3-(4-Chlorophenyl)glutaric acid

Product Name: 3-(4-Chlorophenyl)glutaric acid
CAS No.: 35271-74-0
Chemical Name: 3-(4-Chlorophenyl)glutaric acid
Synonyms: CBI-BB ZERO/006271;Baclofen impurity C;Baclofen Impurity 3;Baclofen Impurity 1;Baclofen EP Impurity C;3-(4-chlorophenyl) glutarate;-(4-Chlorophenyl)glutaricacid;-(p-Chlorophenyl)glutaric Acid;b-(p-Chlorophenyl)glutaric Acid;3-(4-CHLOROPHENYL)GLUTARIC ACID
CBNumber: CB1419706
Molecular Formula: C11H11ClO4
Formula Weight: 242.66
MOL File: 35271-74-0.mol

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3-(4-Chlorophenyl)glutaric acid Property

Melting point:: 164-166°C
Boiling point:: 394.4±27.0 °C(Predicted)
Density: 1.396±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
solubility: Soluble in dimethyl sulfoxide. Slightly soluble in methanol.
form: Solid
pka: 4.01±0.10(Predicted)
color: White to Light Yellow
BRN: 1976828
InChI: InChI=1S/C11H11ClO4/c12-9-3-1-7(2-4-9)8(5-10(13)14)6-11(15)16/h1-4,8H,5-6H2,(H,13,14)(H,15,16)
InChIKey: URXVLIVRJJNJII-UHFFFAOYSA-N
SMILES: C(O)(=O)CC(C1=CC=C(Cl)C=C1)CC(O)=O
CAS DataBase Reference: 35271-74-0(CAS DataBase Reference)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36
HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: C378250
Product name: 3-(4-Chlorophenyl)glutaricAcid
Packaging: 250mg
Price: $95
Updated: 2021/12/16

TRC

Product number: C378250
Product name: 3-(4-Chlorophenyl)glutaricAcid
Packaging: 1g
Price: $120
Updated: 2021/12/16

TRC

Product number: C378250
Product name: 3-(4-Chlorophenyl)glutaricAcid
Packaging: 5g
Price: $135
Updated: 2021/12/16

TRC

Product number: C378250
Product name: 3-(4-Chlorophenyl)glutaricAcid
Packaging: 10g
Price: $155
Updated: 2021/12/16

AK Scientific

Product number: J50023
Product name: 3-(4-Chlorophenyl)glutaricacid
Packaging: 25g
Price: $22
Updated: 2021/12/16

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3-(4-Chlorophenyl)glutaric acid Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

3-(4-Chlorophenyl)glutaric Acid (cas# 35271-74-0) is a compound useful in organic synthesis. Baclofen Impurity 1

Synthesis

19411-80-4

35271-74-0

The general procedure for the synthesis of 3-(4-chlorophenyl)glutaric acid using baclofen impurity 9 as starting material: the intermediate Π was dissolved in 420 mL of a 30 N aqueous solution of potassium hydroxide and the reaction was stirred for 2 hr at 85-90 °C. The reaction process was monitored by thin layer chromatography (TLC) and the unfolding agent was a mixture of ethyl acetate and petroleum ether (2:3, v/v). After completion of the reaction, the reaction mixture was cooled to room temperature and 400 mL of dichloromethane and 500 mL of deionized water were added sequentially. After stirring for 20 min, the organic and aqueous layers were separated and the organic layer was discarded. The aqueous layer was acidified to pH 1-2 with 6 M hydrochloric acid and the precipitated solid was subsequently filtered. The solid was washed with deionized water and dried under vacuum at 55-60°C for 5 h to give 157 g of white solid intermediate in 86.4% yield. The melting point of the intermediate was 166.5~167.3 °C.

References

[1] Patent: CN106187794, 2016, A. Location in patent: Paragraph 0023; 0028

3-(4-Chlorophenyl)glutaric acid Preparation Products And Raw materials

Raw materials

Preparation Products

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Hebei Chuanghai Biotechnology Co., Ltd

Product: 3-(4-Chlorophenyl)glutaric acid 35271-74-0
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 500000kg
Release date: 2024-10-29

Henan Aochuang Chemical Co.,Ltd.

Product: 3-(4-Chlorophenyl)glutaric acid 35271-74-0
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-10

Hebei Yanxi Chemical Co., Ltd.

Product: 3-(4-Chlorophenyl)glutaric acid 35271-74-0
Price: US $20.00/kg
Min. Order: 1kg
Purity: 0.99
Supply Ability: 10 tons
Release date: 2023-09-05

35271-74-0, 3-(4-Chlorophenyl)glutaric acid Related Search:

3-(4-CHLOROPHENYL)GLUTARIC ACID MONOAMIDE,B-(4-CHLOROPHENYL) GLUTARIC ACID MONOAMIDE,beta-(4-Chlorophenyl)glutaric acid monoamide 3-(4-CHLOROPHENYL) GLUTARIMIDE 4-(4-Chlorophenyl)-2-pyrrolidinone Baclofen-d4 Baclofen impurity 6 3-(4-CHLOROPHENYL)GLUTARIC ACID ANHYDRIDE Baclofen Impurity 3 (Mixture of Diastereomers) Baclofen Impurity 2 (beta-(4-Chlorophenyl)-gama-Hydroxybutyric Acid) 3-(4-Chlorophenyl)glutaric acid (2R,3S)-BETA-P-CHLOROPHENYLGLUTAMIC ACID 3-(4-chlorophenyl)glutaric acid (intermediate of baclofen) SS-(4-CHLOROPHENYL)GLUTARIC ACID DIETHYL 2-AMINO-1,4-BIS(4-CHLOROPHENYL)-6-METHYL-1,4-DIHYDRO-3,5-PYRIDINEDICARBOXYLATE AKOS B024755 DIETHYL 4-(4-CHLORO-3-NITROPHENYL)-2,6-DIHYDROXY-2,6-BIS(TRIFLUOROMETHYL)PIPERIDINE-3,5-DICARBOXYLATE 3-BENZYL 5-METHYL 4-(2,4-DICHLOROPHENYL)-2,6-DIMETHYL-1,4-DIHYDRO-3,5-PYRIDINEDICARBOXYLATE 4-(2,4-DICHLOROPHENYL)-5-(METHOXYCARBONYL)-2,6-DIMETHYL-1,4-DIHYDRO-3-PYRIDINECARBOXYLIC ACID BIS(2-METHOXYETHYL) 2-(4-CHLOROPHENYL)-4-HYDROXY-4-METHYL-6-OXO-1,3-CYCLOHEXANEDICARBOXYLATE

3-(4-CHLOROPHENYL)-PENTANEDIOIC ACID

3-(4-CHLOROPHENYL)GLUTARIC ACID

CBI-BB ZERO/006271

BETA-(4-CHLOROPHENYL)GLUTARIC ACID

B-(4-CHLOROPHENYL) GLUTARIC ACID

-(4-Chlorophenyl)glutaricacid

-(p-Chlorophenyl)glutaric Acid

3-(4-chlorophenyl) glutarate

b-(p-Chlorophenyl)glutaric Acid

pentanedioic acid, 3-(4-chlorophenyl)-

Baclofen Impurity (3-(4-Chlorophenyl)-glutaric acid)

3-(4-chlorophenyl)pentane-1,5-dioic acid

Baclofen impurity C

3-(3-chlorophenyl)pentanedioicacid

3-(4 CHLORO PHENYL) GLUTARIC ACID (BACLOFEN INTERMEDIATES) ( 35271-74-0)

Baclofen Impurity 3

Baclofen EP Impurity C

Baclofen Impurity 1

3-(4-chlorophenyl) glutaric AcidQ: What is 3-(4-chlorophenyl) glutaric Acid Q: What is the CAS Number of 3-(4-chlorophenyl) glutaric Acid Q: What is the storage condition of 3-(4-chlorophenyl) glutaric Acid

35271-74-0

C11H11ClO4

Raw material

Miscellaneous Biochemicals

(intermediate of baclofen)

Aromatics