Chloroform-d

ChemicalBook > CAS DataBase List > Chloroform-d

Water peak Application

Product Name: Chloroform-d
CAS No.: 865-49-6
Chemical Name: Chloroform-d
Synonyms: deuterated chloroform;CHLOROFORM-D1;Deuteriochloroform;Deuterotrichloromethane;Methane-d, trichloro-;Chloroform-d, 99.8 atom % D, anhydrous;CHLOROFORM-D, 99.8 ATOM % D(CONTAINS 1%V/V TMS);Chloroform-d,for NMR,100.0 atom % D, packagedin 0.50 ml ampules;oroform-d;d,ChloroforM
CBNumber: CB2103569
Molecular Formula: CCl3D
Formula Weight: 120.38
MOL File: 865-49-6.mol

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Chloroform-d Property

Melting point:: −64 °C(lit.)
Boiling point:: 60.9 °C(lit.)
Density: 1.500 g/mL at 25 °C(lit.)
vapor pressure: 211 hPa (20 °C)
refractive index: n20/D 1.444(lit.)
Flash point:: 62°C
storage temp.: Store at +2°C to +8°C.
solubility: Miscible with organic solvents, ethyl acetate and acetone.
form: Liquid
Specific Gravity: 1.505
color: White to beige
Sensitive: Moisture Sensitive
BRN: 1697633
Exposure limits: ACGIH: TWA 10 ppm
OSHA: Ceiling 50 ppm(240 mg/m3)
NIOSH: IDLH 500 ppm; STEL 2 ppm(9.78 mg/m3)
Stability:: Stable. Incompatible with strong bases, alkali metals, aluminium, magnesium, strong oxidizing agents.
InChIKey: HEDRZPFGACZZDS-MICDWDOJSA-N
LogP: 1.5-1.6 at 20-23℃ and pH9
Surface tension: 72.3mN/m at 998.5mg/L and 20℃
CAS DataBase Reference: 865-49-6(CAS DataBase Reference)
EPA Substance Registry System: Chloroform-d (865-49-6)

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Safety

Hazard Codes: Xn,T
Risk Statements: 22-38-40-48/20/22-48/20-36/38-20/22-63
Safety Statements: 36/37
RIDADR: UN 1888 6.1/PG 3
WGK Germany: 2
HazardClass: 6.1
PackingGroup: III
HS Code: 28459000
Toxicity: LD50 orally in Rabbit: 695 mg/kg LD50 dermal Rabbit > 3980 mg/kg

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H331Toxic if inhaled

H336May cause drowsiness or dizziness

H351Suspected of causing cancer

H372Causes damage to organs through prolonged or repeated exposure

Precautionary statements

P201Obtain special instructions before use.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P308+P313IF exposed or concerned: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 151823
Product name: Chloroform-d
Purity: 99.8 atom % D
Packaging: 10x0.6ml
Price: $38.4
Updated: 2024/03/01

Sigma-Aldrich

Product number: 151823
Product name: Chloroform-d
Purity: 99.8 atom % D
Packaging: 10x0.75ml
Price: $40.2
Updated: 2024/03/01

Sigma-Aldrich

Product number: 1.03420
Product name: Chloroform-D1
Purity: deuteration degree min. 99.8% for NMR spectroscopy (stabilized with silver) MagniSolv?
Packaging: 25mL
Price: $43.4
Updated: 2024/03/01

Sigma-Aldrich

Product number: 1.03420
Product name: Chloroform-D1
Purity: deuteration degree min. 99.8% for NMR spectroscopy (stabilized with silver) MagniSolv?
Packaging: 100mL
Price: $109
Updated: 2024/03/01

Sigma-Aldrich

Product number: 1.03420
Product name: Chloroform-D1
Purity: deuteration degree min. 99.8% for NMR spectroscopy (stabilized with silver) MagniSolv?
Packaging: 500mL
Price: $449
Updated: 2024/03/01

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Chloroform-d Chemical Properties,Usage,Production

Water peak

The position of the water peak in different deuterated reagents is not the same. The water peak of heavy water is about 4.67 ppm. There is a trend that the more water the low field.
Chloroform-D is less soluble with water and the water content is low, so its water peak near 1.59 ppm. Deuterated acetone is about 2.8 ppm and the deuterated dimethylsulfoxide has a water peak of about 3.4 ppm. If water is added to deuterated acetone, the water peak will gradually move to a low field and eventually stop at about 4.7 ppm.

Application

Reagents for nuclear magnetic instruments

Chemical Properties

colourless liquid

Uses

Chloroform-d is widely used in the organic solvent for the NMR analysis.

Uses

Chloroform-d may be used in the synthesis of dichlorofluoromethane-d (DCFM).

Uses

Labelled Chloroform, generally in trimethylsilane solution, used in NMR spectroscopy as a solvent. Unlabelled chloroform has been used an an anaesthetic due to its action on the central nervous system .

Definition

ChEBI: Deuterated chloroform is a deuterated compound that is an isotopologue of chloroform in which the hydrogen atom is replaced with deuterium. Commonly used as a solvent in proton NMR spectroscopy. It has a role as a non-polar solvent, a NMR solvent and a NMR chemical shift reference compound. It is a deuterated compound and a member of chloromethanes.

General Description

Chloroform-d (Deuterochloroform, CDCl₃), deuterated chloroform, is a 100% isotopically enriched NMR (Nuclear Magnetic Resonance) solvent. It is widely employed in high resolution NMR studies due to its high chemical and isotopic purity. Quantitaive infrared spectral investigations of carbon-deuterium stretching bands of chloroform-d in various organic solvents have been reported. Raman difference spectroscopic studies of mixtures of chloroform-d and liquid chloroform have been conducted to evaluate frequency shifts in the in the ν₁ and ν₂ bands of CHCl₃ and CDCl₃.

Chloroform-d Preparation Products And Raw materials

Raw materials

Preparation Products

4-AMINO-3-FORMYLPYRIDINE

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View Lastest Price from Chloroform-d manufacturers

Henan Fengda Chemical Co., Ltd

Product: Chloroform-d 865-49-6
Price: US $100.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-23

Hebei Duling International Trade Co. LTD

Product: Chloroform-d 865-49-6
Price: US $30.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 tons
Release date: 2023-03-30

Hangzhou ICH Biofarm Co., Ltd

Product: Chloroform-D 865-49-6
Price: US $0.00/kg
Min. Order: 200kg
Purity: 99%
Supply Ability: plenty of stock
Release date: 2023-07-05

865-49-6, Chloroform-dRelated Search:

Ethyl (2,4,6-trimethylbenzoyl) phenylphosphinate 5α-Cholestane NMR REF STD, 0.0485M TRIPHENYLPHOSPHATE IN CHLOROFORM-D, 99.9 ATOM % D,NMR REF STD, 0.0485M TRIPHENYLPHOSPHATEIN CHLOROFORM-D,99.8 ATOM % D PHENOL:CHLOROFORM:ISOAMYLALCOHOL 49.5:49 .5:1,PHENOL:CHLOROFORM:ISOAMYL ALC. 125:24:1, FOR MOL. BIOLOGY BETA-SITOSTEROL 1X1ML CHLOROFORM 100UG/M L Dichloromethane 100 MG/ML CHOLESTERYL ACETATE IN CHLOROFORM-D Chloroform Chloroform-d DICHLOROMETHANE D CHLOROFORM-D + 1% TMS (V/V) ACETONE-D6 ACETONE CHLOROFORM HEMIHYDRATE DAB, PH. EUR., B.P., N. F., PH. FRANC. TRIS(DIBENZYLIDENEACETONE)DIPALLADIUM(0) CHLOROFORM ADDUCT 98+% METHANE (D1) DEUTERIUM HYDRIDE 0.1% ETHYLBENZENE IN CHLOROFORM-D (540 PP TUBE) 30% MENTHOL IN CHLOROFORM-D

Deuterotrichloromethane

Trichloro(2H)methane

trichloro-deuterio-methane

CHLOROFORM-D >99.95 (ATOM % D) STAB.

CHLOROFORM-D, "100" (MIN. 99.96 ATOM % D)(1PK=10 X 0.75ML)

CHLOROFORM-D, "100" (MIN. 99.96 ATOM % D)(1PK=10 X 0.25ML)

Chloroform-d, 99.8 atom % D, anhydrous

CHLOROFORM-D, 99.8 ATOM % D(CONTAINS 1%V/V TMS)

CHLOROFORM-D, 99.8 ATOM % D, STABILIZEDWITH 0.5 WT% SILVER FOIL (CONTAINS 0.03%(

CHLOROFORM-D, "100" (MIN. 99.96 ATOM % D) CONTAINS 0.03% V/V TMS(1PK=10 X 0.75ML

CHLOROFORM-D, 99.9 ATOM % D (CONTAINS 0.03% V/V TMS)

CHLOROFORM-D, 99.8 ATOM % D (CONTAINS 0.03% V/V TMS)

CHLOROFORM-D, "100" (MIN. 99.96 ATOM % D) CONTAINS 0.03% V/V TMS

Chloroform-D,IsotopicPurity>99Atom%D

Chloroform-d, isotopic purity

Chloroform-d,100%D(Isotopic),contains0.03%v/vTMS

Chloroform-d,99.8%(Isotopic),contains0.03%v/vTMS

Chloroform-d, 100 atom % D, packaged in 0.75 ml ampules, for NMR

Chloroform-d, 100.0 atom % D, for NMR

Chloroform-d, 100.0 atom % D, packaged in 0.50 ml ampules, for NMR

Chloroform-d, 99.6+ atom % D, for NMR

Chloroform-d, 99.8 atom % D, contains 1 v/v% TMS, for NMR

Chloroform-d, 99.8 atom % D, for NMR

Chloroform-d, 99.8 atom % D, packaged in 0.75 ml ampules, for NMR

Chloroform-d, 99.8 atom % D, packaged in 1 ml ampules, for NMR

Chloroform-d, 99.8 atom % D, stabilized with silver foil, for NMR

Chloroform-d, 99.8% D, stabilized with silver foil, 1 v/v% TMS, for NMR

Chloroform-d, 99.8+ atom % D, contains 0.03 v/v% TMS, for NMR

Chloroform-d, 99.8+% D, stab. with silver foil, 0.03 v/v% TMS, for NMR

ChloroformD>99.96%10x0.75ml

ChloroformD>99.96%+0.03%tms

ChloroformD>99.8%+0.03%tms

ChloroformD>99.8%10x0.75ml

ChloroformD>99.8%5x10ml

ChloroformD>99.96%10x0.6ml

ChloroformD>99.96%

ChloroformD>99.96%10x0.75ml(+0.03%tms)

Chloroform-d,for NMR,100.0 atom % D, packagedin 0.50 ml ampules

Chloroform-d,for NMR,99.8+ atom % D, contains0.03 v/v% TMS

Chloroform-d,for NMR,contains 0.03 v/v% TMS,99.8+ atom % D

Chloroform-d,for NMR,99.8 atom % D

Chloroform-d,for NMR,99.6+ atom % D

Chloroform-d,for NMR,99.8 atom % D, contains1 v/v% TMS

Chloroform-d,for NMR,99.8% D, stabilized withsilver foil, 1 v/v% TMS

Chloroform-d,for NMR,100 atom % D, packaged in 0.75 ml ampules

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Chloroform-d,for NMR,99.8+% D, stab. with silver foil, 0.03 v/v% TMS

Chloroform-d,for NMR,99.8 atom % D, packagedin 0.75 ml ampules

Chloroform-d,for NMR,99.8 atom % D, stabilized with silver foil

Chloroform-d,Deuterochloroform

Chloroform-d "100%" - DELETED

Chloroform-d, (D99.8%)+TMS(0.03%)

Chloroform-d, 100 atom % D, packaged in 0.75 ml ampoules, for NMR

Chloroform-d, 99.8 atom % D, packaged in 0.75 ml ampoules, for NMR

Chloroform-d, 99.8 atom % D, packaged in 1 ml ampoules, for NMR

Chloroform-d, 99.8 atom % D, AcroSeal, for NMR

ChloroforM-d, for NMR, 99.8 atoM % D, packaged in 1 Ml aMpoules

ChloroforM-d, for NMR, 100 atoM % D, packaged in 0.75 Ml aMpoules