4-(Pyridin-2-yl)butan-1-ol

Product Name: 4-(Pyridin-2-yl)butan-1-ol
CAS No.: 17945-79-8
Chemical Name: 4-(Pyridin-2-yl)butan-1-ol
Synonyms: 2-Pyridinebutanol;4-(2-Pyridyl)-1-butanol;4-(2-pyridinyl)-1-butanol;4-(pyridin-2-yl)butan-1-ol
CBNumber: CB21563861
Molecular Formula: C9H13NO
Formula Weight: 151.21
MOL File: 17945-79-8.mol

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4-(Pyridin-2-yl)butan-1-ol Property

Boiling point:: 127-128 °C(Press: 5 Torr)
Density: 1.035±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 15.09±0.10(Predicted)

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: P996975
Product name: 4-(Pyridin-2-yl)butan-1-ol
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: OR918342
Product name: 4-(Pyridin-2-yl)butan-1-ol
Purity: 95%
Packaging: 1g
Price: $335
Updated: 2021/12/16

AK Scientific

Product number: 6014AJ
Product name: 4-(Pyridin-2-yl)butan-1-ol
Packaging: 10g
Price: $658
Updated: 2021/12/16

Alichem

Product number: 17945798
Product name: 4-(Pyridin-2-yl)butan-1-ol
Packaging: 10g
Price: $692.01
Updated: 2021/12/16

AccelPharmtech

Product number: C1516
Product name: 4-(pyridin-2-yl)butan-1-ol
Purity: 97.00%
Packaging: 5G
Price: $1830
Updated: 2021/12/16

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4-(Pyridin-2-yl)butan-1-ol Chemical Properties,Usage,Production

Synthesis

395652-44-5

17945-79-8

GENERAL STEPS: 4-(2-pyridyl)-3-butyn-1-ol (0.4 g, 2.72 mmol) was dissolved in ethanol (12 mL) to prepare a 0.23 M solution. The solution was passed through a hydrogenation reactor equipped with 10% Pd(OH)2 catalyst (flow rate: 1.0 mL/min; pressure: 1.0 bar; temperature: 25°C). Upon completion of the reaction, the effluent was concentrated to dryness to afford 4-(2-pyridyl)-1-butanol (0.36 g, 88% yield), and the product could be used in the subsequent steps without further purification. rf = 1.11 mm. mass spectra (ESI) m/z: 152 [M+H]+, 174 [M+Na]+. 1H NMR (DMSO-d6) δ: 8.49-8.43 (m, 2H), 7.68 (td, 1H, J = 7.6, 1.9 Hz), 7.23 (d, 1H, J = 7.6 Hz), 7.18 (ddd, 1H, J = 7.6, 5.4, 1.9 Hz), 3.40 (t, 2H, J = 6.6 Hz), 2.71 (t, 2H, J = 6.6 Hz), 1.74-1.63 (m 2H), 1.50-1.39 (m, 2H).

References

[1] European Journal of Organic Chemistry, 2011, # 2, p. 271 - 279
[2] Patent: WO2014/144836, 2014, A2. Location in patent: Paragraph 0528; 0529
[3] Bioorganic and Medicinal Chemistry Letters, 2001, vol. 11, # 8, p. 1077 - 1080

4-(Pyridin-2-yl)butan-1-ol Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(Pyridin-2-yl)butan-1-ol Suppliers

China 31 Germany 1 India 1 United Kingdom 1 United States 6 Global 40

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17945-79-8