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3-Fluoropyridine-2-carboxylic acid

Product Name
3-Fluoropyridine-2-carboxylic acid
CAS No.
152126-31-3
Chemical Name
3-Fluoropyridine-2-carboxylic acid
Synonyms
3-Fluoropicolinicaci;3-FLUOROPICOLINIC ACID;REF DUPL: 3-fluoropicolinic acid;3-Fluoropyridin-2-carboxylic acid;3-fluropyridine-2-carboxylic acid;3-Fluoro-2-pyridinecarboxylic acid;3-FLUOROPYRIDINE-2-CARBOXYLIC ACID;3-Fluoropyridine-3-Carboxylic Acid;2-Pyridinecarboxylicacid, 3-fluoro-;3-Fluoropyridine-2-carboxylicacid98%
CBNumber
CB2140247
Molecular Formula
C6H4FNO2
Formula Weight
141.1
MOL File
152126-31-3.mol
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3-Fluoropyridine-2-carboxylic acid Property

Melting point:
154°C
Boiling point:
265.2±20.0 °C(Predicted)
Density 
1.419±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,2-8°C
pka
2.71±0.10(Predicted)
form 
powder
color 
White
InChI
InChI=1S/C6H4FNO2/c7-4-2-1-3-8-5(4)6(9)10/h1-3H,(H,9,10)
InChIKey
IRERRSXDWUCFIY-UHFFFAOYSA-N
SMILES
C1(C(O)=O)=NC=CC=C1F
CAS DataBase Reference
152126-31-3(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,Xn
HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC
Product number
F621400
Product name
3-Fluoropicolinicacid
Packaging
250mg
Price
$55
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
F1709
Product name
3-Fluoropyridine-2-carboxylicacid
Purity
98%
Packaging
1g
Price
$8
Updated
2021/12/16
Matrix Scientific
Product number
032594
Product name
3-Fluoro-2-pyridinecarboxylic acid
Purity
98%
Packaging
1g
Price
$14
Updated
2021/12/16
Apolloscientific
Product number
PC7057
Product name
3-Fluoropyridine-2-carboxylicacid
Packaging
1g
Price
$15
Updated
2021/12/16
SynQuest Laboratories
Product number
4H21-3-Y7
Product name
3-Fluoropyridine-2-carboxylic acid
Packaging
1g
Price
$16
Updated
2021/12/16
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3-Fluoropyridine-2-carboxylic acid Chemical Properties,Usage,Production

Uses

3-Fluoropyridine-2-carboxylic acid is mainly used as an intermediate in organic synthesis and medicinal chemistry. It is a synthetic intermediate of tridentate nitrogen ligands in pesticide molecules and transition metal catalytic reactions.

Synthesis

372-47-4

124-38-9

152126-31-3

To a diethyl ether (50 ml) solution of 1,4-diazabicyclo[2.2.2]octane (1.15 g, 10.3 mmol) was slowly added n-butyllithium (2.6 M hexane solution, 3.95 ml, 10.3 mmol) dropwise at -78 °C. The reaction mixture was stirred at -20°C for 1 hr, then a diethyl ether (30 ml) solution of 3-fluoropyridine (1.00 g, 10.29 mmol) was added dropwise at -78°C. The resulting yellow suspension was stirred at -60°C for 1 hr and subsequently cooled to -78°C and an excess of dry ice was added. The reaction solution was slowly warmed to -10°C over a period of 20 min. The precipitate was collected by filtration and the residue was washed with ether to give pure 3-fluoropyridine-2-carboxylic acid (1.20 g, 8.51 mmol, 83% yield).

References

[1] Tetrahedron, 1998, vol. 54, # 42, p. 12859 - 12886
[2] Patent: WO2014/82737, 2014, A1. Location in patent: Page/Page column 38

3-Fluoropyridine-2-carboxylic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Fluoropyridine-2-carboxylic acid Suppliers

Fuxin Fengcheng Chemical Technology Development Co., Ltd.
Tel
0418-2868000 13464847801
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+86-418-3810066
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jingxuan.lu@fcmeditech.com
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China
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Jinan LuoHe PharmaTech Co., Ltd.
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86-0531-68658065 15726150375
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0531-68658065
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1071018499@qq.com
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China
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J & K SCIENTIFIC LTD.
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18210857532; 18210857532
Fax
86-10-82849933
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jkinfo@jkchemical.com
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China
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INTATRADE GmbH
Tel
+49 3493/605464
Fax
+49 3493/605470
Email
sales@intatrade.de
Country
Germany
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ZHIWE CHEMTECH CO LTD
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021-20221225 13917446399
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QQ:115820162
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zwchem@163.com
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China
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Alfa Aesar
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400-6106006
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021-67582001/03/05
Email
saleschina@alfa-asia.com
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China
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30123
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Energy Chemical
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021-021-58432009 400-005-6266
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021-58436166
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sales8178@energy-chemical.com
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China
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Shijiazhuang Sdyano Fine Chemical Co., Ltd.
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0311-89250318 031166536426
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4000311741
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master@sjzsdyn.com
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China
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Wuhan Chemwish Technology Co., Ltd
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86-027-67849912
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86-027-87531808
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sales@chemwish.com
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China
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35896
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Capot Chemical Co., Ltd
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+86 (0) 571 85 58 67 18
Fax
0086-571-85864795
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China
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View Lastest Price from 3-Fluoropyridine-2-carboxylic acid manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
3-FLUOROPYRIDINE-2-CARBOXYLIC ACID 152126-31-3
Price
US $1.10/g
Min. Order
1g
Purity
99.0% min
Supply Ability
100 tons min
Release date
2021-05-26
Henan Aochuang Chemical Co.,Ltd.
Product
3-Fluoropyridine-2-carboxylicacid 152126-31-3
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1Ton
Release date
2022-10-14
PNP Biotech Co. Ltd
Product
3-Fluoropyridine-2-carboxylic acid 152126-31-3
Price
US $0.00/kg
Min. Order
25kg
Purity
98%
Supply Ability
Inquiry
Release date
2023-07-12

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