3-CHLOROPHENETHYL BROMIDE, 97%

Product Name: 3-CHLOROPHENETHYL BROMIDE, 97%
CAS No.: 16799-05-6
Chemical Name: 3-CHLOROPHENETHYL BROMIDE, 97%
Synonyms: 3-chlorobromoethylbenzene;3-CHLOROPHENETHYLBROMIDE,97%;Benzene, 1-(2-bromoethyl)-3-chloro-
CBNumber: CB1972735
Molecular Formula: C8H8BrCl
Formula Weight: 219.51
MOL File: 16799-05-6.mol

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3-CHLOROPHENETHYL BROMIDE, 97% Property

Boiling point:: 85 °C(Press: 0.1 Torr)
Density: 1.489±0.06 g/cm3(Predicted)
Flash point:: 110 °C
storage temp.: Sealed in dry,Room Temperature
Appearance: Colorless to light yellow Liquid

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Safety

Hazard Codes: Xn,N
Risk Statements: 22-41-51/53
Safety Statements: 26-36/37-39-61
RIDADR: UN 3082 9/PG 3
WGK Germany: 2
HS Code: 2903998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 655058
Product name: 3-Chlorophenethyl bromide
Purity: 97%
Packaging: 5g
Price: $130
Updated: 2025/07/31

Sigma-Aldrich

Product number: 655058
Product name: 3-Chlorophenethyl bromide
Purity: 97%
Packaging: 10g
Price: $294
Updated: 2023/06/20

AK Scientific

Product number: 4892AJ
Product name: 1-(2-Bromoethyl)-3-chlorobenzene
Packaging: 1g
Price: $83
Updated: 2021/12/16

Matrix Scientific

Product number: 126824
Product name: 1-(2-Bromoethyl)-3-chlorobenzene
Purity: >95%
Packaging: 5g
Price: $144
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0066637
Product name: 3-CHLOROPHENETHYL BROMIDE
Purity: 95.00%
Packaging: 5G
Price: $932
Updated: 2021/12/16

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3-CHLOROPHENETHYL BROMIDE, 97% Chemical Properties,Usage,Production

Synthesis

5182-44-5

16799-05-6

General procedure for the synthesis of 1-(2-bromoethyl)-3-chlorobenzene from 3-chlorobenzene ethanol: Triphenylphosphine (3.90 g, 14.9 mmol) was added to a stirred solution containing 3-chlorobenzene ethanol (2.0 mL, 14.8 mmol), carbon tetrabromide (4.91 g, 14.8 mmol), and anhydrous dichloromethane (100 mL), under nitrogen protection. The reaction mixture was stirred at room temperature for 5 hours. After completion of the reaction, the reaction mixture was washed sequentially with water (100 mL) and brine (100 mL). The organic layer was separated, dried with magnesium sulfate, filtered and concentrated on a rotary evaporator to give the crude product. The crude product was purified by rapid chromatography on silica gel using 100% hexane as eluent to give 2.30 g (71% yield) of 1-(2-bromoethyl)-3-chlorobenzene. Thin layer chromatography (TLC) analysis: Rf value was 0.27 in 100% hexane; 1H NMR (CDCl3) data: δ 7.26-7.11 (m, 3H), 7.09-7.07 (m, 1H), 3.54 (t, 2H), 3.12 (t, 2H).

References

[1] Journal of Medicinal Chemistry, 1996, vol. 39, # 20, p. 4017 - 4026
[2] Patent: WO2004/26305, 2004, A1. Location in patent: Page/Page column 67-68
[3] Patent: US2002/19531, 2002, A1
[4] Journal of the Chemical Society, 1964, p. 1548 - 1553
[5] Tetrahedron Asymmetry, 1998, vol. 9, # 15, p. 2725 - 2737

3-CHLOROPHENETHYL BROMIDE, 97% Preparation Products And Raw materials

Raw materials

Preparation Products

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3-CHLOROPHENETHYL BROMIDE, 97% Suppliers

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View Lastest Price from 3-CHLOROPHENETHYL BROMIDE, 97% manufacturers

Henan Fengda Chemical Co., Ltd

Product: 3-CHLOROPHENETHYL BROMIDE, 97% 16799-05-6
Price: US $101.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-29

16799-05-6, 3-CHLOROPHENETHYL BROMIDE, 97%Related Search:

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3-CHLOROPHENETHYLBROMIDE,97%

Benzene, 1-(2-bromoethyl)-3-chloro-

3-chlorobromoethylbenzene

16799-05-6

ClC6H4CH2CH2Br