(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE
- Product Name
- (S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE
- CAS No.
- 132873-57-5
- Chemical Name
- (S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE
- Synonyms
- (S)-NITRESOLVE;(S)-(+)-1-(4-NITROPHENYL)-ETHYLAMINE HCL;(S)-alpha-methyl-4-nitrobenzenemethanamine;(S)-(+)-ALPHA-METHYL-4-NITROBENZYLAMINE HCL;(S)-α-Methyl-4-nitrobenzylamineHydrochloride;(S)-4-NITROPHENYL-1-ETHYLAMINE HYDROCHLORIDE;1-(S)-4-Nitrophenyl ethylamine hydrochloride;(S)-4-Nitro-α-methylbenzylamine hydrochloride;(S)-1-(4-Nitrophenyl)ethanaMine hydrochloride;(S)-α-Methyl-4-nitrobenzylamine Hydrochloride
- CBNumber
- CB1467176
- Molecular Formula
- C8H11ClN2O2
- Formula Weight
- 202.64
- MOL File
- 132873-57-5.mol
(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE Property
- Melting point:
- 248-250 °C(lit.)
- refractive index
- -7.2 ° (C=1, 0.05mol/L NaOH)
- storage temp.
- Inert atmosphere,Room Temperature
- form
- powder to crystal
- color
- White to Light yellow
- optical activity
- [α]25/D 6.5°, c = 1 in 0.05 M NaOH
- Water Solubility
- faint turbidity
- CAS DataBase Reference
- 132873-57-5(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- 339822
- Product name
- (S)-α-Methyl-4-nitrobenzylamine hydrochloride
- Purity
- 97%
- Packaging
- 1g
- Price
- $49.6
- Updated
- 2024/03/01
- Product number
- N0543
- Product name
- (S)-alpha-Methyl-4-nitrobenzylamine Hydrochloride
- Purity
- >99.0%(T)
- Packaging
- 1g
- Price
- $57
- Updated
- 2024/03/01
- Product number
- N545280
- Product name
- (S)-1-(4-Nitrophenyl)ethanamineHydrochloride
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 37513
- Product name
- (S)-α-Methyl-4-nitrobenzylaminehydrochloride,99%(T)
- Purity
- 99%(T)
- Packaging
- 1G
- Price
- $60.48
- Updated
- 2021/12/16
- Product number
- CS-M0682
- Product name
- (S)-1-(4-nitrophenyl)ethanamineHydrochloride
- Purity
- >99.0%
- Packaging
- 25g
- Price
- $110
- Updated
- 2021/12/16
(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE Chemical Properties,Usage,Production
Uses
(S)-α-Methyl-4-nitrobenzylamine hydrochloride can be used as:
- A fluorescence-quenching guest in the determination of chiral recognition capabilities of binaphthocrown ether and polythiophene complex.
- A starting material in the synthesis of chiral cyclopalladated complexes with applications in the resolution of racemic compounds.
Purification Methods
To ensure dryness, the hydrochloride (ca 175 g) is extracted with EtOH (3x100mL) and evaporated to dryness (any residual H2O increases the solubility in EtOH and lowers the yield). The hydrochloride residue is triturated with absolute EtOH and dried in vacuo. The product is further purified by refluxing with absolute EtOH (200 mL for 83g) for 1hour, and cool to 10o to give 76.6g of hydrochloride m 243-245o(dec). The free base is prepared by dissolving in N NaOH, extracting with CH2Cl2 (3 x 500mL), drying (Na2CO3), filtering, evaporating and distilling it. It has m 27o, b 119-120o/0.5mm (105-107o/0.5mm, 157-159o/9mm, d 1.1764, n 1.5688, [] ±17.7o (neat) [Perry et al. Synthesis 492 1977,ORD: Nerdel & Liebig Justus Liebigs Ann Chem 621 142 1959]. [Beilstein 12 IV 2451.]
(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE Preparation Products And Raw materials
Raw materials
Preparation Products
(S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE Suppliers
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- him@interchim.com
- Country
- France
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View Lastest Price from (S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE manufacturers
- Product
- (S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE 132873-57-5
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-14
- Product
- (S)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE 132873-57-5
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-14