Methyl tetrahydro-3-furoate
- Product Name
- Methyl tetrahydro-3-furoate
- CAS No.
- 53662-85-4
- Chemical Name
- Methyl tetrahydro-3-furoate
- Synonyms
- Methyl tetrahydro-3-furoate;Methyl tetrahydrofuran-3-...;methyl oxolane-3-carboxylate;Methyl tetrahydrofuran-3-carboxylate;Tetrahydro-3-furancarboxylic acid methyl ester;3-Furancarboxylic acid, tetrahydro-, methyl ester
- CBNumber
- CB1971657
- Molecular Formula
- C6H10O3
- Formula Weight
- 130.14
- MOL File
- 53662-85-4.mol
Methyl tetrahydro-3-furoate Property
- Boiling point:
- 61-65 °C(Press: 12 Torr)
- Density
- 1.108±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2932190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H226Flammable liquid and vapour
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- P000356377
- Product name
- Methyl tetrahydrofuran-3-carboxylate
- Purity
- 95%
- Packaging
- 100mg
- Price
- $14
- Updated
- 2021/12/16
- Product number
- P000356377
- Product name
- Methyl tetrahydrofuran-3-carboxylate
- Purity
- 95%
- Packaging
- 250mg
- Price
- $23
- Updated
- 2021/12/16
- Product number
- P000356377
- Product name
- Methyl tetrahydrofuran-3-carboxylate
- Purity
- 95%
- Packaging
- 1g
- Price
- $47
- Updated
- 2021/12/16
- Product number
- OR938707
- Product name
- Methyltetrahydrofuran-3-carboxylate
- Purity
- 95%
- Packaging
- 1g
- Price
- $135
- Updated
- 2021/12/16
- Product number
- P000356377
- Product name
- Methyl tetrahydrofuran-3-carboxylate
- Purity
- 95%
- Packaging
- 5g
- Price
- $142
- Updated
- 2021/12/16
Methyl tetrahydro-3-furoate Chemical Properties,Usage,Production
Synthesis
67-56-1
89364-31-8
53662-85-4
Concentrated sulfuric acid (27.54 mL, 517 mmol) was slowly added to a solution of tetrahydro-3-furancarboxylic acid (20.00 g, 172 mmol) in methanol (350 mL). The reaction mixture was heated to reflux and kept for 18 hours. Upon completion of the reaction, the mixture was cooled to room temperature and concentrated in a rotary evaporator to remove most of the methanol. The concentrated residue was dissolved in water (500 mL) and dichloromethane (200 mL) for partitioning. The organic and aqueous phases were separated and the aqueous phase was extracted once more with dichloromethane (200 mL). All organic phases were combined and washed sequentially with saturated aqueous sodium bicarbonate (200 mL) and brine (200 mL). The organic phases were dried with anhydrous sodium sulfate, filtered and concentrated to afford methyl 3-tetrahydrofurancarboxylate (15.0 g, 67% yield) as a light yellow oil. The product was confirmed by 1H NMR (400 MHz, DMSO-d6): δ 3.85 (t, J = 8.4 Hz, 1H), 3.77-3.66 (m, 3H), 3.62 (s, 3H), 3.07-3.22 (m, 1H), 1.97-2.12 (m, 2H).
References
[1] Journal of Organic Chemistry, 1996, vol. 61, # 8, p. 2690 - 2694
[2] Patent: US2018/201610, 2018, A1. Location in patent: Paragraph 0076; 0077
[3] Advanced Synthesis and Catalysis, 2010, vol. 352, # 2-3, p. 463 - 477
Methyl tetrahydro-3-furoate Preparation Products And Raw materials
Raw materials
Preparation Products
Methyl tetrahydro-3-furoate Suppliers
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9310
- Advantage
- 66
- Tel
- 400-6009262 16621234537
- Fax
- 021-64823266
- chenyj@titansci.com
- Country
- China
- ProdList
- 14101
- Advantage
- 59
- Tel
- 021-56491756 13512199871
- Fax
- 021-5649-1756
- 2819742715@qq.com
- Country
- China
- ProdList
- 4000
- Advantage
- 55
- Tel
- 18986259541
- Fax
- 027-87840182
- sales@3stc.com
- Country
- China
- ProdList
- 3765
- Advantage
- 58
- Tel
- 18993966060
- Fax
- 0943-8288977
- sales@techbiochem.com
- Country
- China
- ProdList
- 806
- Advantage
- 61
- Tel
- +86-021-69895597 13776836200 +86-13776836200
- Fax
- 021-61292409
- tocopharm@gmail.com
- Country
- China
- ProdList
- 196
- Advantage
- 55
- Tel
- 021-68367562 15002147577;
- Fax
- 021-68369562
- sales@haoyunchem.com
- Country
- China
- ProdList
- 457
- Advantage
- 55
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 42446
- Advantage
- 60
- Tel
- 0512-63009836 18994340901
- Fax
- 0512-63006936
- helen@struchem.com
- Country
- China
- ProdList
- 3981
- Advantage
- 60
- Tel
- Fax
- -
- eric_feng1954@126.com
- Country
- China
- ProdList
- 9248
- Advantage
- 55
View Lastest Price from Methyl tetrahydro-3-furoate manufacturers
- Product
- Methyl tetrahydro-3-furoate 53662-85-4
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-11-18
- Product
- Methyl tetrahydro-3-furoate 53662-85-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 500kg
- Release date
- 2018-08-16