ChemicalBook > CAS DataBase List > 2-IODO-5-NITROANISOLE

2-IODO-5-NITROANISOLE

Uses

Product Name: 2-IODO-5-NITROANISOLE
CAS No.: 5458-84-4
Chemical Name: 2-IODO-5-NITROANISOLE
Synonyms: 2-IODO-5-NITROANISOLE;2-IODO-5-NITROANISOLE 97%;2-iodo-5-nitrobenzyl ether;4-Iodo-3-methoxynitrobenzene;I-Iodo-2-Methoxy-4-nitrobenzene;1-Iodo-2-methoxy-4-nitrobenzene;Benzene, 1-iodo-2-methoxy-4-nitro-;2-Iodo-5-nitroanisole【4-Iodo-3-methoxynitrobenzene】;4-Iodo-3-Methoxynitrobenzene[2-Iodo-5-nitroanisole]
CBNumber: CB2321488
Molecular Formula: C7H6INO3
Formula Weight: 279.03
MOL File: 5458-84-4.mol

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2-IODO-5-NITROANISOLE Property

Melting point:: 128-130°C
Boiling point:: 341.2±32.0 °C(Predicted)
Density: 1.893±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
Appearance: White to light brown Solid
CAS DataBase Reference: 5458-84-4(CAS DataBase Reference)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HS Code: 29093090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S362824
Product name: 2-IODO-5-NITROANISOLE
Purity: Aldrich<sup>CPR</sup>
Packaging: 1 unit
Price: $185
Updated: 2025/07/31

Sigma-Aldrich

Product number: S362824
Product name: 2-IODO-5-NITROANISOLE
Purity: Aldrich
Packaging: 250mg
Price: $179
Updated: 2024/03/01

TRC

Product number: I737043
Product name: 2-Iodo-5-nitroanisole
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: I737043
Product name: 2-Iodo-5-nitroanisole
Packaging: 500mg
Price: $75
Updated: 2021/12/16

Oakwood

Product number: 149002
Product name: 2-Iodo-5-nitroanisole
Purity: 97%
Packaging: 1g
Price: $9
Updated: 2021/12/16

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2-IODO-5-NITROANISOLE Chemical Properties,Usage,Production

Uses

2-Iodo-5-nitrobenzyl ether is a useful research chemical for organic synthesis and other chemical processes.

Synthesis

97-52-9

5458-84-4

General procedure for the synthesis of 2-iodo-5-nitroanisole from 2-methoxy-4-nitroaniline: Potassium iodide (5.0 mmol) and sodium nitrite (3.0 mmol) were sequentially added to an acetic acid solution (30 mL) containing 2-methoxy-4-nitroaniline (2.5 mmol) and camphorsulphonic acid (3.0 mmol) at room temperature. The reaction mixture was stirred continuously for 24 h, during which nitrogen release was observed. Upon completion of the reaction, the reaction endpoint was confirmed by β-naphthol test and thin layer chromatography (TLC), followed by removal of solvent using a rotary evaporator. The resulting solid was washed with water and extracted with dichloromethane (CH2Cl2). The extract was dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure to remove the solvent. Finally, the product was purified by column chromatography, and the eluting solvent was a mixed system of hexane/dichloromethane. The physical properties and 1H NMR spectral data of the obtained product were consistent with the commercially available analytically pure sample.

References

[1] Tetrahedron, 2013, vol. 69, # 16, p. 3511 - 3517
[2] Chemical and Pharmaceutical Bulletin, 2014, vol. 62, # 10, p. 979 - 988
[3] Journal of Medicinal Chemistry, 2009, vol. 52, # 15, p. 4869 - 4882
[4] Chem. Zentralbl., 1901, vol. 72, # I, p. 739
[5] Privatmitteilung,

2-IODO-5-NITROANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-IODO-5-NITROANISOLE Suppliers

China 112 France 1 Germany 1 India 5 United Kingdom 6 United States 17 Global 142

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View Lastest Price from 2-IODO-5-NITROANISOLE manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 2-IODO-5-NITROANISOLE 5458-84-4
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-11-26

Career Henan Chemical Co

Product: 1-Iodo-2-methoxy-4-nitrobenzene 5458-84-4
Price: US $8.00/KG
Min. Order: 1KG
Purity: ≥98%
Supply Ability: kg--ton
Release date: 2020-03-08

Career Henan Chemical Co

Product: 2-IODO-5-NITROANISOLE 5458-84-4
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

5458-84-4, 2-IODO-5-NITROANISOLERelated Search:

2-(2'-BROMOPHENOXY)PROPANE 2-IODO-5-NITROTOLUENE Anisole 4-IODO-3-NITROANISOLE,4-Iodo-3-Nitroanisole 3-Nitro-4-Iodoanisole,4-IODO-3-NITROANISOLE, 98+% 3-IODO-4-NITROANISOLE 2-IODO-4-NITROANISOLE 2-Iodo-3-nitroanisole 4-IODO-2-NITROANISOLE 2-IODO-5-NITROPHENOL 2-IODO-5-NITROANISOLE iodoanisole 1-Iodo-4-nitrobenzene

2-IODO-5-NITROANISOLE

2-IODO-5-NITROANISOLE 97%

4-Iodo-3-methoxynitrobenzene

1-Iodo-2-methoxy-4-nitrobenzene

I-Iodo-2-Methoxy-4-nitrobenzene

4-Iodo-3-Methoxynitrobenzene[2-Iodo-5-nitroanisole]

2-Iodo-5-nitroanisole【4-Iodo-3-methoxynitrobenzene】

Benzene, 1-iodo-2-methoxy-4-nitro-

2-iodo-5-nitrobenzyl ether

5458-84-4

HALOGEN

Anisoles, Alkyloxy Compounds & Phenylacetates

Iodine Compounds

Nitro Compounds

Anisole