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Burgess reagent

Product Name
Burgess reagent
CAS No.
29684-56-8
Chemical Name
Burgess reagent
Synonyms
Burgess;(methoxycarbonyl)[(triethylazaniumyl)sulfonyl]azanide;(1E)-1-methoxy-N-(triethylazaniumyl)sulfonylmethanimidate;TP05704;urgess reagent;BURGESS REAGENT;Burgess's reagent;Burgess reagent ,97%;Burgess Reagent (BGS);Arabinitol Impurity 4
CBNumber
CB2152668
Molecular Formula
C8H18N2O4S
Formula Weight
238.3
MOL File
29684-56-8.mol
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Burgess reagent Property

Melting point:
76-79 °C(lit.)
Density 
1.3023 (rough estimate)
refractive index 
1.6300 (estimate)
storage temp. 
-20°C
solubility 
Soluble in organic solvents.
form 
Crystalline Powder
color 
Slightly yellow
Sensitive 
Moisture Sensitive
Merck 
14,1502
BRN 
1432131
InChI
InChI=1S/C8H18N2O4S/c1-5-10(6-2,7-3)15(12,13)9-8(11)14-4/h5-7H2,1-4H3
InChIKey
YSHOWEKUVWPFNR-UHFFFAOYSA-N
SMILES
[N+](CC)(CC)(CC)S(=O)(=O)[N-]C(=O)OC
CAS DataBase Reference
29684-56-8(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36-37/39
WGK Germany 
3
10-21
TSCA 
No
HS Code 
29299090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
365483
Product name
(Methoxycarbonylsulfamoyl)triethylammonium hydroxide, inner salt
Purity
97%
Packaging
1g
Price
$99.5
Updated
2024/03/01
TCI Chemical
Product number
M1279
Product name
(Methoxycarbonylsulfamoyl)triethylammonium Hydroxide Inner Salt
Purity
>97.0%(N)
Packaging
1g
Price
$38
Updated
2024/03/01
TCI Chemical
Product number
M1279
Product name
(Methoxycarbonylsulfamoyl)triethylammonium Hydroxide Inner Salt
Purity
>97.0%(N)
Packaging
5g
Price
$144
Updated
2024/03/01
Alfa Aesar
Product number
L20155
Product name
Burgess Reagent, 96%
Packaging
1g
Price
$74.65
Updated
2024/03/01
Alfa Aesar
Product number
L20155
Product name
Burgess Reagent, 96%
Packaging
5g
Price
$285
Updated
2024/03/01
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Burgess reagent Chemical Properties,Usage,Production

Chemical Properties

slightly yellow crystalline powder

History

The Burgess reagent has been introduced in 1968 and shown shortly afterwards to act as a mild and selective dehydrating reagent. Next to its importance in the construction of olefins from secondary and tertiary alcohols, the Burgess reagent was also utilized to promote several other transformations of great synthetic values in medicinal chemistry.

Uses

Burgess reagent is a selective dehydrating reagent used in organic synthesis. It is used to convert secondary and tertiary alcohol, with an adjacent proton, into alkenes. Burgess reagent is also utilized to promote great synthetic values in medicinal chemistry. It has been used in dehydration of primary amides, formamides and primary nitroalkanes to generate nitriles, isocyanides and nitrile oxides respectively. It forms urethanes when it reacts with primary alcohols.

Uses

Reagent for dehydration of secondary and tertiary alcohols; source of heteroatoms (N, O, S) in organic synthesis.

Preparation

Methoxycarbonylsulfamoyl]triethylammonium hydroxide, inner salt is easily prepared in two simple steps from chlorosulfonyl isocyanate as shown in the following scheme. The white crystalline solid Burgess reagent (m.p : 71-72°C from toluene) is air and moisture sensitive and, as such, needs to be stored in the cold and under an inert atmosphere.

Burgess reagent Preparation Products And Raw materials

Raw materials

Preparation Products

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Burgess reagent Suppliers

Hubei Jingxiang Technology Co., Ltd.
Tel
13347833233
Email
120300346@qq.com
Country
China
ProdList
31
Advantage
58
Aikon International Limited
Tel
025-66028182 18112977050
Fax
(3)02557626880
Email
cfzhang@aikonchem.com
Country
China
ProdList
15818
Advantage
58
Suzhou Stone Lake Pharma Tech Co., Ltd.
Tel
0512-63926206 18913193865
Email
3576139417@qq.com
Country
China
ProdList
63
Advantage
58
Cool Pharm, Ltd
Tel
021-60455363 18019463053
Fax
50966098
Email
sales@coolpharm.com
Country
China
ProdList
12346
Advantage
58
Wuhan chuanghao Biotechnology Co., Ltd
Tel
13361917963
Email
876725023@qq.com
Country
China
ProdList
295
Advantage
58
Shanghai Qianlai Pharmaceutical Technology Co., Ltd.
Tel
021-57216911 17740831186
Email
482109853@qq.com
Country
China
ProdList
462
Advantage
58
Hubei huizepu Pharmaceutical Technology Co., Ltd
Tel
027-027-027-59212684 19371278702
Fax
QQ:2188308251
Email
p19107121455@163.com
Country
China
ProdList
459
Advantage
58
Nanjing Yihua Biotechnology Co., Ltd
Tel
15952064210
Email
184982398@qq.com
Country
China
ProdList
296
Advantage
58
Shanghai Boyle Chemical Co., Ltd.
Tel
021-50182298 021-50180596
Fax
+86-21-57758967
Email
sales@boylechem.com
Country
China
ProdList
2208
Advantage
55
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
94657
Advantage
76
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View Lastest Price from Burgess reagent manufacturers

Henan Fengda Chemical Co., Ltd
Product
Burgess reagent 29684-56-8
Price
US $5.00-0.50/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2024-01-13
Zhuozhou Wenxi import and Export Co., Ltd
Product
(Methoxycarbonylsulfamoyl)triethylammonium hydroxide, inner salt 29684-56-8
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-06-27
Career Henan Chemical Co
Product
Burgess reagent 29684-56-8
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
10KG
Release date
2019-08-05

29684-56-8, Burgess reagentRelated Search:


  • BURGESS REAGENT
  • METHOXYCARBONYLSULFAMOYL-TRIETHYLAMMON. HYDROXIDE,INNER SALT
  • MethylN-(Triethylammoniumsulphonyl)Carbamate
  • (METHOXYCARBONYLSULFAMOYL)TRIETHYLAMMONIUM HYDROXIDE
  • (METHOXYCARBONYLSULFAMOYL)TRIETHYLAMMONIUM HYDROXIDE, INNER SALT
  • METHYL N-(TRIETHYLAMMONIOSULFONYL)CARBAMATE
  • N,N-DIETHYL-N-(((METHOXYCARBONYL)AMINO)SULFONYL)ETHANAMINIUM, INNER SALT
  • BURGESS REAGENT METHYL N-(TRIETHYLAMMONIUMSULPHONYL)CARBAMATE
  • ((methoxycarbonyl)sulfamoyl)triethylammonium
  • (METHOXYCARBONYLSULFAMOYL) TRIETHYLAMMONIUM HYDROX
  • (METHOXYCARBONYLSULFAMOYL)TRIETHYLAMMONIUM HYDROXIDE, INNER SALT (BURGESS REAGENT)
  • Burgess
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  • Burgess reagent, Methyl N-(triethylammoniosulfonyl)carbamate
  • Burgess reagent ,97%
  • (Methoxycarbonylsulfamoyl)triethylammonium hydroxide, 97%, inner salt
  • (Methoxycarbonyl)[(triethylaminio)sulfonyl]amineanion
  • [(Triethylaminio)sulfonyl](methoxycarbonyl)amineanion
  • Methoxycarbonyl(triethylaminiosulfonyl)amineanion
  • N-(Triethylaminiosulfonyl)-1-oxo-2-oxa-1-propanamine anion
  • Triethylaminiosulfonyl(methoxycarbonyl)amineanion
  • METHYL (TRIETHYLAMMONIOSULFONYL)CARBAMATE
  • (MethoxycarbonylsulfaMoyl)triethylaMMoniuM hydroxide, inner salt, 97% 5GR
  • Burgess Reagent (CarboxysulfaMoyl)triethylaMMoniuM hydroxide inner salt Methyl ester
  • (MethoxycarbonylsulfaMoyl)triethylaMMoniuM hydroxide, inner salt 97%
  • (1E)-1-methoxy-N-(triethylazaniumyl)sulfonylmethanimidate
  • Burgess's reagent
  • (methoxycarbonyl)[(triethylazaniumyl)sulfonyl]azanide
  • (Methoxycarbonylsulfamoyl)triethylammoniumHydroxideInnerSalt&gt
  • Burgess reagent, 97%, for synthesis
  • TP05704
  • Ethanaminium, N,N-diethyl-N-[[(methoxycarbonyl)amino]sulfonyl]-, inner salt
  • triethyl({[(E)-[methoxy(oxido)methylidene]amino]sulfonyl})azanium
  • Burgess Reagent,(Methoxycarbonylsulfamoyl)triethylammonium Hydroxide Inner Salt
  • WIDELY Burgess reagent
  • triethyl({[(methoxycarbonyl)imino](oxido)oxo-λ-sulfanyl})azanium
  • triethyl(methoxycarbonylsulfamoyl)azanium
  • urgess reagent
  • Ethanaminium, N,N-diethyl-N-[[(methoxycarbonyl)amino]sulfonyl]-, inner salt (9CI, ACI)
  • 1-Methoxy-N-triethylammoniosulfonyl-methanimidate (burges reagent)
  • Burgess Reagent (BGS)
  • Arabinitol Impurity 4
  • 29684-56-8
  • C8H18N2O4S1
  • CH3O2CNSO2NC2H53
  • C8H19N2O4S
  • C8H18N2O4S
  • Synthetic Reagents
  • Dehydrating Reagents
  • Quaternary Ammonium Compounds
  • Ammonium Polyhalides, etc. (Quaternary)
  • Ammonium Polyhalides, etc. (Quaternary)
  • Quaternary Ammonium Compounds
  • API intermediates
  • Burgess reagent
  • 3
  • 1
  • API