1-METHYL-5-NITRO-1H-INDAZOLE

Product Name: 1-METHYL-5-NITRO-1H-INDAZOLE
CAS No.: 5228-49-9
Chemical Name: 1-METHYL-5-NITRO-1H-INDAZOLE
Synonyms: SW-35;SWF-35;1-METHYL-5-NITROINDAZOLE;1-METHYL-5-NITRO-1H-INDAZOLE;5-Nitro-1-methyl-1H-indazole;1H-Indazole, 1-methyl-5-nitro-;1-METHYL-5-NITRO-1H-INDAZOLE, 98+%;1-methyl-5-nitro-1H-indazole, 1-methyl-5-nitroindazole, 1-methyl-5-nitro-1H-indazole, 1-Methyl-5-nitro-1H-indazol, 1-methyl-5-nitro-indazole, 1-Methyl-5-nitro-indazol, 1-Methyl-5-nitroindazol
CBNumber: CB1239421
Molecular Formula: C8H7N3O2
Formula Weight: 177.16
MOL File: 5228-49-9.mol

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1-METHYL-5-NITRO-1H-INDAZOLE Property

Melting point:: 161-162°C
Boiling point:: 332.9±15.0 °C(Predicted)
Density: 1.42±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: solid
pka: -0.82±0.30(Predicted)
color: yellow
BRN: 168080
CAS DataBase Reference: 5228-49-9(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 20/22-68
Safety Statements: 22-36/37
RIDADR: 2811
HazardClass: IRRITANT
PackingGroup: II
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H302Harmful if swallowed

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N-Bromosuccinimide Price

TRC

Product number: M218795
Product name: 1-Methyl-5-nitro-1H-indazole
Packaging: 500mg
Price: $75
Updated: 2021/12/16

Apolloscientific

Product number: OR14146
Product name: 1-Methyl-5-nitro-1H-indazole
Packaging: 250mg
Price: $15
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-1-V8
Product name: 1-Methyl-5-nitro-1H-indazole
Packaging: 250mg
Price: $16
Updated: 2021/12/16

Apolloscientific

Product number: OR14146
Product name: 1-Methyl-5-nitro-1H-indazole
Packaging: 1g
Price: $28
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-1-V8
Product name: 1-Methyl-5-nitro-1H-indazole
Packaging: 1g
Price: $31
Updated: 2021/12/16

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1-METHYL-5-NITRO-1H-INDAZOLE Chemical Properties,Usage,Production

Synthesis

5401-94-5

74-88-4

5228-48-8

5228-49-9

GENERAL METHOD: Cesium carbonate (12.26 mmol) was added to a solution of 5-nitroindazole (6.13 mmol) in tetrahydrofuran (THF; 25 mL) at 0 °C. The reaction mixture was stirred at 0 °C for 15 min before iodomethane or allyl bromide (6.13 mmol) was added dropwise. The progress of the reaction was monitored by thin layer chromatography (TLC) until the starting material completely disappeared. After completion of the reaction, the mixture was concentrated. The crude product was dissolved in ethyl acetate (EtOAc; 50 mL), washed sequentially with water and brine, and the organic phase was dried over anhydrous magnesium sulfate (MgSO?). The solvent was removed by evaporation under reduced pressure, and the resulting residue was purified by silica gel column chromatography with ethyl acetate/hexane (3:7, v/v) as eluent to afford 1-alkyl-5-nitroindazole and 2-alkyl-5-nitroindazole, respectively.

References

[1] Synthetic Communications, 2015, vol. 45, # 17, p. 2005 - 2013
[2] Tetrahedron, 2008, vol. 64, # 28, p. 6711 - 6723
[3] Patent: US2014/371219, 2014, A1. Location in patent: Paragraph 0659; 0660; 0661
[4] Patent: WO2016/57834, 2016, A1. Location in patent: Paragraph 000406

1-METHYL-5-NITRO-1H-INDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-METHYL-5-NITRO-1H-INDAZOLE Suppliers

China 104 France 1 Germany 2 India 3 The Netherlands 2 United Kingdom 6 United States 22 Global 140

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View Lastest Price from 1-METHYL-5-NITRO-1H-INDAZOLE manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 1-METHYL-5-NITRO-1H-INDAZOLE 5228-49-9
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: 1-METHYL-5-NITRO-1H-INDAZOLE 5228-49-9
Price: US $0.10/KG
Min. Order: 1KG
Purity: 95%-99%
Supply Ability: 1kg; 50kg; 500kg
Release date: 2019-12-24

5228-49-9, 1-METHYL-5-NITRO-1H-INDAZOLERelated Search:

tert-butyl 4-(4-broMothiazol-2-yl)piperazine-1-carboxylate (6-Methylpyridazin-3-yl)MethanaMine dihydrochloride No Chinese name rac-4-(6-chloro-2-oxo-2,3-dihydro-1H-indol-3-yl)-piperidine-1-carboxylic acid tert-butyl 5-METHYL-4,5,6,7-TETRAHYDRO[1,3]THIAZOLO[5,4-C]PYRIDIN-2-AMINE 2,4-dichloro-7H-Pyrrolo[2,3-d]pyriMidine-7-carboxylic acid 1,1-diMethylethyl ester 5-BROMO-2-METHYL-3-NITROPHENYL METHYLCARBOXYLATE 1H-Pyrrolo[2,3-b]pyridine, 2-methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)- Pyrrolidine-3-carboxaMide hydrochloride 5-Bromoindazole (2R,5S)-tert-butyl 4-benzyl-2,5-diMethylpiperazine-1-carboxylate 2-cyclopylcyclopropane-1-carboxylic acid 4-FLUORO-2-HYDROXYBENZALDEHYDE 4-CYANO-7-AZAINDOLE 5-Bromoindole (+/-)-BOC-ALPHA-PHOSPHONOGLYCINE TRIMETHYL ESTER 1-Boc-4-(Hydroxymethyl)-4-methyl-piperidine 4-CYANOPYRAZOLE

1-METHYL-5-NITROINDAZOLE

1-METHYL-5-NITRO-1H-INDAZOLE

1-methyl-5-nitro-1H-indazole, 1-methyl-5-nitroindazole, 1-methyl-5-nitro-1H-indazole, 1-Methyl-5-nitro-1H-indazol, 1-methyl-5-nitro-indazole, 1-Methyl-5-nitro-indazol, 1-Methyl-5-nitroindazol

1-METHYL-5-NITRO-1H-INDAZOLE, 98+%

5-Nitro-1-methyl-1H-indazole

1H-Indazole, 1-methyl-5-nitro-

SWF-35

SW-35

5228-49-9

Indazoles