product number: 2123-H-02
Product name: 4-Iodobutyl acetate
Packaging: 10g
Price: $141
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0023951
Product name: 4-IODOBUTYLACETATE
Purity: 95.00%
Packaging: 10G
Price: $166.32
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2123-H-02
Product name: 4-Iodobutyl acetate
Packaging: 50g
Price: $312
Updated: 2021/12/16

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4-IODOBUTYL ACETATE Chemical Properties,Usage,Production

Chemical Properties

CLEAR DARK BROWN LIQUID

Uses

4-Iodobutyl acetate is used in the preparation of tricyclohexyl(acetoxybutyl))phosphonium iodide, tri-n-hexyl(acetoxybutyl))phosphonium iodide

Synthesis Reference(s)

Synthetic Communications, 24, p. 951, 1994 DOI: 10.1080/00397919408020770

Synthesis

The synthesis of 4-IODOBUTYL ACETATE is as follows:Acetic acid (0.30mmol, 1.0 equivalent), CuI (0.03mmol, 10.0mol%, 5.7mg) and NaI (0.60mmol, 2.0 equivalent, 89.9mg) were added to a 10mL Schlenk tube equipped with a magnetic stirring device. Vacuum the flask with a pump and backfill it three times with nitrogen. Then, 1.0 mL tetrahydrofuran (12.30 mmol, 41.0 equivalence, 1 mL, c=0.30 M), deionized water (0.45 mmol, 1.5 equivalence) and TMSCF3 (0.36 mmol, 1.2 equivalence) were added under N2 atmosphere. The mixture is stirred at 150°C (thermostatic oil bath pot) for 12 hours. After cooling to room temperature, dilute the mixture with ethyl acetate (15 mL), wash with water and brine, and dry on anhydrousNa2SO4. After Extraction by EtOAc (5 mL x 3), the combined organic layer was dehydrated with anhydrousNa2SO4 and concentrated under reduced pressure. The crude product is purified by rapid chromatography on silica gel to obtain alkyl iodide.

4-IODOBUTYL ACETATE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-IODOBUTYL ACETATE Suppliers

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View Lastest Price from 4-IODOBUTYL ACETATE manufacturers

Hebei Mojin Biotechnology Co., Ltd

Product: 4-IODOBUTYL ACETATE 40596-44-9
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50000KG/month
Release date: 2023-07-27

Zhuozhou Wenxi import and Export Co., Ltd

Product: 4-IODOBUTYL ACETATE 40596-44-9
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

40596-44-9, 4-IODOBUTYL ACETATERelated Search:

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1-ACETOXY-4-IODOBUTANE

4-ACETOXY-BUTAN-1-IODIDE

4-IODOBUTYL ACETATE

4-IODOBUTYL ACETATE, TECH., 85%

ACETIC ACID 4-IODO-BUTYL ESTER

4-iodo-1-butanol acetate

4-Iodobutylacetate, 85%, tech.

4-Iodobutylacetate1-Acetoxy-4-iodobutane

4-Iodobutyl acetate, 97%, stab

4-Iodobutyl acetate, 97%, stab. with copper

4-Iodobutyl acetate, stabilized with copper

4-Iodobutyl acetate, 96%, stab. with copper

4-Iodobutyl acetate,stab. with copper

4-iodobutyl acetate 96%

1-Butanol, 4-iodo-, 1-acetate

40596-44-9

C6H11IO2

CH3CO2CH24I

Carbonyl Compounds

C6 to C7

Building Blocks

Esters

Organic Building Blocks

Building Blocks

C6 to C7

Carbonyl Compounds

Chemical Synthesis

Esters

Organic Building Blocks