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3-Hydroxy-4-methoxybenzyl alcohol

Product Name
3-Hydroxy-4-methoxybenzyl alcohol
CAS No.
4383-06-6
Chemical Name
3-Hydroxy-4-methoxybenzyl alcohol
Synonyms
5-(Hydroxymethyl)-2-methoxyphenol;RARECHEM AL BD 0068;ISOVANILLYL ALCOHOL;3-Hydroxy-4-methoxyb;IsovanillylAlcohol>2-methoxy-5-methylol-phenol;2-methyl-1-phenylprop-2-en-1-ol;3-HYDROXY-4-METHOXYBENZYL ALCOHOL;2-Methoxy-5-(hydroxymethyl)phenol;3-Hydroxy-4-methoxybenzenemethanol
CBNumber
CB2279536
Molecular Formula
C8H10O3
Formula Weight
154.16
MOL File
4383-06-6.mol
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3-Hydroxy-4-methoxybenzyl alcohol Property

Melting point:
135-137 °C (lit.)
Boiling point:
315.8±27.0 °C(Predicted)
Density 
1.226±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
solubility 
soluble in Methanol
form 
powder to crystal
pka
9.75±0.10(Predicted)
color 
White to Almost white
BRN 
1867860
CAS DataBase Reference
4383-06-6(CAS DataBase Reference)
NIST Chemistry Reference
3-Hydroxy-4-methoxybenzyl alcohol(4383-06-6)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
22-24/25-36-26
WGK Germany 
3
HS Code 
29094990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
188433
Product name
3-Hydroxy-4-methoxybenzyl alcohol
Purity
98%
Packaging
10g
Price
$113
Updated
2024/03/01
TCI Chemical
Product number
I0648
Product name
Isovanillyl Alcohol
Purity
>98.0%(GC)
Packaging
5g
Price
$16
Updated
2024/03/01
Alfa Aesar
Product number
A14786
Product name
3-Hydroxy-4-methoxybenzyl alcohol, 98%
Packaging
50g
Price
$135
Updated
2023/06/20
Alfa Aesar
Product number
A14786
Product name
3-Hydroxy-4-methoxybenzyl alcohol, 98%
Packaging
10g
Price
$37.3
Updated
2021/12/16
Matrix Scientific
Product number
075345
Product name
3-Hydroxy-4-methoxybenzyl alcohol
Purity
95+%
Packaging
100g
Price
$68
Updated
2021/12/16
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3-Hydroxy-4-methoxybenzyl alcohol Chemical Properties,Usage,Production

Chemical Properties

White crystalline

Uses

3-Hydroxy-4-methoxybenzyl alcohol was used in preparation of 2-hydroxymethyl-5-methoxy-2,5-cyclohexadiene-1,4-dione by oxidation with Fremy′s salt.

Synthesis

3-Hydroxy-4-methoxybenzyl alcohol is synthesised using isovanillin as raw material by chemical reaction. The specific synthesis steps are as follows:
In a round-bottom flask equipped with magnetic stirrer was added 15 sodium borohydride (0.2mmol; 0.01g) to the solution of 9 1 (0.2mmol; 0.03g) prepared in ethanol (1mL). The mixture was stirred at room temperature for 30min. The consumption of all starting material was detected by thin layer chromatography (TLC); the solvent was evaporated under reduced pressure. Subsequently, 10mL of saturated NaCl solution was added and then extracted with ethyl acetate (3×10mL). The organic phase was dried over anhydrous MgSO4, filtered and evaporated, providing 0.03g of colorless oil, 90% yield of 3-Hydroxy-4-methoxybenzyl alcohol.

3-Hydroxy-4-methoxybenzyl alcohol Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Hydroxy-4-methoxybenzyl alcohol Suppliers

UkrOrgSynthesis Ltd.
Tel
--
Fax
--
Email
y.barysheva@ukrorgsynth.com
Country
Ukraine
ProdList
6230
Advantage
38
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View Lastest Price from 3-Hydroxy-4-methoxybenzyl alcohol manufacturers

Career Henan Chemical Co
Product
3-Hydroxy-4-methoxybenzyl alcohol 4383-06-6
Price
US $1.00/kg
Min. Order
1kg
Purity
95%-99%
Supply Ability
as request
Release date
2018-12-24

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