ChemicalBook > CAS DataBase List > 4-IODO-3-NITROANISOLE

4-IODO-3-NITROANISOLE

Product Name
4-IODO-3-NITROANISOLE
CAS No.
58755-70-7
Chemical Name
4-IODO-3-NITROANISOLE
Synonyms
NSC 158572;3-Nitro-4-iodoanisol;3-Nitro-4-Iodoanisole;4-IODO-3-NITROANISOLE;4-Iodo-3-nitrianisole;4-IODO-3-NITROANISOLE, 98+%;1-IODO-4-METHOXY-2-NITROBENZENE;4-Iodo-3-nitrophenyl Methyl Ether;Benzene, 1-iodo-4-Methoxy-2-nitro-;4-Iodo-3-Nitroanisole 3-Nitro-4-Iodoanisole
CBNumber
CB8729947
Molecular Formula
C7H6INO3
Formula Weight
279.03
MOL File
58755-70-7.mol
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4-IODO-3-NITROANISOLE Property

Melting point:
61-62°C
Boiling point:
173 °C(Press: 0.9 Torr)
Density 
1.893
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
form 
solid
color 
Light brown to brown
Sensitive 
Light Sensitive
BRN 
2365592
CAS DataBase Reference
58755-70-7(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36/37/39-37
HazardClass 
IRRITANT, LIGHT SENSITIVE
HS Code 
29093090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
S544981
Product name
4-IODO-3-NITROANISOLE
Purity
Aldrich<sup>CPR</sup>
Packaging
1 unit
Price
$185
Updated
2025/07/31
Sigma-Aldrich
Product number
S544981
Product name
4-IODO-3-NITROANISOLE
Purity
Aldrich
Packaging
1g
Price
$179
Updated
2024/03/01
TCI Chemical
Product number
I1136
Product name
1-Iodo-4-methoxy-2-nitrobenzene
Purity
min. 98.0 %
Packaging
5G
Price
$41
Updated
2025/07/31
TCI Chemical
Product number
I1136
Product name
1-Iodo-4-methoxy-2-nitrobenzene
Purity
min. 98.0 %
Packaging
25G
Price
$123
Updated
2025/07/31
TRC
Product number
I737050
Product name
4-Iodo-3-nitroanisole
Packaging
100mg
Price
$60
Updated
2021/12/16
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4-IODO-3-NITROANISOLE Chemical Properties,Usage,Production

Synthesis

96-96-8

58755-70-7

General procedure for the synthesis of 4-iodo-3-nitroanisole from 2-nitro-4-methoxyaniline: 11.9 mmol of 2-nitro-4-methoxyaniline was dissolved in 20 mL of concentrated sulfuric acid at a mass concentration of 71%. The temperature of the system was lowered to -5°C. 10 mL of 2 mol/L sodium nitrite solution was rapidly added to the reaction system at 0 °C and under vigorous stirring. The reaction was kept at 0°C for 10 minutes. Subsequently, the reaction mixture was poured into 5 mL of 4 mol/L sodium iodide solution at 0 °C and the reaction was continued for 30 min. Upon completion of the reaction, the solid residue was collected by filtration and washed sequentially with 6N hydrochloric acid and water. The crude product was recrystallized by hexane to give a yellow solid A.

References

[1] Patent: CN105669525, 2016, A. Location in patent: Paragraph 0072; 0073; 0082
[2] Synlett, 2016, vol. 27, # 14, p. 2095 - 2100
[3] Synlett, 2005, # 16, p. 2469 - 2472
[4] Journal of Organic Chemistry, 2001, vol. 66, # 13, p. 4525 - 4542
[5] Angewandte Chemie - International Edition, 2011, vol. 50, # 32, p. 7354 - 7358

4-IODO-3-NITROANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-IODO-3-NITROANISOLE Suppliers

J & K SCIENTIFIC LTD.
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18210857532; 18210857532
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86-10-82849933
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jkinfo@jkchemical.com
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China
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Alfa Aesar
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400-6106006
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021-67582001/03/05
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saleschina@alfa-asia.com
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Beijing Ouhe Technology Co., Ltd
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010-010-82967028 13522913783
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+86-10-82967029
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Shanghai Longsheng chemical Co.,Ltd.
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ChangZhou SIDU chemical Co., Ltd.
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siduchem@hotmail.com
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T&W GROUP
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contact@trustwe.com
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View Lastest Price from 4-IODO-3-NITROANISOLE manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
4-IODO-3-NITROANISOLE 58755-70-7
Price
US $0.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
10000KGS
Release date
2025-04-02

58755-70-7, 4-IODO-3-NITROANISOLERelated Search:


  • 1-IODO-4-METHOXY-2-NITROBENZENE
  • 4-IODO-3-NITROANISOLE
  • 4-Iodo-3-Nitroanisole 3-Nitro-4-Iodoanisole
  • 3-Nitro-4-iodoanisol
  • 3-Nitro-4-Iodoanisole
  • 4-IODO-3-NITROANISOLE, 98+%
  • 4-Iodo-3-nitrianisole
  • NSC 158572
  • Benzene, 1-iodo-4-Methoxy-2-nitro-
  • 4-Iodo-3-nitrophenyl Methyl Ether
  • 58755-70-7
  • HALOGEN
  • Aromatic Ethers