ChemicalBook > CAS DataBase List > 2-Chloroveratraldehyde

2-Chloroveratraldehyde

Product Name: 2-Chloroveratraldehyde
CAS No.: 5417-17-4
Chemical Name: 2-Chloroveratraldehyde
Synonyms: TIMTEC-BB SBB003539;Vanillin Impurity 20;2-CHLOROVERATRALDEHYDE;LABOTEST-BB LT01147597;2-Chlorveratrumaldehyd;2‐Chlorovanillin methyl ether;2-Chloro-3,4-dimethoxybenzalde;2-CHLORO-3,4-DIMETHOXYBENZALDEHYDE;2-CHLORO-3,4-DIMETHOXYBENZALDE 98%;Benzaldehyde, 2-chloro-3,4-dimethoxy-
CBNumber: CB1386257
Molecular Formula: C9H9ClO3
Formula Weight: 200.62
MOL File: 5417-17-4.mol

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2-Chloroveratraldehyde Property

Melting point:: 71-74 °C (lit.)
Boiling point:: 300.9±37.0 °C(Predicted)
Density: 1.245±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
solubility: Chloroform (Sparingly), Ethyl Acetate (Slightly)
form: Solid
color: White to Pale Yellow
Sensitive: Air Sensitive
BRN: 2109344
InChI: InChI=1S/C9H9ClO3/c1-12-7-4-3-6(5-11)8(10)9(7)13-2/h3-5H,1-2H3
InChIKey: SAWHDJTZESXNMM-UHFFFAOYSA-N
SMILES: C(=O)C1=CC=C(OC)C(OC)=C1Cl
CAS DataBase Reference: 5417-17-4(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 37/39-26
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 29124900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 566004
Product name: 2-Chloro-3,4-dimethoxybenzaldehyde
Purity: 98%
Packaging: 5g
Price: $209
Updated: 2023/01/07

TCI Chemical

Product number: C1997
Product name: 2-Chloro-3,4-dimethoxybenzaldehyde
Purity: >98.0%(GC)
Packaging: 5g
Price: $42
Updated: 2025/07/31

TCI Chemical

Product number: C1997
Product name: 2-Chloro-3,4-dimethoxybenzaldehyde
Purity: >98.0%(GC)
Packaging: 25g
Price: $96
Updated: 2025/07/31

TRC

Product number: C427660
Product name: 2-Chloro-3,4-dimethoxybenzaldehyde
Packaging: 25g
Price: $250
Updated: 2021/12/16

AK Scientific

Product number: J96165
Product name: 2-Chloro-3,4-dimethoxybenzaldehyde
Packaging: 25g
Price: $75
Updated: 2021/12/16

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2-Chloroveratraldehyde Chemical Properties,Usage,Production

Chemical Properties

beige-yellow to beige crystalline powder

Uses

2-Chloro-3,4-dimethoxybenzaldehyde is a useful reagent in the synthesis of the human TLR4 agonist euodenine A. 2-Chloro-3,4-dimethoxybenzaldehyde is also used as a reagent in the synthesis of novel 2-methoxyacylhydrazones as potent, selective PDE10A inhibitors with activity in animal models of schizophrenia.

Synthesis

37687-57-3

74-88-4

5417-17-4

Step 2 - Formation of 2-chloro-3,4-dimethoxybenzaldehyde: To a 100 mL solution of 8.03 g (43 mmol) of 2-chloro-3-hydroxy-4-methoxybenzaldehyde in acetonitrile was added 7.7 g (55 mmol) of powdered potassium carbonate, followed by the addition of 8.3 mL (0.13 mol) of iodomethane. The reaction mixture was slowly heated to reflux and stirred continuously at this temperature for 24 hours. Upon completion of the reaction, it was cooled to room temperature, the suspension was filtered and the filtrate was evaporated under vacuum to remove the solvent to give 8.5 g (42 mmol, 98% yield) of white solid. The resulting solid was confirmed to be 2-chloro-3,4-dimethoxybenzaldehyde by 1H NMR analysis.

References

[1] Synlett, 2014, vol. 25, # 20, p. 2891 - 2894
[2] Patent: US5866513, 1999, A

2-Chloroveratraldehyde Preparation Products And Raw materials

Raw materials

Isovanillin Potassium hydroxide Acetone Manganese dioxide Potassium carbonate Carbon tetrachloride Ethyl acetate Hydrochloric acid Isopropyl alcohol Iodomethane

Preparation Products

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View Lastest Price from 2-Chloroveratraldehyde manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 2-Chloroveratraldehyde 5417-17-4
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-12-04

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Chloroveratraldehyde 5417-17-4
Price: US $0.00-0.00/g
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-15

Career Henan Chemical Co

Product: 2-Chloroveratraldehyde 5417-17-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-31

5417-17-4, 2-ChloroveratraldehydeRelated Search:

2,5-Dimethoxybenzaldehyde 2,3-Dimethoxybenzaldehyde 3,5-Dimethoxybenzaldehyde Veratraldehyde 2,4-Dimethoxybenzaldehyde Diphenyldimethoxysilane p-Anisaldehyde 3-Methoxybenzaldehyde 4-Dimethylaminobenzaldehyde 2,6-Dimethoxybenzaldehyde Dimethyldimethoxysilane 1,1-Dimethoxyethane o-Anisaldehyde Difluorochloromethane Quincarbate 5-CHLORO-2 3-DIMETHOXYBENZALDEHYDE 2-CHLORO-4,6-DIMEHOXYBENZALDEHYDE ETHYL 2-CHLORO-3,4-DIMETHOXYBENZOATE

LABOTEST-BB LT01147597

2-CHLORO-3,4-DIMETHOXYBENZALDEHYDE

2-CHLOROVERATRALDEHYDE

TIMTEC-BB SBB003539

2-Chloro-3,4-dimethoxybenzalde

2-CHLORO-3,4-DIMETHOXYBENZALDE 98%

2‐Chlorovanillin methyl ether

2-Chloro-3,4-dimethoxybenzaldehyde,98%

(1S,2S)-1-[(2S)-2-oxiranyl]-2-[(2R)-2-oxiranyl]ethane-1,2-diol

2-Chloro-3,4-dimethoxybenzaldehyde &gt

2-Chlorveratrumaldehyd

Benzaldehyde, 2-chloro-3,4-dimethoxy-

2-chloro vertaldehyde OR 2 chloro -3,4-dimethoxy benzaldehyde

Vanillin Impurity 20

5417-17-4

ALDEHYDE

Carbonyl Compounds

Building Blocks

Aldehydes

Organic Building Blocks

Fenoldopam

Benzaldehyde

(intermediate of fenoldopam)