4-Iodoanisole
Description References- Product Name
- 4-Iodoanisole
- CAS No.
- 696-62-8
- Chemical Name
- 4-Iodoanisole
- Synonyms
- 1-IODO-4-METHOXYBENZENE;P-IODOANISOLE;4-IODOANISOL;Isoform;p-iodoanisol;4-IODANISOLE;4-lodoanisole;4-METHOXYIODOBENZENE;CREM-α;4-iodoether
- CBNumber
- CB6450614
- Molecular Formula
- C7H7IO
- Formula Weight
- 234.03
- MOL File
- 696-62-8.mol
4-Iodoanisole Property
- Melting point:
- 50-53 °C(lit.)
- Boiling point:
- 237 °C726 mm Hg(lit.)
- Density
- 1.7904 (estimate)
- Flash point:
- >230 °F
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- Soluble in ethanol, ether, chloroform.
- form
- Crystalline Powder and Chunks
- color
- Off-white to brown
- Sensitive
- Light Sensitive
- BRN
- 1906692
- InChIKey
- SYSZENVIJHPFNL-UHFFFAOYSA-N
- CAS DataBase Reference
- 696-62-8(CAS DataBase Reference)
- NIST Chemistry Reference
- Benzene, 1-iodo-4-methoxy-(696-62-8)
- EPA Substance Registry System
- Benzene, 1-iodo-4-methoxy- (696-62-8)
Safety
- Hazard Codes
- Xi,Xn
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36-24/25
- WGK Germany
- 3
- F
- 8
- TSCA
- Yes
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- I7608
- Product name
- 4-Iodoanisole
- Purity
- 98%
- Packaging
- 25g
- Price
- $46.8
- Updated
- 2024/03/01
- Product number
- I7608
- Product name
- 4-Iodoanisole
- Purity
- 98%
- Packaging
- 100g
- Price
- $140
- Updated
- 2024/03/01
- Product number
- I0378
- Product name
- 4-Iodoanisole
- Purity
- >99.0%(GC)
- Packaging
- 25g
- Price
- $30
- Updated
- 2024/03/01
- Product number
- I0378
- Product name
- 4-Iodoanisole
- Purity
- >99.0%(GC)
- Packaging
- 100g
- Price
- $82
- Updated
- 2024/03/01
- Product number
- A12144
- Product name
- 4-Iodoanisole, 98+%
- Packaging
- 25g
- Price
- $34.1
- Updated
- 2024/03/01
4-Iodoanisole Chemical Properties,Usage,Production
Description
4-Iodoanisole (chemical formula: C7H7IO) is an organic compound being soluble in ethanol, ether and chloroform. It has a wide range of medicals industrial applications. For example, it can be used as human and animal nutrition products, antiseptics, disinfectants, pharmaceutical intermediates, polarizing films for liquid crystal display (LCD) chemicals. Its iodine derivatives can also be used as organic building blocks and analytic reagents.
References
https://www.fishersci.pt/shop/products/4-iodoanisole-98-7/11480113
Chemical Properties
off-white to brown crystalline powder and chunks. Melting point 51-52 ℃, boiling point 237 ℃ (96.8kPa). Soluble in organic solvents such as alcohol and ether, but insoluble in water. Iodine can be easily separated and analyzed by light.
Uses
4-Iodoanisole is used in wide range of medicals industrial applications as well as in human and animal nutrition products, pharmaceutical intermediates, polarizing films for Liquid Crystal Display (LCD) chemicals. Iodine derivatives are also used as organic building blocks, analytical reagents.
Preparation
4-Iodoanisole is synthesized by the reaction of anisole with iodine chloride. Add anisole to glacial acetic acid, stir and slowly add iodine chloride. After the addition was completed, the temperature was refluxed for 3.5h. Cool, pour into ice water, and precipitate p-iodoanisole. After it was separated, the free iodine was washed with 5% sodium sulfite, then washed with water, distilled under reduced pressure, and the fractions with a boiling point of 140-160 °C (5.33 kPa) were collected and cooled to 0 °C for filtration. Wash with methanol and recrystallize to obtain the finished product.
Definition
ChEBI: (alpha-D-mannosyl)7-beta-D-mannosyl-diacetylchitobiosyl-L-asparagine, isoform B (protein) is a member of methoxybenzenes.
Synthesis Reference(s)
The Journal of Organic Chemistry, 58, p. 2058, 1993 DOI: 10.1021/jo00060a020
Tetrahedron Letters, 27, p. 3497, 1986 DOI: 10.1016/S0040-4039(00)84832-7
Purification Methods
Crystallise 4-iodoanisole from aqueous EtOH and/or distil it under vacuum. [Beilstein 6 H 208, 6 I 109, 6 II 199, 6 III 744, 6 IV 1075.]
4-Iodoanisole Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-Iodoanisole manufacturers
- Product
- 4-Iodoanisole 696-62-8
- Price
- US $100.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-24
- Product
- 4-Iodoanisole 696-62-8
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 50000KG/month
- Release date
- 2023-09-06
- Product
- 4-Iodoanisole 696-62-8
- Price
- US $10.00/PCS
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2021-03-10