ChemicalBook > CAS DataBase List > 2-METHOXY-5-NITROBENZALDEHYDE

2-METHOXY-5-NITROBENZALDEHYDE

Product Name: 2-METHOXY-5-NITROBENZALDEHYDE
CAS No.: 25016-02-8
Chemical Name: 2-METHOXY-5-NITROBENZALDEHYDE
Synonyms: AKOS B028867;5-Nitro-o-anisaldehyde;5-Nitro-o-anisaldehyde;2-METHOXY-5-NITROBENZALDEHYDE;2-methoxy-5-nitro-benzaldehyd;Benzaldehyde, 2-methoxy-5-nitro-;4-(4-morpholinyl)-6-[[4-(phenylmethyl)-1-piperazinyl]methyl]-1,3,5-triazin-2-amine
CBNumber: CB1676781
Molecular Formula: C8H7NO4
Formula Weight: 181.15
MOL File: 25016-02-8.mol

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2-METHOXY-5-NITROBENZALDEHYDE Property

Melting point:: 89-92 °C (lit.)
Boiling point:: 336.7±27.0 °C(Predicted)
Density: 1.322±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
solubility: very soluble in Dimethylformamide
form: powder to crystal
color: White to Light yellow to Light orange
CAS DataBase Reference: 25016-02-8
EPA Substance Registry System: Benzaldehyde, 2-methoxy-5-nitro- (25016-02-8)

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Safety

WGK Germany: 3
HS Code: 2913000090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 515760
Product name: 2-Methoxy-5-nitrobenzaldehyde
Purity: 97%
Packaging: 5g
Price: $296
Updated: 2022/05/15

TCI Chemical

Product number: N1034
Product name: 5-Nitro-o-anisaldehyde
Purity: min. 98.0 %
Packaging: 5G
Price: $36
Updated: 2025/07/31

TCI Chemical

Product number: N1034
Product name: 5-Nitro-o-anisaldehyde
Purity: min. 98.0 %
Packaging: 25G
Price: $108
Updated: 2025/07/31

AK Scientific

Product number: J94624
Product name: 2-Methoxy-5-nitrobenzaldehyde
Packaging: 5g
Price: $119
Updated: 2021/12/16

AK Scientific

Product number: 1946AB
Product name: 2-Methoxy-5-nitrobenzaldehyde
Packaging: 5g
Price: $149
Updated: 2021/12/16

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2-METHOXY-5-NITROBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

97-51-8

74-88-4

25016-02-8

General procedure for the synthesis of 2-methoxy-5-nitrobenzaldehyde from 5-nitrosalicylaldehyde and iodomethane: Sodium hydride (NaH, 246 mg) and iodomethane (2.56 g) were added to a solution of 5-nitrosalicylaldehyde (1.00 g, 6.0 mmol) in N,N-dimethylformamide (DMF, 20 ml). The reaction mixture was stirred at 0°C for 8.5 hours. After completion of the reaction, the reaction mixture was extracted with ether and the organic phase was washed sequentially with aqueous sodium bicarbonate, saturated brine and 5% hydrochloric acid/saturated brine. The organic phase was dried with anhydrous magnesium sulfate and concentrated under reduced pressure to give 2-methoxy-5-nitrobenzaldehyde (0.95 g, 87.8% yield) as yellow needle-like crystals. The product was characterized by 1H NMR (CDCl3): δ 10.45 (s, 1H), 8.70 (d, J = 2.9Hz, 1H), 8.45 (dd, J = 8.8, 2.9Hz, 1H), 7.14 (d, J = 8.8Hz, 1H), 4.08 (s, 3H).

References

[1] Angewandte Chemie - International Edition, 2011, vol. 50, # 15, p. 3435 - 3438
[2] Patent: US2013/261295, 2013, A1. Location in patent: Paragraph 0166; 0167
[3] Journal of the American Chemical Society, 2017, vol. 139, # 19, p. 6654 - 6662
[4] Patent: US5837711, 1998, A
[5] Journal of the Chemical Society, 1951, p. 2462,2466

2-METHOXY-5-NITROBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Silver oxide Diethyl ether 5-Nitrosalicylaldehyde Methanol Iodomethane

Preparation Products

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2-METHOXY-5-NITROBENZALDEHYDE Suppliers

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View Lastest Price from 2-METHOXY-5-NITROBENZALDEHYDE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 2-Methoxy-5-nitrobenzaldehyde 25016-02-8
Price: US $0.00-0.00/KG
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-15

25016-02-8, 2-METHOXY-5-NITROBENZALDEHYDERelated Search:

2,6-DIMETHOXY-3-NITROBENZOIC ACID 3-CHLORO-2,6-DIMETHOXY-5-NITROBENZOIC ACID 3-METHOXY-5-NITROBENZALDEHYDE 2-METHOXY-4-NITROBENZALDEHYDE 4-HYDROXY-3-METHOXY-5-NITROBENZALDEHYDE 5-METHOXY-2-NITROBENZALDEHYDE 4-METHOXY-3-NITROBENZALDEHYDE 3-METHOXY-2-NITROBENZALDEHYDE,3-METHOXY-2-NITROBENZALDEHYDE, 97+% 2-HYDROXY-3-METHOXY-5-NITROBENZALDEHYDE 98%,2-HYDROXY-3-METHOXY-5-NITROBENZALDEHYDE 2-(4-METHOXYPHENOXY)-5-NITROBENZOIC ACID 2,6-DIMETHOXY-3-NITROBENZAMIDE 2-[4-(TERT-BUTYL)PHENOXY]-5-NITROBENZALDEHYDE 2-[(6-CHLORO-4H-1,3-BENZODIOXIN-8-YL)METHOXY]-5-NITROBENZALDEHYDE,2-[(6-Chloro-4H-1,3-benzodiox-8-yl)methoxy]-5-nitrobenzaldehyde 2-[(3-FLUOROBENZYL)OXY]-5-NITROBENZALDEHYDE 2-(4-METHOXYPHENOXY)-5-NITROBENZENE-1-CARBONYL CHLORIDE 2-FORMYL-4-NITROPHENOXYACETIC ACID 3-FORMYL-6-NITROCHROMONE METHYL 2,6-DIMETHOXY-3-NITROBENZOATE

2-methoxy-5-nitro-benzaldehyd

AKOS B028867

2-METHOXY-5-NITROBENZALDEHYDE

Benzaldehyde, 2-methoxy-5-nitro-

5-Nitro-o-anisaldehyde

5-Nitro-<i>o</i>-anisaldehyde

4-(4-morpholinyl)-6-[[4-(phenylmethyl)-1-piperazinyl]methyl]-1,3,5-triazin-2-amine

25016-02-8

Carbonyl Compounds

Building Blocks

Aldehydes

Organic Building Blocks

Aldehydes

Carbonyl Compounds