TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE

Product Name: TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE
CAS No.: 150008-24-5
Chemical Name: TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE
Synonyms: tert-Butyl 4-(hydroxyimino);1-Boc-4-(hydroxyimino)piperidine;N-BOC-4-(hydroxyimino)piperidine;tert-butyl 4-(hydroxyimino)piperidin-1-carboxylate;TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE;4-Hydroxyimino-piperidine-1-carboxylic acid tert-butyl ester;1-Piperidinecarboxylic acid, 4-(hydroxyiMino)-, 1,1-diMethylethyl ester
CBNumber: CB22464657
Molecular Formula: C10H18N2O3
Formula Weight: 214.26
MOL File: 150008-24-5.mol

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TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Off-white to yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B809913
Product name: tert-Butyl4-(hydroxyimino)piperidine-1-carboxylate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: W3277
Product name: tert-Butyl4-(hydroxyimino)piperidine-1-carboxylate
Packaging: 1g
Price: $70
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0385380
Product name: TERT-BUTYL-4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE
Purity: 95.00%
Packaging: 5MG
Price: $497.62
Updated: 2021/12/16

Ambeed

Product number: A467950
Product name: tert-Butyl4-(hydroxyimino)piperidine-1-carboxylate
Purity: 98%
Packaging: 1g
Price: $11
Updated: 2021/12/16

Acints

Product number: RH-12D-002
Product name: 4-Hydroxyimino-piperidine-1-carboxylicacidtert-butylester
Purity: 95%+
Packaging: 1g
Price: $14.5
Updated: 2021/12/16

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TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE Chemical Properties,Usage,Production

Uses

tert-Butyl 4-(hydroxyimino)piperidine-1-carboxylate is a useful intermediate for organic synthesis.

Synthesis

79099-07-3

150008-24-5

The general procedure for the synthesis of 4-oxime-1-Boc-piperidine using N-Boc-4-piperidone as starting material is as follows: 1 equiv. of N-Boc-4-piperidone, 1.6 equiv. of hydroxylamine hydrochloride, and 2.0 equiv. of sodium acetate were dissolved in an aqueous methanol solution, mixed homogeneously, and then heated to reflux the reaction. Upon completion of the reaction, the target product 4-oxime-1-Boc-piperidine was obtained in quantitative yield. The synthetic method was applicable for the preparation of all oxime substrates in this study.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2010, vol. 20, # 9, p. 2942 - 2945
[2] Tetrahedron Letters, 2010, vol. 51, # 24, p. 3216 - 3217
[3] Tetrahedron Letters, 2011, vol. 52, # 10, p. 1074 - 1077
[4] Patent: EP1477490, 2004, A1. Location in patent: Page 109
[5] Patent: WO2008/150447, 2008, A1. Location in patent: Page/Page column 206

TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE Suppliers

China 44 India 1 Switzerland 1 United States 7 Global 53

Pure Chemistry Scientific Inc.

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View Lastest Price from TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE manufacturers

Career Henan Chemical Co

Product: TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE 150008-24-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-08

150008-24-5, TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATERelated Search:

tert-Butyl 4-bromobutanoate TERT-BUTYL 4-CYANO-4-(PYRIDIN-2-YL)PIPERIDINE-1-CARBOXYLATE 5-BROMO-3-IODOINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER tert-butyl 3,8-diazabicyclo[3.2.1]octane-3-carboxylate tert-Butyl 2,6-dichloroisonicotinate tert-Butyl methacrylate tert-Butyl N-((2S,1S)-2-hydroxycyclohexyl)carbamate TERT-BUTYL 4-OXO-3,4-DIHYDROQUINOLINE-1(2H)-CARBOXYLATE tert-Butyl 4-(4-bromophenoxy)piperidine-1-carboxylate ethyl 4-(hydroxyimino)piperidine-1-carboxylate TERT-BUTYL 5-(HYDROXYIMINO)-2-AZABICYCLO[2.2.1]HEPTANE-2-CARBOXYLATE TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE

TERT-BUTYL 4-(HYDROXYIMINO)PIPERIDINE-1-CARBOXYLATE

1-Piperidinecarboxylic acid, 4-(hydroxyiMino)-, 1,1-diMethylethyl ester

1-Boc-4-(hydroxyimino)piperidine

tert-Butyl 4-(hydroxyimino)

N-BOC-4-(hydroxyimino)piperidine

4-Hydroxyimino-piperidine-1-carboxylic acid tert-butyl ester

tert-butyl 4-(hydroxyimino)piperidin-1-carboxylate

150008-24-5