2-(3-AMINOPHENYL)PYRIDINE
- Product Name
- 2-(3-AMINOPHENYL)PYRIDINE
- CAS No.
- 15889-32-4
- Chemical Name
- 2-(3-AMINOPHENYL)PYRIDINE
- Synonyms
- p60068;3-(2-Pyridinyl)aniline;3-(Pyridin-2-yl)aniline;2-(m-Aminophenyl)pyridine;2-(3-AMINOPHENYL)PYRIDINE;3-Pyridin-2-yl-phenylaMine;3-(2-Pyridinyl)benzenamine;Benzenamine, 3-(2-pyridinyl)-
- CBNumber
- CB3730351
- Molecular Formula
- C11H10N2
- Formula Weight
- 170.21
- MOL File
- 15889-32-4.mol
2-(3-AMINOPHENYL)PYRIDINE Property
- Melting point:
- 72-73℃
- Boiling point:
- 145-147 °C(Press: 0.1 Torr)
- Density
- 1.133±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- pka
- 4.81±0.12(Predicted)
- Appearance
- Off-white to light brown Solid
Safety
- Hazard Codes
- T
- Risk Statements
- 25-36/37/38
- Safety Statements
- 26-45
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- P841118
- Product name
- 3-(2-Pyridyl)aniline
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- W3447
- Product name
- 2-(3-Aminophenyl)pyridinedihydrochloride
- Packaging
- 250mg
- Price
- $122
- Updated
- 2021/12/16
- Product number
- 081174
- Product name
- 2-(3-Aminophenyl)pyridine
- Purity
- 95%
- Packaging
- 1g
- Price
- $237
- Updated
- 2021/12/16
- Product number
- CHM0093741
- Product name
- 3-(2-PYRIDYL)ANILINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $504.21
- Updated
- 2021/12/16
- Product number
- 69R1005
- Product name
- 3-Pyridin-2-yl-phenylamine
- Purity
- 96%
- Packaging
- 100mg
- Price
- $78
- Updated
- 2021/12/16
2-(3-AMINOPHENYL)PYRIDINE Chemical Properties,Usage,Production
Synthesis
109-04-6
30418-59-8
15889-32-4
General procedure for the synthesis of 3-(2-pyridyl)aniline from 2-bromopyridine and 3-aminophenylboronic acid: cf. Example 31; to a suspension of 2-bromopyridine (0.5 g, 3.2 mmol), 3-aminophenylboronic acid (0.49 g, 3.2 mmol), anhydrous K2CO3 (0.87 g, 6.3 mmol) and Pd(PPh3)4 (0.36 g, 0.32 mmol) in a suspension of 1,2-dimethoxyethane (50 mL) and water (0.66 mL) under argon protection. The reaction mixture was heated at 80 °C under argon atmosphere overnight. After completion of the reaction, it was cooled to room temperature and extracted by adding water and EtOAc. The organic and aqueous phases were separated, and the combined organic phase was dried with Na2SO4 and concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography using a mixed solvent of gradient polarity hexane-EtOAc as eluent to give 0.22 g of 3-(2-pyridinyl)aniline (Yield: 42%). LC-MS (Method 1): tR = 1.46 min; m/z = 171.2 [M + H]+.
References
[1] Molecular Crystals and Liquid Crystals, 2006, vol. 458, # 1, p. 227 - 235
[2] Journal of Medicinal Chemistry, 2000, vol. 43, # 6, p. 1123 - 1134
[3] Patent: WO2007/339, 2007, A1. Location in patent: Page/Page column 52
[4] Tetrahedron, 2006, vol. 62, # 49, p. 11483 - 11498
[5] Patent: US2006/94644, 2006, A1. Location in patent: Page/Page column 23
2-(3-AMINOPHENYL)PYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-(3-AMINOPHENYL)PYRIDINE manufacturers
- Product
- 2-(3-AMINOPHENYL)PYRIDINE 15889-32-4
- Price
- US $2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- Customise
- Release date
- 2018-08-09