ChemicalBook > CAS DataBase List > 3-Pyridin-3-ylaniline

3-Pyridin-3-ylaniline

Product Name
3-Pyridin-3-ylaniline
CAS No.
57976-57-5
Chemical Name
3-Pyridin-3-ylaniline
Synonyms
AKOS BAR-2462;3-(3-Pyridyl)aniline;3-PYRIDIN-3-YLANILINE;3-PYRIDINE-3-YLANILINE;3-(3-Aminophenyl)pyridine;3-(Pyridin-3-yl)aniline97%;3-PYRIDIN-3-YL-PHENYLAMINE;3-(Pyridin-3-yl)benzenamine;3-(Pyridin-3-yl)aniline 97%;Benzenamine, 3-(3-pyridinyl)-
CBNumber
CB3692248
Molecular Formula
C11H10N2
Formula Weight
170.21
MOL File
57976-57-5.mol
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3-Pyridin-3-ylaniline Property

Melting point:
72-74
Boiling point:
0
Density 
1.133±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
pka
4.85±0.11(Predicted)
form 
solid
color 
Off-white
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Safety

Hazard Codes 
Xn
Risk Statements 
20/21/22-36/37/38
Safety Statements 
22-26-36/37/39
Hazard Note 
Harmful
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
P993760
Product name
3-(pyridin-3-yl)aniline
Packaging
50mg
Price
$45
Updated
2021/12/16
BroadPharm
Product number
BP-21489
Product name
3-(Pyridine-3-yl)aniline
Purity
95%
Packaging
250mg
Price
$55
Updated
2021/12/16
Matrix Scientific
Product number
130614
Product name
3-(Pyridin-3-yl)aniline
Packaging
1g
Price
$429
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0024119
Product name
3-PYRIDIN-3-YLANILINE
Purity
95.00%
Packaging
1G
Price
$632.1
Updated
2021/12/16
AK Scientific
Product number
W7125
Product name
3-(Pyridin-3-yl)benzenamine
Packaging
5g
Price
$651
Updated
2021/12/16
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3-Pyridin-3-ylaniline Chemical Properties,Usage,Production

Synthesis

59020-10-9

591-19-5

57976-57-5

4.3.8 Synthesis of 3-(3-aminophenyl)pyridine (3ha): m-Bromoaniline (0.5 mmol), base (1 mmol), cuprous iodide (20 mol%), 3-(1,1,1-tributylmethylstannyl)pyridine (0.75 mmol), and catalyst (1 mol%) were placed in a 10 mL vial protected by nitrogen and DMF (2 mL) was added to dissolve. ) was added to dissolve. The reaction mixture was heated to a specific temperature and reacted for 12 hours. Upon completion of the reaction, the reaction was quenched with water. The mixture was diluted with ethyl acetate (10 mL), filtered through a pad of diatomaceous earth and subsequently extracted three times with ethyl acetate. The organic layers were combined, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The residue was purified by rapid column chromatography on silica gel (eluent: ethyl acetate/hexane) to afford the target product 3-(3-aminophenyl)pyridine (3ha) as a yellow solid with a melting point of 69-70 °C. The residue was purified by fast column chromatography on silica gel (eluent: ethyl acetate/hexane). Product characterization data: 1H NMR (400 MHz, CDCl3): δ = 8.80 (d, J = 1.44 Hz, 1H), 8.55 (d, J = 4.20 Hz, 1H), 7.81 (dt, J = 7.92, 1.68 Hz, 1H), 7.29-7.32 (m, 1H), 7.23 (t, J = 7.80 Hz, 1H), 6.93 (d , J = 7.64 Hz, 1H), 6.85-6.86 (m, 1H), 3.91 (s, 2H). 13C NMR (100 MHz, CDCl3): δ = 113.5, 114.7, 117.2, 123.5, 130.0, 134.3, 136.9, 138.8, 147.3, 148.1, 148.2.

References

[1] Tetrahedron, 2013, vol. 69, # 2, p. 902 - 909

3-Pyridin-3-ylaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Pyridin-3-ylaniline manufacturers

Career Henan Chemical Co
Product
3-Pyridin-3-ylaniline 57976-57-5
Price
US $8.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
10tons
Release date
2018-12-24

57976-57-5, 3-Pyridin-3-ylanilineRelated Search:

3-Aminopyridine 2-Aminopyridine 2-Chloro-3-cyanopyridine 4-Dimethylaminopyridine 3-(3-Pyridyl)aniline Dihydrochloride 3-(3-Aminophenyl)-4-pyridinecarboxylicacidethylester 4-(2-aminophenethyl)pyridine 3-PYRIDIN-4-YLANILINE 4-PYRIDIN-3-YLANILINE 3-(3-QUINOLINYL)ANILINE 3-(3-NITROPHENYL)PYRIDINE 5-(3-NITROPHENYL)NICOTINIC ACID 3-CHLORO-4-[1,3]OXAZOLO[4,5-B]PYRIDIN-2-YLANILINE N-[3-FLUORO-5-(3-PYRINDYL)PHENYL]-2,3-DIHYDRO-5-METHOXY-6-(TRIFLUOROMETHYL)-1H-INDOLE-1-CARBOXAMIDE 4-CHLORO-3-[1,3]OXAZOLO[4,5-B]PYRIDIN-2-YLANILINE 3-IMIDAZO[1,2-A]PYRIDIN-2-YLANILINE 2-PYRIDIN-3-YLANILINE 4-IMIDAZO[1,2-A]PYRIDIN-2-YLANILINE

  • 3-PYRIDIN-3-YLANILINE
  • 3-PYRIDIN-3-YL-PHENYLAMINE
  • AKOS BAR-2462
  • 3-(3-Aminophenyl)pyridine
  • 3-(Pyridin-3-yl)aniline 97%
  • 3-(Pyridin-3-yl)benzenamine
  • 3-PYRIDINE-3-YLANILINE
  • 3-(3-Pyridyl)aniline
  • 3-(Pyridin-3-yl)aniline97%
  • Benzenamine, 3-(3-pyridinyl)-
  • 57976-57-5
  • Amines and Anilines
  • Heterocycles