3-Pyridin-3-ylaniline
- Product Name
- 3-Pyridin-3-ylaniline
- CAS No.
- 57976-57-5
- Chemical Name
- 3-Pyridin-3-ylaniline
- Synonyms
- AKOS BAR-2462;3-(3-Pyridyl)aniline;3-PYRIDIN-3-YLANILINE;3-PYRIDINE-3-YLANILINE;3-(3-Aminophenyl)pyridine;3-(Pyridin-3-yl)aniline97%;3-PYRIDIN-3-YL-PHENYLAMINE;3-(Pyridin-3-yl)benzenamine;3-(Pyridin-3-yl)aniline 97%;Benzenamine, 3-(3-pyridinyl)-
- CBNumber
- CB3692248
- Molecular Formula
- C11H10N2
- Formula Weight
- 170.21
- MOL File
- 57976-57-5.mol
3-Pyridin-3-ylaniline Property
- Melting point:
- 72-74
- Boiling point:
- 0
- Density
- 1.133±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 4.85±0.11(Predicted)
- form
- solid
- color
- Off-white
Safety
- Hazard Codes
- Xn
- Risk Statements
- 20/21/22-36/37/38
- Safety Statements
- 22-26-36/37/39
- Hazard Note
- Harmful
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- P993760
- Product name
- 3-(pyridin-3-yl)aniline
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- BP-21489
- Product name
- 3-(Pyridine-3-yl)aniline
- Purity
- 95%
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- 130614
- Product name
- 3-(Pyridin-3-yl)aniline
- Packaging
- 1g
- Price
- $429
- Updated
- 2021/12/16
- Product number
- CHM0024119
- Product name
- 3-PYRIDIN-3-YLANILINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $632.1
- Updated
- 2021/12/16
- Product number
- W7125
- Product name
- 3-(Pyridin-3-yl)benzenamine
- Packaging
- 5g
- Price
- $651
- Updated
- 2021/12/16
3-Pyridin-3-ylaniline Chemical Properties,Usage,Production
Synthesis
59020-10-9
591-19-5
57976-57-5
4.3.8 Synthesis of 3-(3-aminophenyl)pyridine (3ha): m-Bromoaniline (0.5 mmol), base (1 mmol), cuprous iodide (20 mol%), 3-(1,1,1-tributylmethylstannyl)pyridine (0.75 mmol), and catalyst (1 mol%) were placed in a 10 mL vial protected by nitrogen and DMF (2 mL) was added to dissolve. ) was added to dissolve. The reaction mixture was heated to a specific temperature and reacted for 12 hours. Upon completion of the reaction, the reaction was quenched with water. The mixture was diluted with ethyl acetate (10 mL), filtered through a pad of diatomaceous earth and subsequently extracted three times with ethyl acetate. The organic layers were combined, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The residue was purified by rapid column chromatography on silica gel (eluent: ethyl acetate/hexane) to afford the target product 3-(3-aminophenyl)pyridine (3ha) as a yellow solid with a melting point of 69-70 °C. The residue was purified by fast column chromatography on silica gel (eluent: ethyl acetate/hexane). Product characterization data: 1H NMR (400 MHz, CDCl3): δ = 8.80 (d, J = 1.44 Hz, 1H), 8.55 (d, J = 4.20 Hz, 1H), 7.81 (dt, J = 7.92, 1.68 Hz, 1H), 7.29-7.32 (m, 1H), 7.23 (t, J = 7.80 Hz, 1H), 6.93 (d , J = 7.64 Hz, 1H), 6.85-6.86 (m, 1H), 3.91 (s, 2H). 13C NMR (100 MHz, CDCl3): δ = 113.5, 114.7, 117.2, 123.5, 130.0, 134.3, 136.9, 138.8, 147.3, 148.1, 148.2.
References
[1] Tetrahedron, 2013, vol. 69, # 2, p. 902 - 909
3-Pyridin-3-ylaniline Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-Pyridin-3-ylaniline manufacturers
- Product
- 3-Pyridin-3-ylaniline 57976-57-5
- Price
- US $8.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10tons
- Release date
- 2018-12-24