preparation
ChemicalBook > CAS DataBase List > 4-Fluorobenzhydrazide

4-Fluorobenzhydrazide

preparation
Product Name
4-Fluorobenzhydrazide
CAS No.
456-06-4
Chemical Name
4-Fluorobenzhydrazide
Synonyms
YTO*;AKOS B020279;ASISCHEM R36621;AKOS BBS-00004506;BUTTPARK 35\03-73;TIMTEC-BB SBB002375;4-FLUOROBENZHYDRAZIDE;p-Fluorobenzhydrazide;4-fluorobenzohydrazide;4-fluoroenzoylhydrazide
CBNumber
CB2281902
Molecular Formula
C7H7FN2O
Formula Weight
154.14
MOL File
456-06-4.mol
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4-Fluorobenzhydrazide Property

Melting point:
162-166 °C (lit.)
Density 
1.272±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
Soluble in methanol.
form 
Crystalline Powder
pka
12.17±0.10(Predicted)
color 
Orange to light brown
CAS DataBase Reference
456-06-4(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
RTECS 
DH1310000
HazardClass 
IRRITANT
HS Code 
29280000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
536334
Product name
4-Fluorobenzoic hydrazide
Purity
96%
Packaging
5g
Price
$51.5
Updated
2024/03/01
TCI Chemical
Product number
F0540
Product name
4-Fluorobenzohydrazide
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$127
Updated
2024/03/01
TCI Chemical
Product number
F0540
Product name
4-Fluorobenzohydrazide
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$470
Updated
2024/03/01
Alfa Aesar
Product number
H53496
Product name
4-Fluorobenzhydrazide, 97%
Packaging
5g
Price
$48.65
Updated
2024/03/01
Alfa Aesar
Product number
H53496
Product name
4-Fluorobenzhydrazide, 97%
Packaging
25g
Price
$154.65
Updated
2024/03/01
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4-Fluorobenzhydrazide Chemical Properties,Usage,Production

preparation

The synthesized ester (12.5ml) was taken into a round  bottom flask (250ml), 50ml of absolute ethanol &  37.5ml of hydrazine hydrate was added in the flask.  The ester, ethanol & hydrazine hydrate for the synthesis of hydrazide must be in following ratio: Ester: Absolute ethanol: Hydrazine hydrate 1 : 4 : 3  Then round bottom flask was covered with aluminium  foil, placed on hot plate & allowed to stir it for almost  12-15 hrs. As the solid product appeared, reaction  completion was checked by performing TLC using n-hexane, ethyl acetate & TLC cards & observed under  UV lamp. After completion of reaction n-hexane was added.  Solution filtered as needle like crystals appeared.  Allowed it to dry & a shiny off white product was  obtained that was hydrazide & product was calculated  (79%).

Chemical Properties

White solid

Uses

Used in the stnthesis of fluorinated poly (1, 3, 4-oxadiazole-ether-imide). N-(3,5-dinitrobenzoyl)-N?-(4-fluorobenzoyl)-hydrazine with 4-Fluorobenzhydrazide as solvent in NMP.

4-Fluorobenzhydrazide Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Fluorobenzhydrazide Suppliers

TCI AMERICA
Tel
800-4238616
Fax
+1-888-520-1075 / +1-503-283-1987
Email
sales@tciamerica.com
Country
Americas
ProdList
23653
Advantage
75
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View Lastest Price from 4-Fluorobenzhydrazide manufacturers

Career Henan Chemical Co
Product
4-Fluorobenzhydrazide 456-06-4
Price
US $1.00/KG
Min. Order
1G
Purity
99%
Supply Ability
100KG
Release date
2018-08-13

456-06-4, 4-FluorobenzhydrazideRelated Search:


  • ASISCHEM R36621
  • BUTTPARK 35\03-73
  • 4-FLUOROBENZENECARBOHYDRAZIDE
  • 4-FLUOROBENZOYLHYDRAZINE HYDRATE
  • 4-FLUOROBENZHYDRAZIDE
  • 4-FLUOROBENZOHYDRAZIDE HYDRATE
  • 4-FLUOROBENZOIC HYDRAZIDE
  • 4-FLUOROBENZOIC HYDRAZIDE HYDRATE
  • AKOS BBS-00004506
  • AKOS B020279
  • TIMTEC-BB SBB002375
  • (p-fluorobenzoyl)-hydrazin
  • 4-fluoro-benzoicacihydrazide
  • p-fluorobenzoicacidhydrazide
  • p-fluoro-benzoicacihydrazide
  • 4-FluoroBenzoylHyhrazine
  • 4-fluorobenzohydrazide
  • YTO*
  • 4-Fluorobenzhydrazide98%
  • 4-fluoroenzoylhydrazide
  • 4-Fluoro-benzoic acid hydrazide
  • hydrazide 4-fluoro-Benzoic acid
  • p-Fluorobenzhydrazide
  • 4-Fluorobenzoic acid hydrazidedisc same as 6190 9/01
  • 4-Fluorobenzoic acid hydrazide 98%
  • 4-Fluorobenzoic Hydrazide 4-Fluorobenzoylhydrazine
  • 4-Fluorobenzohydrazide, 4-Fluorobenzenecarbohydrazide
  • 4-Fluorobenzoic hydrazide 96%
  • 4-Fluorobenzohydrazide&gt
  • Benzoic acid, 4-fluoro-, hydrazide
  • 456-06-4
  • C7H7FN2OxH2O
  • Building Blocks
  • Carbonyl Compounds
  • Hydrazides
  • Organic Building Blocks
  • Fluorine Compounds
  • Phenyls & Phenyl-Het
  • Carbonyl Compounds
  • Hydrazides
  • Organic Building Blocks
  • Phenyls & Phenyl-Het
  • Benzenes
  • Fluorobenzene