Water peak Application
ChemicalBook > CAS DataBase List > Chloroform-d

Chloroform-d

Water peak Application
Product Name
Chloroform-d
CAS No.
865-49-6
Chemical Name
Chloroform-d
Synonyms
deuterated chloroform;CHLOROFORM-D1;Deuteriochloroform;Deuterotrichloromethane;Methane-d, trichloro-;Chloroform-d, 99.8 atom % D, anhydrous;CHLOROFORM-D, 99.8 ATOM % D(CONTAINS 1%V/V TMS);Chloroform-d,for NMR,100.0 atom % D, packagedin 0.50 ml ampules;oroform-d;d,ChloroforM
CBNumber
CB2103569
Molecular Formula
CCl3D
Formula Weight
120.38
MOL File
865-49-6.mol
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Chloroform-d Property

Melting point:
−64 °C(lit.)
Boiling point:
60.9 °C(lit.)
Density 
1.500 g/mL at 25 °C(lit.)
vapor pressure 
211 hPa (20 °C)
refractive index 
n20/D 1.444(lit.)
Flash point:
62°C
storage temp. 
Store at +2°C to +8°C.
solubility 
Miscible with organic solvents, ethyl acetate and acetone.
form 
Liquid
Specific Gravity
1.505
color 
White to beige
Sensitive 
Moisture Sensitive
BRN 
1697633
Exposure limits
ACGIH: TWA 10 ppm
OSHA: Ceiling 50 ppm(240 mg/m3)
NIOSH: IDLH 500 ppm; STEL 2 ppm(9.78 mg/m3)
Stability:
Stable. Incompatible with strong bases, alkali metals, aluminium, magnesium, strong oxidizing agents.
InChIKey
HEDRZPFGACZZDS-MICDWDOJSA-N
LogP
1.5-1.6 at 20-23℃ and pH9
Surface tension
72.3mN/m at 998.5mg/L and 20℃
CAS DataBase Reference
865-49-6(CAS DataBase Reference)
EPA Substance Registry System
Chloroform-d (865-49-6)
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Safety

Hazard Codes 
Xn,T
Risk Statements 
22-38-40-48/20/22-48/20-36/38-20/22-63
Safety Statements 
36/37
RIDADR 
UN 1888 6.1/PG 3
WGK Germany 
2
HazardClass 
6.1
PackingGroup 
III
HS Code 
28459000
Toxicity
LD50 orally in Rabbit: 695 mg/kg LD50 dermal Rabbit > 3980 mg/kg
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H331Toxic if inhaled

H336May cause drowsiness or dizziness

H351Suspected of causing cancer

H372Causes damage to organs through prolonged or repeated exposure

Precautionary statements

P201Obtain special instructions before use.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P308+P313IF exposed or concerned: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
151823
Product name
Chloroform-d
Purity
99.8 atom % D
Packaging
10x0.6ml
Price
$38.4
Updated
2024/03/01
Sigma-Aldrich
Product number
151823
Product name
Chloroform-d
Purity
99.8 atom % D
Packaging
10x0.75ml
Price
$40.2
Updated
2024/03/01
Sigma-Aldrich
Product number
1.03420
Product name
Chloroform-D1
Purity
deuteration degree min. 99.8% for NMR spectroscopy (stabilized with silver) MagniSolv?
Packaging
25mL
Price
$43.4
Updated
2024/03/01
Sigma-Aldrich
Product number
1.03420
Product name
Chloroform-D1
Purity
deuteration degree min. 99.8% for NMR spectroscopy (stabilized with silver) MagniSolv?
Packaging
100mL
Price
$109
Updated
2024/03/01
Sigma-Aldrich
Product number
1.03420
Product name
Chloroform-D1
Purity
deuteration degree min. 99.8% for NMR spectroscopy (stabilized with silver) MagniSolv?
Packaging
500mL
Price
$449
Updated
2024/03/01
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Chloroform-d Chemical Properties,Usage,Production

Water peak

The position of the water peak in different deuterated reagents is not the same. The water peak of heavy water is about 4.67 ppm. There is a trend that the more water the low field.
Chloroform-D is less soluble with water and the water content is low, so its water peak near 1.59 ppm. Deuterated acetone is about 2.8 ppm and the deuterated dimethylsulfoxide has a water peak of about 3.4 ppm. If water is added to deuterated acetone, the water peak will gradually move to a low field and eventually stop at about 4.7 ppm.

Application

Chloroform-d has been employed as solvent in a 1H NMR (Proton Nuclear Magnetic Resonance) spectroscopic study. It has been employed as solvent during the 31PNMR (Phosphorus-31 nuclear magnetic resonance) spectral investigation of triphenyl phosphate and tris(2-chloroethyl) phosphate. It has also been used as the deuterated solvent in the 1H NMR spectral studies of 2-(4-bromobenzyl)-3-hydroxypropanoic acid and 3-hydroxy-2-(4-methoxybenzyl)propanoic acid. It has also been used as the deuterated solvent for the 1HNMR spectral studies of  3,3′-dihydroxy-4,4′-diamino-biphenyl (HAB) and 2,2′-bis-(3,4-dicarboxy-phenyl) hexafluoropropane dianhydride (6FDA) polyimide.Chloroform-d has been employed as solvent in a 1H NMR (Proton Nuclear Magnetic Resonance) spectroscopic study. It has been employed as solvent during the 31PNMR (Phosphorus-31 nuclear magnetic resonance) spectral investigation of triphenyl phosphate and tris(2-chloroethyl) phosphate. It has also been used as the deuterated solvent in the 1H NMR spectral studies of 2-(4-bromobenzyl)-3-hydroxypropanoic acid and 3-hydroxy-2-(4-methoxybenzyl)propanoic acid. It has also been used as the deuterated solvent for the 1HNMR spectral studies of  3,3′-dihydroxy-4,4′-diamino-biphenyl (HAB) and 2,2′-bis-(3,4-dicarboxy-phenyl) hexafluoropropane dianhydride (6FDA) polyimide.

Description

Deuterated chloroform (CDCl3), also known as chloroform-d, is an excellent everyday solvent choice for scientists who demand exceptional results. Commonly used as a solvent in proton NMR (1H NMR) spectroscopy, chloroform-d can dissolve a vast array of compounds with ease due to its weak polarity. It is often used in combination with methanol-d as a cosolvent. Plus, its low boiling point makes it relatively easy to recover a sample post-NMR analysis or during organic syntheses.

Chemical Properties

colourless liquid

Uses

Chloroform-d is widely used in the organic solvent for the NMR analysis.

Uses

Chloroform-d may be used in the synthesis of dichlorofluoromethane-d (DCFM).

Uses

Labelled Chloroform, generally in trimethylsilane solution, used in NMR spectroscopy as a solvent. Unlabelled chloroform has been used an an anaesthetic due to its action on the central nervous system .

Definition

ChEBI: Deuterated chloroform is a deuterated compound that is an isotopologue of chloroform in which the hydrogen atom is replaced with deuterium. Commonly used as a solvent in proton NMR spectroscopy. It has a role as a non-polar solvent, a NMR solvent and a NMR chemical shift reference compound. It is a deuterated compound and a member of chloromethanes.

General Description

Chloroform-d (Deuterochloroform, CDCl3), deuterated chloroform, is a 100% isotopically enriched NMR (Nuclear Magnetic Resonance) solvent. It is widely employed in high resolution NMR studies due to its high chemical and isotopic purity. Quantitaive infrared spectral investigations of carbon-deuterium stretching bands of chloroform-d in various organic solvents have been reported. Raman difference spectroscopic studies of mixtures of chloroform-d and liquid chloroform have been conducted to evaluate frequency shifts in the in the ν1 and ν2 bands of CHCl3 and CDCl3.

Chloroform-d Preparation Products And Raw materials

Raw materials

Preparation Products

4-AMINO-3-FORMYLPYRIDINE
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View Lastest Price from Chloroform-d manufacturers

Henan Fengda Chemical Co., Ltd
Product
Chloroform-d 865-49-6
Price
US $100.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-23
Hangzhou ICH Biofarm Co., Ltd
Product
Chloroform-D 865-49-6
Price
US $0.00/kg
Min. Order
200kg
Purity
99%
Supply Ability
plenty of stock
Release date
2023-07-05
Hebei Senko Biotechnology Co., Ltd.
Product
Chloroform-d 865-49-6
Price
US $100.00/KG/Tin
Min. Order
1KG
Purity
99%
Supply Ability
10Tons
Release date
2021-07-20

865-49-6, Chloroform-dRelated Search:

Ethyl (2,4,6-trimethylbenzoyl) phenylphosphinate 5α-Cholestane NMR REF STD, 0.0485M TRIPHENYLPHOSPHATE IN CHLOROFORM-D, 99.9 ATOM % D,NMR REF STD, 0.0485M TRIPHENYLPHOSPHATEIN CHLOROFORM-D,99.8 ATOM % D PHENOL:CHLOROFORM:ISOAMYLALCOHOL 49.5:49 .5:1,PHENOL:CHLOROFORM:ISOAMYL ALC. 125:24:1, FOR MOL. BIOLOGY BETA-SITOSTEROL 1X1ML CHLOROFORM 100UG/M L Dichloromethane 100 MG/ML CHOLESTERYL ACETATE IN CHLOROFORM-D Chloroform Chloroform-d DICHLOROMETHANE D CHLOROFORM-D + 1% TMS (V/V) ACETONE-D6 ACETONE CHLOROFORM HEMIHYDRATE DAB, PH. EUR., B.P., N. F., PH. FRANC. TRIS(DIBENZYLIDENEACETONE)DIPALLADIUM(0) CHLOROFORM ADDUCT 98+% METHANE (D1) DEUTERIUM HYDRIDE 0.1% ETHYLBENZENE IN CHLOROFORM-D (540 PP TUBE) 30% MENTHOL IN CHLOROFORM-D

  • Deuterotrichloromethane
  • Trichloro(2H)methane
  • trichloro-deuterio-methane
  • CHLOROFORM-D >99.95 (ATOM % D) STAB.
  • CHLOROFORM-D, "100" (MIN. 99.96 ATOM % D)(1PK=10 X 0.75ML)
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  • Chloroform-d, 99.8 atom % D, anhydrous
  • CHLOROFORM-D, 99.8 ATOM % D(CONTAINS 1%V/V TMS)
  • CHLOROFORM-D, 99.8 ATOM % D, STABILIZEDWITH 0.5 WT% SILVER FOIL (CONTAINS 0.03%(
  • CHLOROFORM-D, "100" (MIN. 99.96 ATOM % D) CONTAINS 0.03% V/V TMS(1PK=10 X 0.75ML
  • CHLOROFORM-D, 99.9 ATOM % D (CONTAINS 0.03% V/V TMS)
  • CHLOROFORM-D, 99.8 ATOM % D (CONTAINS 0.03% V/V TMS)
  • CHLOROFORM-D, "100" (MIN. 99.96 ATOM % D) CONTAINS 0.03% V/V TMS
  • Chloroform-D,IsotopicPurity>99Atom%D
  • Chloroform-d, isotopic purity
  • Chloroform-d,100%D(Isotopic),contains0.03%v/vTMS
  • Chloroform-d,99.8%(Isotopic),contains0.03%v/vTMS
  • Chloroform-d, 100 atom % D, packaged in 0.75 ml ampules, for NMR
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  • Chloroform-d, 99.6+ atom % D, for NMR
  • Chloroform-d, 99.8 atom % D, contains 1 v/v% TMS, for NMR
  • Chloroform-d, 99.8 atom % D, for NMR
  • Chloroform-d, 99.8 atom % D, packaged in 0.75 ml ampules, for NMR
  • Chloroform-d, 99.8 atom % D, packaged in 1 ml ampules, for NMR
  • Chloroform-d, 99.8 atom % D, stabilized with silver foil, for NMR
  • Chloroform-d, 99.8% D, stabilized with silver foil, 1 v/v% TMS, for NMR
  • Chloroform-d, 99.8+ atom % D, contains 0.03 v/v% TMS, for NMR
  • Chloroform-d, 99.8+% D, stab. with silver foil, 0.03 v/v% TMS, for NMR
  • ChloroformD>99.96%10x0.75ml
  • ChloroformD>99.96%+0.03%tms
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  • ChloroformD>99.8%10x0.75ml
  • ChloroformD>99.8%5x10ml
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  • ChloroformD>99.96%
  • ChloroformD>99.96%10x0.75ml(+0.03%tms)
  • Chloroform-d,for NMR,100.0 atom % D, packagedin 0.50 ml ampules
  • Chloroform-d,for NMR,99.8+ atom % D, contains0.03 v/v% TMS
  • Chloroform-d,for NMR,contains 0.03 v/v% TMS,99.8+ atom % D
  • Chloroform-d,for NMR,99.8 atom % D
  • Chloroform-d,for NMR,99.6+ atom % D
  • Chloroform-d,for NMR,99.8 atom % D, contains1 v/v% TMS
  • Chloroform-d,for NMR,99.8% D, stabilized withsilver foil, 1 v/v% TMS
  • Chloroform-d,for NMR,100 atom % D, packaged in 0.75 ml ampules
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  • Chloroform-d,for NMR,99.8 atom % D, packagedin 0.75 ml ampules
  • Chloroform-d,for NMR,99.8 atom % D, stabilized with silver foil
  • Chloroform-d,Deuterochloroform
  • Chloroform-d "100%" - DELETED
  • Chloroform-d, (D99.8%)+TMS(0.03%)
  • Chloroform-d, 100 atom % D, packaged in 0.75 ml ampoules, for NMR
  • Chloroform-d, 99.8 atom % D, packaged in 0.75 ml ampoules, for NMR
  • Chloroform-d, 99.8 atom % D, packaged in 1 ml ampoules, for NMR
  • Chloroform-d, 99.8 atom % D, AcroSeal, for NMR
  • ChloroforM-d, for NMR, 99.8 atoM % D, packaged in 1 Ml aMpoules
  • ChloroforM-d, for NMR, 100 atoM % D, packaged in 0.75 Ml aMpoules