ChemicalBook > CAS DataBase List > 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE

4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE

Product Name
4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE
CAS No.
175204-45-2
Chemical Name
4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE
Synonyms
BUTTPARK 43\57-20;4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE;Pyridine, 4-(bromomethyl)-2,6-dichloro-;4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE, TECH.;4-(Bromomethyl)-2,6-Dichloro-Pyridine 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE, TECH.
CBNumber
CB1395480
Molecular Formula
C6H4BrCl2N
Formula Weight
240.91
MOL File
175204-45-2.mol
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4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE Property

Boiling point:
299.2±35.0 °C(Predicted)
Density 
1.770±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka
-3.01±0.10(Predicted)
form 
Crystalline Powder
color 
Yellow
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Safety

Hazard Codes 
T
Risk Statements 
36/37/38
Safety Statements 
26-36/37/39
HS Code 
29333999
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B808163
Product name
4-(Bromomethyl)-2,6-dichloropyridine
Packaging
50mg
Price
$60
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB53490
Product name
4-(Bromomethyl)-2,6-dichloropyridine
Packaging
50mg
Price
$50
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB53490
Product name
4-(Bromomethyl)-2,6-dichloropyridine
Packaging
100mg
Price
$80
Updated
2021/12/16
Apolloscientific
Product number
OR27145
Product name
4-(Bromomethyl)-2,6-dichloropyridine
Packaging
1g
Price
$131
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-D-Z6
Product name
4-(Bromomethyl)-2,6-dichloropyridine
Packaging
1g
Price
$144
Updated
2021/12/16
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4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE Chemical Properties,Usage,Production

Synthesis

101990-69-6

175204-45-2

General procedure for the synthesis of 4-bromomethyl-2,6-dichloropyridine using 2,6-dichloropyridine-4-methanol as starting material: a tetrahydrofuran solution of (2,6-dichloropyridin-4-yl)methanol was mixed with triphenylphosphine and N-bromosuccinimide at 0 °C, maintained at this temperature and the reaction mixture was stirred. After 2 hours of reaction, the reaction mixture was diluted with water and extracted with ethyl acetate (3 x 150 mL). The organic phases were combined and washed with brine (2 x 100 mL) and subsequently dried over anhydrous sodium sulfate. The dried organic phase was filtered and concentrated to give the crude product. The crude product was purified by column chromatography to yield 1.1 g of 4-bromomethyl-2,6-dichloropyridine [0795] as a colorless liquid. Mass spectral analysis showed MS (M + 1)+ = 241.8.

References

[1] Patent: US2017/355708, 2017, A1. Location in patent: Paragraph 0193; 0195

4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE Suppliers

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View Lastest Price from 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE manufacturers

Career Henan Chemical Co
Product
4-(Bromomethyl)-2,6-dichloropyridine 175204-45-2
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
1ton
Release date
2020-01-10

175204-45-2, 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINERelated Search:


  • BUTTPARK 43\57-20
  • 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE, TECH.
  • 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE
  • 4-(Bromomethyl)-2,6-Dichloro-Pyridine 4-(BROMOMETHYL)-2,6-DICHLOROPYRIDINE, TECH.
  • Pyridine, 4-(bromomethyl)-2,6-dichloro-
  • 175204-45-2