ChemicalBook > CAS DataBase List > N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE

Product Name
N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
CAS No.
2842-44-6
Chemical Name
N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
Synonyms
FirstCure MHPT;2-(N-Methyl-p-toluidino);HYDROXYETHYL METHYLTOLUIDINE;Hydroxyethyl methyltolylamine;2-(N-methyl-p-toluidino)ethanol;2-(Methyl(p-tolyl)aMino)ethanol;N-methyl-hydroxyethyl-p-toluidine;2-(N-Methyl-N-4-tolylamino)ethanol;2-(N-methyl-N-p-tolylamino)ethanol;2-(Methyl(p-tolyl)amino)ethan-1-ol
CBNumber
CB2158428
Molecular Formula
C10H15NO
Formula Weight
165.23
MOL File
2842-44-6.mol
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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Property

Boiling point:
152-154 °C(Press: 10 Torr)
Density 
1.047±0.06 g/cm3(Predicted)
vapor pressure 
0.062-0.115Pa at 20-25℃
storage temp. 
Sealed in dry,Room Temperature
form 
Liquid:viscous
pka
14.69±0.10(Predicted)
LogP
2.2 at 25℃ and pH6
EPA Substance Registry System
Ethanol, 2-[methyl(4-methylphenyl)amino]- (2842-44-6)
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Safety

HS Code 
2933599590
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
CHM0290557
Product name
N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
Purity
98.00%
Packaging
5MG
Price
$502.35
Updated
2021/12/16
Labseeker
Product number
SC-91423
Product name
2-(Methyl(p-tolyl)amino)ethanol
Purity
95
Packaging
1kg
Price
$700
Updated
2021/12/16
Crysdot
Product number
CD12088559
Product name
2-(Methyl(p-tolyl)amino)ethanol
Purity
95+%
Packaging
100g
Price
$50
Updated
2021/12/16
Crysdot
Product number
CD12088559
Product name
2-(Methyl(p-tolyl)amino)ethanol
Purity
95+%
Packaging
500g
Price
$150
Updated
2021/12/16
Chemenu
Product number
CM274824
Product name
2-(Methyl(p-tolyl)amino)ethanol
Purity
95%
Packaging
1000g
Price
$234
Updated
2021/12/16
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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Chemical Properties,Usage,Production

Uses

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE is an amine organic compound, which can be used as intermediate in organic synthesis.

Synthesis

Add reactant (0.2 mmol, 1.0 equiv), THF (2.0 mL) and CH2Br2 (0.6 mmol, 3.0 equiv) to a flame-dried 10 mL Schlenk tube in a glove box. Seal and take out of the glove box. Cool the reaction mixture to -78°C. Add nBuLi (0.56 mmol, 2.8 equiv) dropwise under N2 atmosphere within 3minutes. Stir the reaction at -78°C for 30 minutes and add ZnCl2 (0.1 mL, 0.5equiv, 1.0 M in Et2O). Allow the mixture to warm to room temperature and stir for 1 hour. Cool the mixture to 0°C. Add a premixture of H2O2 (30% in H2O, 0.5 mL) and NaOH (2.0 M, 1.0 mL). Stir the mixture at room temperature for another 1 hour and dilute with water (20 mL). Extract with DCM (30 mL x 2) and dry over Na2SO4. Filter and concentrate under vacuum. Purify the crude product by silica gel flash column chromatography to obtain product. 1H NMR (CDCl3, 500 MHz) δ 7.08 (d, J = 8.4 Hz, 2H), 6.78 (d, J = 8.4 Hz,2H), 3.80 (t, J = 5.6 Hz, 2H), 3.43 (t, J = 5.4 Hz, 2H), 2.93 (s, 3H), 2.28 (s, 3H), 2.01 (brs, 1H). 13C NMR (CDCl3, 125 MHz) δ 148.3, 129.8, 127.1, 114.0, 60.1, 56.2, 39.1, 20.4.
Fig The synthetic method of N-(2-hydroxyethyl)-N-methyl-4-toluidine

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Suppliers

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View Lastest Price from N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE manufacturers

Hebei Mojin Biotechnology Co., Ltd
Product
N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 2842-44-6
Price
US $0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
50000KG/month
Release date
2023-08-29
Hebei Guanlang Biotechnology Co., Ltd.
Product
N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 2842-44-6
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2021-07-30

2842-44-6, N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINERelated Search:

N-(2-Hydroxyethyl)-N-methylaniline N-Methylaniline 4-Nitro-N-methylphthalimide 2,2'-(P-TOLYLIMINO)DIETHANOL Riboflavin 2-[(2-amino-5-methylph2-[(2-amino-5-methylphenoxy)methyl]-6-methoxy-8-aminoquinoline-n,n,n',n'-tetraacetic acid tetrapotassium saltenoxy)methyl]-6-methoxy-8-aminoquinoline-n,n,n FLAVIN ADENINE DINUCLEOTIDE Riboflavin 5'-Monophosphate Sodium Salt 4-MORPHOLINOACETOPHENONE 3-AMINO-4-(4-MORPHOLINO)BENZOTRIFLUORIDE Fura 2-AM Diisopropanol-p-toluidine N-METHYL-P-TOLUIDINE 4'-MORPHOLINOPROPIOPHENONE 1-(4-MORPHOLINO-3-NITROPHENYL)-1-ETHANONE 4-MORPHOLINOBENZOPHENONE INDO 1-AM INDO 1 PENTAPOTASSIUM SALT

  • N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
  • 2-(N-methyl-p-toluidino)ethanol
  • N-Methyl-N-hydroxyethyl-P-toluidine
  • N-(2-Hydroxyethyl)-N-methyl-p-toluidine
  • 2-[Methyl(4-methylphenyl)amino]ethanol
  • 2-(N-Methyl-N-4-tolylamino)ethanol
  • FirstCure MHPT
  • N-Methyl-N-(2-hydroxyethyl)-p-toluidine
  • 2-(Methyl(p-tolyl)aMino)ethanol
  • 2-(N-methyl-N-p-tolylamino)ethanol
  • N-(2-HYDROXYETHYL)-N-METHYL-PARA-TOLUIDINE(MPHT)
  • N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE(MHPT)
  • Hydroxyethyl methyltolylamine
  • (5S,8R,9S,10S,13S,14S,17R)-17-ethynyl-3,3-difluoro-10,13-dimethyl-2,4,5,6,7,8,9,11,12,14,15,16-dodecahydro-1H-cyclopenta[a]phenanthren-17-ol
  • 2-(N-Methyl-p-toluidino)
  • Ethanol, 2-[methyl(4-methylphenyl)amino]-
  • N-methyl-hydroxyethyl-p-toluidine
  • HYDROXYETHYL METHYLTOLUIDINE
  • 2842-44-6 N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
  • 2-(Methyl(p-tolyl)amino)ethan-1-ol
  • 2842-44-6
  • 42-44-6