4-(2-PYRIDYL)ANILINE

Product Name: 4-(2-PYRIDYL)ANILINE
CAS No.: 18471-73-3
Chemical Name: 4-(2-PYRIDYL)ANILINE
Synonyms: 4-(pyridin-2-yl)aniline;4-(2-Pyridinyl)aniline;2-(4-AMINOPHENYL)PYRIDINE;4-(2-Pyridyl);2-Pyridyl-3-aniline;4-(2-PYRIDYL)ANILINE;4-(2-Pyridyl)aminobenzene;4-Pyridin-2-yl-phenylaMine;4-(2-Pyridinyl)benzenamine;Benzenamine, 4-(2-pyridinyl)-
CBNumber: CB1745067
Molecular Formula: C11H10N2
Formula Weight: 170.21
MOL File: 18471-73-3.mol

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4-(2-PYRIDYL)ANILINE Property

Melting point:: 95 °C
Boiling point:: 322.8±17.0 °C(Predicted)
Density: 1.133±0.06 g/cm3(Predicted)
storage temp.: 2-8°C, protect from light
form: solid
pka: 5.72±0.25(Predicted)
color: Brown

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: P991913
Product name: 4-(2-Pyridyl)aniline
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 074092
Product name: 4-(2-Pyridyl)aniline
Purity: 95+%
Packaging: 5g
Price: $75
Updated: 2021/12/16

Rieke Metals

Product number: 11500
Product name: 4-(2-Pyridyl)aniline
Purity: 97%
Packaging: 2g
Price: $490
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0024408
Product name: 4-(2-PYRIDYL)ANILINE
Purity: 95.00%
Packaging: 1G
Price: $653.73
Updated: 2021/12/16

AK Scientific

Product number: W3992
Product name: 4-(2-Pyridyl)aniline
Packaging: 10g
Price: $133
Updated: 2021/12/16

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4-(2-PYRIDYL)ANILINE Chemical Properties,Usage,Production

Synthesis

4282-47-7

18471-73-3

General procedure for the synthesis of 4-(2-pyridyl)aniline from 2-(4-nitrophenyl)pyridine: the compound 2-(4-nitrophenyl)pyridine (0.2 g, 1.03 mmol) was dissolved in methanol (10 mL), 10% palladium-carbon (20 mg) was added as a catalyst, and the reduction reaction was carried out under hydrogen atmosphere. The reaction mixture was stirred at room temperature for 18 hours. Upon completion of the reaction, the catalyst was removed by filtration through a Celite pad, which was washed with methanol (50 mL). After combining the filtrates, the solvent was removed by evaporation under reduced pressure to give the crude product. The crude product was purified by rapid chromatography on silica gel with the eluent dichloromethane-methanol-ammonia (95:4.5:0.5, v/v/v) to afford the target compound 4-(2-pyridyl)aniline (0.15 g, 87% yield) as a brown solid. The physical and spectroscopic data of the product were as follows: melting point 89-92 °C (literature value 94-95 °C); IR spectra (νmax/cm?1) 3333, 3210, 1606, 1586, 1519, 1294, 1181; 1H NMR (500 MHz, CDCl?) δ 8.62 (1H, dt, J=1.0, 5.0 Hz), 7.83 (2H, d, J=8.5 Hz), 7.68-7.61 (2H, m), 7.11 (1H, m), 6.75 (2H, d, J=8.5 Hz), 3.83 (2H, br s); 13C NMR (125 MHz, CDCl?) δ 157.6, 149.5, 147.5, 136.6, 129.8, 128.1, 121.0, 119.4, 115.2; mass spectrometry (ESI) m/z 171 ([M + H]? , 100).

References

[1] European Journal of Medicinal Chemistry, 2015, vol. 95, p. 277 - 301
[2] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1988, vol. 24, # 11, p. 1221 - 1225
[3] Khimiya Geterotsiklicheskikh Soedinenii, 1988, vol. 24, # 11, p. 1476 - 1480
[4] Molecular crystals and liquid crystals, 1980, vol. 62, # 1-2, p. 103 - 114
[5] Chemische Berichte, 1896, vol. 29, p. 168

4-(2-PYRIDYL)ANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(2-PYRIDYL)ANILINE Suppliers

China 73 India 1 Poland 1 United Kingdom 1 United States 9 Global 85

J & K SCIENTIFIC LTD.

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Shanghai Topbiochem Technology Co., Ltd

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View Lastest Price from 4-(2-PYRIDYL)ANILINE manufacturers

Career Henan Chemical Co

Product: 4-(2-PYRIDYL)ANILINE 18471-73-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2018-08-08

18471-73-3, 4-(2-PYRIDYL)ANILINERelated Search:

pyritidium bromide 2-(4-Nitrophenyl)pyridine 3-(2-Pyridyl)aniline Dihydrochloride 4-(3-PYRIDYL)ANILINE 3-(4-PYRIDYL)ANILINE 3-Pyridin-3-ylaniline 3-(3-Pyridyl)aniline Dihydrochloride 2-(3-AMINOPHENYL)PYRIDINE AKOS AUF2113 2-(4-NITRO-PHENYL)-QUINOLINE-4-CARBOXYLIC ACID AKOS BC-0609 2-(5-METHYL-FURAN-2-YL)-6-(4-NITRO-PHENYL)-4-PHENYL-PYRIDINE 3-METHYL-2-(4-NITROPHENYL)PYRIDINE 2-(4-AMINO-PHENYL)-QUINOLINE-4-CARBOXYLIC ACID 2-[4-(ACETYLAMINO)PHENYL]QUINOLINE-4-CARBOXYLIC ACID N-(3-Pyridyl)aniline 2-(2-PYRIDYL)ANILINE N-(4-Pyridyl)aniline

4-(2-PYRIDYL)ANILINE

2-(4-AMINOPHENYL)PYRIDINE

2-Pyridyl-3-aniline

4-(2-Pyridinyl)aniline

4-(pyridin-2-yl)aniline

4-Pyridin-2-yl-phenylaMine

4-(2-Pyridyl)

4-(2-Pyridyl)aminobenzene

Benzenamine, 4-(2-pyridinyl)-

4-(2-Pyridinyl)benzenamine

4-(2-Pyridyl)aniline - [P54256]

18471-73-3

1847-73-3

pharmacetical