3-(Acetylamino)-5-bromopyridine

Product Name: 3-(Acetylamino)-5-bromopyridine
CAS No.: 15862-46-1
Chemical Name: 3-(Acetylamino)-5-bromopyridine
Synonyms: N-(5-Bromopyridin-3-yl);N-(5-Bromo-3-pyridyl)acetamide;3-(Acetylamino)-5-bromopyridine;N-(5-bromopyridin-3-yl)acetamide;Acetamide, N-(5-bromo-3-pyridinyl)-
CBNumber: CB22194679
Molecular Formula: C7H7BrN2O
Formula Weight: 215.05
MOL File: 15862-46-1.mol

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3-(Acetylamino)-5-bromopyridine Property

storage temp.: Inert atmosphere,Room Temperature
Appearance: Light yellow to brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B704203
Product name: N-(5-Bromopyridin-3-yl)acetamide
Packaging: 10mg
Price: $45
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0369737
Product name: N-(5-BROMOPYRIDIN-3-YL)ACETAMIDE
Purity: 95.00%
Packaging: 5MG
Price: $502.67
Updated: 2021/12/16

AK Scientific

Product number: 2727AQ
Product name: N-(5-BROMOPYRIDIN-3-YL)ACETAMIDE
Packaging: 1g
Price: $503.6
Updated: 2021/12/16

Ambeed

Product number: A245568
Product name: N-(5-Bromopyridin-3-yl)acetamide
Purity: 95+%
Packaging: 250mg
Price: $52
Updated: 2021/12/16

Ambeed

Product number: A245568
Product name: N-(5-Bromopyridin-3-yl)acetamide
Purity: 95+%
Packaging: 1g
Price: $131
Updated: 2021/12/16

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3-(Acetylamino)-5-bromopyridine Chemical Properties,Usage,Production

Synthesis

13535-01-8

108-24-7

15862-46-1

To a solution of 3-amino-5-bromopyridine (1.0 g, 5.78 mmol) and pyridine (1.3 mL, 12.9 mmol) in dichloromethane (DCM, 5 mL) was added acetic anhydride (0.6 mL, 6.358 mmol) dropwise. The reaction mixture was stirred at room temperature for 17 hours. Upon completion of the reaction, the mixture was concentrated and the crude product was purified by normal-phase column chromatography with an elution gradient of 0-75% ethyl acetate (EtOAc)/heptane to afford N-(5-bromopyridin-3-yl)acetamide (1.18 g, 95% yield).

References

[1] Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014, vol. 53, # 1, p. 83 - 89
[2] Patent: US2014/323468, 2014, A1. Location in patent: Paragraph 0601
[3] Patent: CN103601745, 2017, B. Location in patent: Paragraph 0035; 0036
[4] Recueil des Travaux Chimiques des Pays-Bas, 1955, vol. 74, p. 1062,1068
[5] Journal fuer Praktische Chemie (Leipzig), 1933, vol. <2> 138, p. 244,257

3-(Acetylamino)-5-bromopyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(Acetylamino)-5-bromopyridine Suppliers

China 38 United States 2 Global 40

Tetranov Biopharm

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3-(Acetylamino)-5-bromopyridine

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15862-46-1