Pyridinium tribromide

Product Name: Pyridinium tribromide
CAS No.: 39416-48-3
Chemical Name: Pyridinium tribromide
Synonyms: PYRIDINIUM BROMIDE PERBROMIDE;PYRIDINIUM HYDROBROMIDE PERBROMIDE;PHBP;PYRIDINE HYDROBROMIDE PERBROMIDE;Pyridinium perbromide;PVPHP;PYRIDINIUM TRIBROMIDE;Pyridinium tribromider;pyridin-1-iuM tribroMide;Pyridinium Tribromide (>
CBNumber: CB1478015
Molecular Formula: C5H6Br3N-2
Formula Weight: 319.82
MOL File: 39416-48-3.mol

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Pyridinium tribromide Property

Melting point:: 127-133 °C
Density: 2.9569 (rough estimate)
refractive index: 1.6800 (estimate)
storage temp.: Store at <= 20°C.
solubility: soluble in Methanol
form: Powder, Crystals and/or Chunks
color: Red-orange to red to brown
Water Solubility: decomposes
Sensitive: Lachrymatory
Merck: 14,7973
BRN: 3690144
Stability:: Stable. Incompatible with strong oxidizing agents, strong bases.
InChIKey: YPCPFIMBGJOEKU-UHFFFAOYSA-O
CAS DataBase Reference: 39416-48-3(CAS DataBase Reference)
EPA Substance Registry System: Pyridinium hydrogen tribromide (39416-48-3)

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Safety

Hazard Codes: C,Xi
Risk Statements: 37/38-34-36
Safety Statements: 26-36/37/39-45-24/25-27
RIDADR: UN 3261 8/PG 2
WGK Germany: 3
F: 3
Hazard Note: Lachrymatory
TSCA: Yes
HazardClass: 8
PackingGroup: III
HS Code: 29333100

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 133248
Product name: Pyridinium tribromide
Purity: technical grade, 90%
Packaging: 25g
Price: $57.3
Updated: 2024/03/01

Sigma-Aldrich

Product number: 8.14345
Product name: Pyridinium bromide-perbromide
Purity: for synthesis
Packaging: 50g
Price: $107
Updated: 2024/03/01

Sigma-Aldrich

Product number: 133248
Product name: Pyridinium tribromide
Purity: technical grade, 90%
Packaging: 100g
Price: $114
Updated: 2024/03/01

TCI Chemical

Product number: P0825
Product name: Pyridinium Bromide Perbromide
Purity: >85.0%(T)
Packaging: 25g
Price: $36
Updated: 2024/03/01

TCI Chemical

Product number: P0825
Product name: Pyridinium Bromide Perbromide
Purity: >85.0%(T)
Packaging: 100g
Price: $95
Updated: 2024/03/01

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Pyridinium tribromide Chemical Properties,Usage,Production

Chemical Properties

red crystals

Uses

Pyridine hydrobromide perbromide is used as a brominating reagent in alfa-bromination and alfa-thiocyanation of ketones, phenols, unsaturated and aromatic ethers. It is used as a raw material in the preparation of beta-adrenergic blocking agents. Furthermore, it is used as an analytical reagent.

Uses

Pyridinium Tribromide is a reagent used in the α-thiocyanation of ketones and has also been applied to the synthesis of β-adrenergic blocking agents (also known as β-blockers) for patients with heart failure.

Uses

In small-scale brominations, where it is much more convenient and agreeable to measure and use than elemental bromine.

Purification Methods

It is a very good brominating agent-liberating one mol of Br2. Purify it by recrystallisation from glacial acetic acid (33g from 100mL of AcOH) to give orange-red crystals. [Fieser & Fieser Reagents for Organic Chemistry 1 967 1967, Englert & McElvain J Am Chem Soc 51 865 1929, Beilstein 20 II 103, 20/5 V 181.]

Pyridinium tribromide Preparation Products And Raw materials

Raw materials

Government regulation

Preparation Products

2,3,4-Trimethoxyphenylboronic acid 4-Bromo-1-chloroisoquinoline

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Pyridinium tribromide Suppliers

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View Lastest Price from Pyridinium tribromide manufacturers

HebeiShuoshengImportandExportco.,Ltd

Product: Pyridinium tribromide 39416-48-3
Price: US $6.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 2000KG/Month
Release date: 2024-08-08

Hebei Longbang Technology Co., Ltd

Product: Pyridinium tribromide 39416-48-3
Price: US $6.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20TONS
Release date: 2024-04-29

Hebei Jingbo New Material Technology Co., Ltd

Product: Pyridinium tribromide 39416-48-3
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 1000000
Release date: 2023-12-21

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39416-48-3

394116-48-3

39416-48-6

C5H6B3N

C5H5NHBrBr2

C5H5NHBr3

C5H5NxHBr3

C5H6NBrBr2

C5H6N3Br

C5H6Br3N

C5H6Br3N2