2,6-DIBROMOANISOLE

Product Name: 2,6-DIBROMOANISOLE
CAS No.: 38603-09-7
Chemical Name: 2,6-DIBROMOANISOLE
Synonyms: 2,6-DIBROMOANISOLE;2,6-Dibromoanisole,>97%;2,6-Dibromo-1-methoxybenzene;1,3-Dibromo-2-methoxybenzene;Benzene,1,3-dibroMo-2-Methoxy-
CBNumber: CB1397570
Molecular Formula: C7H6Br2O
Formula Weight: 265.93
MOL File: 38603-09-7.mol

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2,6-DIBROMOANISOLE Property

Melting point:: 13°C
Boiling point:: 254℃
Density: 1.823
refractive index: 1.5920 to 1.5960
Flash point:: 100℃
storage temp.: Sealed in dry,Room Temperature
form: clear liquid
color: Colorless to Light yellow
InChI: InChI=1S/C7H6Br2O/c1-10-7-5(8)3-2-4-6(7)9/h2-4H,1H3
InChIKey: BMZVDHQOAJUZJL-UHFFFAOYSA-N
SMILES: C1(Br)=CC=CC(Br)=C1OC
CAS DataBase Reference: 38603-09-7

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Safety

HS Code: 2909303840

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D5279
Product name: 2,6-Dibromoanisole
Purity: >98.0%(GC)
Packaging: 1g
Price: $76
Updated: 2025/07/31

TCI Chemical

Product number: D5279
Product name: 2,6-Dibromoanisole
Purity: >98.0%(GC)
Packaging: 5g
Price: $227
Updated: 2025/07/31

TRC

Product number: D422975
Product name: 2,6-Dibromoanisole
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: D422975
Product name: 2,6-Dibromoanisole
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD142831
Product name: 1,3-Dibromo-2-methoxybenzene
Packaging: 250mg
Price: $62.5
Updated: 2021/12/16

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2,6-DIBROMOANISOLE Chemical Properties,Usage,Production

Uses

2,6-Dibromoanisole is an anisole compound containing a substituent bromine atom that can be used in bromine substitution reactions to prepare other organic ether derivatives. It is also a Lusutrombopag intermediate, which is used to treat thrombocytopenia (low platelets in the blood) in adult patients with chronic liver disease who are scheduled to undergo medical or dental procedures.

Synthesis

608-33-3

74-88-4

38603-09-7

Example 1 Preparation of 2,6-dibromo-4-(6-(3-bromobenzyloxy)pyridazin-3-yl)phenol (Compound 91): to a stirred solution of 2,6-dibromophenol (5.26 g, 20.9 mmol) in acetone (170 mL) was added anhydrous potassium carbonate (4.33 g, 31.3 mmol) and the mixture was stirred at room temperature for 30 minutes. Iodomethane (1.97 mL, 31.4 mmol) was then added and the reaction mixture was heated to reflux at 60 °C for 3 hours. After completion of the reaction, the mixture was filtered and the filtrate was concentrated by rotary evaporation. The residue was extracted by partitioning between petroleum ether (40-60 °C, 100 mL) and water (100 mL). The aqueous layer was extracted once more with petroleum ether (40-60 °C, 100 mL), and the organic phases were combined, washed with brine (50 mL), dried over anhydrous magnesium sulfate, filtered, and concentrated to afford 5.43 g (98% yield) of the target compound, 1 ,3-dibromo-2-methoxybenzene, as a colorless oil.1H NMR (CDCl3, δ ppm): 3.89 (3H, s), 6.86 (1H, t, J = 8.02 Hz), 7.50 (2H, d, J = 8.01 Hz).

References

[1] Tetrahedron Letters, 2008, vol. 49, # 33, p. 4912 - 4914
[2] Patent: US2009/270398, 2009, A1. Location in patent: Page/Page column 35
[3] Journal of the American Chemical Society, 2009, vol. 131, # 47, p. 17371 - 17375
[4] Journal of the American Chemical Society, 2016, vol. 138, # 31, p. 9779 - 9782
[5] Patent: WO2009/103440, 2009, A1. Location in patent: Page/Page column 75

2,6-DIBROMOANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,6-DIBROMOANISOLE Suppliers

Americas 1 Austria 1 Canada 1 China 103 Europe 1 Germany 3 India 2 Japan 1 Norway 1 United Kingdom 5 United States 12 Global 131

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View Lastest Price from 2,6-DIBROMOANISOLE manufacturers

Career Henan Chemical Co

Product: 2,6-DIBROMOANISOLE 38603-09-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-24

38603-09-7, 2,6-DIBROMOANISOLERelated Search:

2-Allyloxy-1,3,5-tribromobenzene 2,4,6-TRIBROMOPHENYL ACETATE Decabromodiphenyl oxide 1,2-Bis(2,4,6-tribromophenoxy)ethane BROMOXYNIL-METHYL ETHER 4,4'-Isopropylidenebis[2-(2,6-dibromophenoxy)ethanol] Bromoxynil octanoate Tetrabromobisphenol A bis(dibromopropyl ether) TRIBROMONEOPENTYL METHACRYLATE 3,5-DIBROMOANISOLE 2,4-DIBROMOANISOLE,2,4-Dibromoanisole, 98+%,4,6-Dibromoanisole 2,4-Dibromoanisole-5-boronic acid 2,4-Dibromoanisole-3-boronic acid 2,5-DIBROMOANISOLE BOC-3,5-DIBROMO-TYR(OBZL)-OH 2,4,6-TRIBROMO-3-METHOXYPHENOL 2,6-DIBROMO-4-FLUOROANISOLE 3,5-DIBROMO-4-METHOXYBENZOIC ACID

1,3-Dibromo-2-methoxybenzene

2,6-Dibromo-1-methoxybenzene

2,6-DIBROMOANISOLE

Benzene,1,3-dibroMo-2-Methoxy-

2,6-Dibromoanisole,>97%

38603-09-7

Anisole