2-Chloro-7-Methoxyquinoline

Product Name: 2-Chloro-7-Methoxyquinoline
CAS No.: 49609-15-6
Chemical Name: 2-Chloro-7-Methoxyquinoline
Synonyms: 2-Chloro-7-Methoxyquinoline;QUINOLINE, 2-CHLORO-7-METHOXY-
CBNumber: CB12618060
Molecular Formula: C10H8ClNO
Formula Weight: 193.63
MOL File: 49609-15-6.mol

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2-Chloro-7-Methoxyquinoline Property

Melting point:: 97-98 °C
Boiling point:: 145 °C(Press: 0.6 Torr)
Density: 1.267±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 0.65±0.50(Predicted)
Appearance: Off-white to light brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C632238
Product name: 2-Chloro-7-methoxyquinoline
Packaging: 10mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C632238
Product name: 2-Chloro-7-methoxyquinoline
Packaging: 50mg
Price: $130
Updated: 2021/12/16

TRC

Product number: C632238
Product name: 2-Chloro-7-methoxyquinoline
Packaging: 100mg
Price: $200
Updated: 2021/12/16

AK Scientific

Product number: 6723AB
Product name: 2-Chloro-7-methoxyquinoline
Packaging: 100mg
Price: $341
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0363643
Product name: 2-CHLORO-7-METHOXYQUINOLINE
Purity: 95.00%
Packaging: 5MG
Price: $501.77
Updated: 2021/12/16

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2-Chloro-7-Methoxyquinoline Chemical Properties,Usage,Production

Synthesis

23981-26-2

49609-15-6

General procedure: 300 mg (1.9 mmol) of 7-methoxyquinolin-2(1H)-one was dissolved in 1.1 mL of phosphorus oxychloride (POCl3, 12 mmol) and the reaction was heated to reflux for 3 hours. Upon completion of the reaction, the reaction mixture was slowly poured into ice water, neutralized to neutral with saturated sodium bicarbonate (NaHCO3) solution and subsequently extracted with ethyl acetate. After treatment, the target product 2-chloro-7-methoxyquinoline was obtained in 98% yield. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3): δ 8.01 (d, J = 8.5 Hz, 1H), 7.68 (d, J = 8.9 Hz, 1H), 7.35 (d, J = 2.4 Hz, 1H), 7.25 (d, J = 8.3 Hz, 1H), 7.20 (dd, J = 8.9, 2.5 Hz, 1H), and 3.93 (s, 3H).

References

[1] Patent: WO2016/130968, 2016, A1. Location in patent: Page/Page column 183-184
[2] Patent: WO2014/85284, 2014, A1. Location in patent: Paragraph 00222

2-Chloro-7-Methoxyquinoline Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Chloro-7-Methoxyquinoline Suppliers

China 46 United States 1 Global 47

SynAsst Chemical.

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View Lastest Price from 2-Chloro-7-Methoxyquinoline manufacturers

Career Henan Chemical Co

Product: 2-Chloro-7-Methoxyquinoline 49609-15-6
Price: US $2.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 100g , 1kg, 5kg , 50kg
Release date: 2020-01-07

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2-Chloro-7-Methoxyquinoline

QUINOLINE, 2-CHLORO-7-METHOXY-

49609-15-6