methyl pyridine-3-acetate

Product Name: methyl pyridine-3-acetate
CAS No.: 39998-25-9
Chemical Name: methyl pyridine-3-acetate
Synonyms: Methyl 2-(pyridin-3-yl)acetate;EOS-62049;Einecs 254-739-0;METHYL 3-PYRIDYLACETATE;methyl pyridine-3-acetate;Methyl pyridin-3-ylacetate;Methyl 2-(3-Pyridyl)acetate;3-Pyridineacetic acid methyl ester;3-Pyridinylacetic acid methyl ester;Pyridin-3-yl-acetic acid methyl ester
CBNumber: CB1894918
Molecular Formula: C8H9NO2
Formula Weight: 151.16
MOL File: 39998-25-9.mol

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methyl pyridine-3-acetate Property

Boiling point:: 112 °C(Press: 10 Torr)
Density: 1.115±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 4.40±0.11(Predicted)
Appearance: Light yellow to yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S363855
Product name: METHYL 3-PYRIDYLACETATE
Purity: Aldrich<sup>CPR</sup>
Packaging: 1 unit
Price: $113
Updated: 2025/07/31

Sigma-Aldrich

Product number: S363855
Product name: METHYL 3-PYRIDYLACETATE
Purity: Aldrich
Packaging: 250mg
Price: $110
Updated: 2024/03/01

TRC

Product number: M219543
Product name: Methyl2-(Pyridin-3-yl)acetate
Packaging: 500mg
Price: $130
Updated: 2021/12/16

AK Scientific

Product number: X5277
Product name: Methylpyridine-3-acetate
Packaging: 250mg
Price: $82
Updated: 2021/12/16

Matrix Scientific

Product number: 113966
Product name: Methyl pyridin-3-ylacetate
Purity: 97%
Packaging: 1g
Price: $371
Updated: 2021/12/16

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methyl pyridine-3-acetate Chemical Properties,Usage,Production

Synthesis

67-56-1

6419-36-9

39998-25-9

To synthesize methyl (pyridin-3-yl)acetate, the following procedure was used: in a 1L four-necked flask equipped with a nitrogen introduction tube, thermometer, Dimroth condenser, and a dropping funnel, 25.12 g (0.145 mol) of pyridine-3-acetic acid hydrochloride was added. Subsequently 500mL of anhydrous methanol was added. Stir at room temperature under nitrogen protection until the hydrochloride is completely dissolved. 31.12 g (0.248 mol) of thionyl chloride was slowly added dropwise. After the dropwise addition was completed, the reaction mixture was heated to reflux and the reaction was continued for 2.5 hours. After completion of the reaction, the mixture was cooled to room temperature and methanol was removed by distillation under reduced pressure by rotary evaporator. The residue was neutralized to pH neutral with saturated aqueous sodium bicarbonate. The aqueous phase was extracted with 100 mL of ethyl acetate in three fractions, the organic phases were combined and dried over anhydrous sodium sulfate. After filtration to remove the desiccant, the solvent was removed by distillation under reduced pressure to give 21.29 g (0.141 mol) of methyl (pyridin-3-yl)acetate in 97% yield.

References

[1] Patent: EP2390243, 2011, A1. Location in patent: Page/Page column 26
[2] Tetrahedron Letters, 1993, vol. 34, # 2, p. 331 - 334

methyl pyridine-3-acetate Preparation Products And Raw materials

Raw materials

Preparation Products

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methyl pyridine-3-acetate Suppliers

China 78 India 5 United States 7 Global 90

Accela ChemBio Inc.

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Matrix Scientific

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Alfa Chemistry

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View Lastest Price from methyl pyridine-3-acetate manufacturers

Career Henan Chemical Co

Product: methyl pyridine-3-acetate 39998-25-9
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1000KG
Release date: 2020-01-02

39998-25-9, methyl pyridine-3-acetateRelated Search:

methyl 2-amino-2-(5-bromopyridin-3-yl)hexanoate ETHYL 3-PYRIDYLACETATE methyl pyridine-3-acetate (6-CHLORO-PYRIDIN-3-YL)-OXO-ACETIC ACID ETHYL ESTER (2-CHLORO-PYRIDIN-3-YL)-OXO-ACETIC ACID ETHYL ESTER 3-PYRIDINEACETIC ACID, A-OXO, ETHYL ESTER 3-PYRIDINEACETIC ACID, 6-METHYL-,ETHYL ESTER RARECHEM AK ML 0009 ETHYL 2-CYANO-2-PYRIDIN-3-YL-ACETATE 2-CHLOROPYRIDINE-5-ACETIC ACID ETHYL ESTER 2,3,5,6-1H,4H-Tetrahydro-9-(3-pyridyl)quinolizino[9,9a,1-gh]coumarin 3-PYRIDINEACETIC ACID, 4-[[(1,1-DIMETHYLETHOXY)CARBONYL]AMINO]-A-OXO-, ETHYL ESTER RARECHEM AK ML 0008 RARECHEM AK HZ 0055 RARECHEM AM LA 0060 3-Pyridineacetic acid, (5-chloro-3-pyridinyl)methyl ester, monohydroch loride methyl 2-(5-bromopyridin-3-yl)acetate 3-AMINO-2-PYRIDIN-3-YL-PROPIONIC ACID ETHYL ESTER

methyl pyridine-3-acetate

Pyridin-3-yl-acetic acid methyl ester

3-Pyridineacetic acid methyl ester

3-Pyridinylacetic acid methyl ester

Einecs 254-739-0

Methyl 2-(pyridin-3-yl)acetate

METHYL 3-PYRIDYLACETATE

Methyl 2-(3-Pyridyl)acetate

Methyl pyridin-3-ylacetate

EOS-62049

39998-25-9