1-Bromo-2-(2-methoxyethoxy)ethane
- Product Name
- 1-Bromo-2-(2-methoxyethoxy)ethane
- CAS No.
- 54149-17-6
- Chemical Name
- 1-Bromo-2-(2-methoxyethoxy)ethane
- Synonyms
- DK815;DKSI138;mPEG2-Br;DKFELEX0212;CAS_54149-17-6;Bromo-PEG2-methoxy;Methyl-PEG2-bromide;1-bromo-3,6-dioxaheptane;MONO METHOXY PEG BROMIDE;1-BROMO-(2-METHOXYETHOXY)ETHANE
- CBNumber
- CB2216300
- Molecular Formula
- C5H11BrO2
- Formula Weight
- 183.04
- MOL File
- 54149-17-6.mol
1-Bromo-2-(2-methoxyethoxy)ethane Property
- Boiling point:
- 156 °C (lit.) 37-40 °C/0.01 mmHg (lit.)
- Density
- 1.3600 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.455(lit.)
- Flash point:
- 163 °F
- storage temp.
- 2-8°C
- form
- Liquid
- color
- Clear colorless to pale yellow
- Water Solubility
- Not miscible in water.
- Sensitive
- Light Sensitive
- BRN
- 2069579
- InChI
- InChI=1S/C5H11BrO2/c1-7-4-5-8-3-2-6/h2-5H2,1H3
- InChIKey
- HUXJXNSHCKHFIL-UHFFFAOYSA-N
- SMILES
- C(OCCBr)COC
- CAS DataBase Reference
- 54149-17-6(CAS DataBase Reference)
- NIST Chemistry Reference
- 1-Bromo-2-(2-methoxyethoxy)ethane(54149-17-6)
N-Bromosuccinimide Price
- Product number
- 639842
- Product name
- 1-Bromo-2-(2-methoxyethoxy)ethane
- Purity
- 95%
- Packaging
- 10g
- Price
- $281
- Updated
- 2024/03/01
- Product number
- 456195
- Product name
- 1-Bromo-2-(2-methoxyethoxy)ethane
- Purity
- 90%
- Packaging
- 10g
- Price
- $99
- Updated
- 2024/03/01
- Product number
- B4736
- Product name
- 1-Bromo-2-(2-methoxyethoxy)ethane (stabilized with Na2CO3)
- Purity
- >90.0%(GC)
- Packaging
- 5g
- Price
- $48
- Updated
- 2024/03/01
- Product number
- B4736
- Product name
- 1-Bromo-2-(2-methoxyethoxy)ethane (stabilized with Na2CO3)
- Purity
- >90.0%(GC)
- Packaging
- 25g
- Price
- $185
- Updated
- 2024/03/01
- Product number
- L05406
- Product name
- 1-Bromo-2-(2-methoxyethoxy)ethane, tech. 90%, stab. with sodium carbonate
- Packaging
- 5g
- Price
- $55.65
- Updated
- 2024/03/01
1-Bromo-2-(2-methoxyethoxy)ethane Chemical Properties,Usage,Production
Chemical Properties
clear colorless to pale yellow liquid
Uses
1-Bromo-2-(2-methoxyethoxy)ethane is an important raw material and intermediate used in organic synthesis, pharmaceuticals, agrochemicals and dyestuff.
Synthesis
General Procedure for Preparation of 1-Bromo-2-(2-methoxyethoxy)ethane: Into a 25-mL round bottomed flask equipped with magnetic stir bar, addition funnel and positive flow of nitrogen were placed 15.60 mmol of a ethyleneglycol monomethyl ether. The solution was stirred for 15 min in an ice bath before the dropwise addition of phosphorous tribromide (7.81 mmol) over a 10 min period. The solution was allowed to gradually warm and stir at room temperature (rt) for 14 hrs. The solution was then heated in a 90 °C oil bath for 1 hr, at which time the solution turned yellow. The solution was allowed to cool to rt, poured onto 30 g of ice/water mixture, and made slightly basic with addition of a 10% solution of NaHCO3 (~6 mL). Subsequent extraction with diethyl ether (Et2O) (3 x 30 mL), followed by drying over MgSO4 and concentration under reduced pressure afforded a colorless oil in sufficient purity for use in subsequent reactions.
1-Bromo-2-(2-methoxyethoxy)ethane Preparation Products And Raw materials
Raw materials
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View Lastest Price from 1-Bromo-2-(2-methoxyethoxy)ethane manufacturers
- Product
- 1-Bromo-2-(2-methoxyethoxy)ethane 54149-17-6
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 30tons/month
- Release date
- 2023-02-21
- Product
- 1-Bromo-2-(2-methoxyethoxy)ethane 54149-17-6
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-11-10
- Product
- 1-Bromo-2-(2-methoxyethoxy)ethane 54149-17-6
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 1000KGS
- Release date
- 2019-12-20