4-Iodoanisole

ChemicalBook > CAS DataBase List > 4-Iodoanisole

Description References

Product Name: 4-Iodoanisole
CAS No.: 696-62-8
Chemical Name: 4-Iodoanisole
Synonyms: 1-IODO-4-METHOXYBENZENE;P-IODOANISOLE;4-IODOANISOL;Isoform;p-iodoanisol;4-IODANISOLE;4-lodoanisole;4-METHOXYIODOBENZENE;CREM-α;4-iodoether
CBNumber: CB6450614
Molecular Formula: C7H7IO
Formula Weight: 234.03
MOL File: 696-62-8.mol

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4-Iodoanisole Property

Melting point:: 50-53 °C(lit.)
Boiling point:: 237 °C726 mm Hg(lit.)
Density: 1.7904 (estimate)
Flash point:: >230 °F
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: Soluble in ethanol, ether, chloroform.
form: Crystalline Powder and Chunks
color: Off-white to brown
Sensitive: Light Sensitive
BRN: 1906692
InChIKey: SYSZENVIJHPFNL-UHFFFAOYSA-N
CAS DataBase Reference: 696-62-8(CAS DataBase Reference)
NIST Chemistry Reference: Benzene, 1-iodo-4-methoxy-(696-62-8)
EPA Substance Registry System: Benzene, 1-iodo-4-methoxy- (696-62-8)

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 36/37/38
Safety Statements: 26-36-24/25
WGK Germany: 3
F: 8
TSCA: Yes
HS Code: 29093090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: I7608
Product name: 4-Iodoanisole
Purity: 98%
Packaging: 25g
Price: $46.8
Updated: 2024/03/01

Sigma-Aldrich

Product number: I7608
Product name: 4-Iodoanisole
Purity: 98%
Packaging: 100g
Price: $140
Updated: 2024/03/01

TCI Chemical

Product number: I0378
Product name: 4-Iodoanisole
Purity: >99.0%(GC)
Packaging: 25g
Price: $30
Updated: 2024/03/01

TCI Chemical

Product number: I0378
Product name: 4-Iodoanisole
Purity: >99.0%(GC)
Packaging: 100g
Price: $82
Updated: 2024/03/01

Alfa Aesar

Product number: A12144
Product name: 4-Iodoanisole, 98+%
Packaging: 25g
Price: $34.1
Updated: 2024/03/01

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4-Iodoanisole Chemical Properties,Usage,Production

Description

4-Iodoanisole (chemical formula: C7H7IO) is an organic compound being soluble in ethanol, ether and chloroform. It has a wide range of medicals industrial applications. For example, it can be used as human and animal nutrition products, antiseptics, disinfectants, pharmaceutical intermediates, polarizing films for liquid crystal display (LCD) chemicals. Its iodine derivatives can also be used as organic building blocks and analytic reagents.

References

https://www.fishersci.pt/shop/products/4-iodoanisole-98-7/11480113

Chemical Properties

off-white to brown crystalline powder and chunks. Melting point 51-52 ℃, boiling point 237 ℃ (96.8kPa). Soluble in organic solvents such as alcohol and ether, but insoluble in water. Iodine can be easily separated and analyzed by light.

Uses

4-Iodoanisole is used in wide range of medicals industrial applications as well as in human and animal nutrition products, pharmaceutical intermediates, polarizing films for Liquid Crystal Display (LCD) chemicals. Iodine derivatives are also used as organic building blocks, analytical reagents.

Preparation

4-Iodoanisole is synthesized by the reaction of anisole with iodine chloride. Add anisole to glacial acetic acid, stir and slowly add iodine chloride. After the addition was completed, the temperature was refluxed for 3.5h. Cool, pour into ice water, and precipitate p-iodoanisole. After it was separated, the free iodine was washed with 5% sodium sulfite, then washed with water, distilled under reduced pressure, and the fractions with a boiling point of 140-160 °C (5.33 kPa) were collected and cooled to 0 °C for filtration. Wash with methanol and recrystallize to obtain the finished product.

Definition

ChEBI: (alpha-D-mannosyl)7-beta-D-mannosyl-diacetylchitobiosyl-L-asparagine, isoform B (protein) is a member of methoxybenzenes.

Synthesis Reference(s)

The Journal of Organic Chemistry, 58, p. 2058, 1993 DOI: 10.1021/jo00060a020
Tetrahedron Letters, 27, p. 3497, 1986 DOI: 10.1016/S0040-4039(00)84832-7

Purification Methods

Crystallise 4-iodoanisole from aqueous EtOH and/or distil it under vacuum. [Beilstein 6 H 208, 6 I 109, 6 II 199, 6 III 744, 6 IV 1075.]

4-Iodoanisole Preparation Products And Raw materials

Raw materials

Sodium sulfite Iodine monochloride Dimethyl ether

Preparation Products

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View Lastest Price from 4-Iodoanisole manufacturers

Hebei Mujin Biotechnology Co.,Ltd

Product: 4-Iodoanisole 696-62-8
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50000KG/month
Release date: 2023-09-06

Hebei Weibang Biotechnology Co., Ltd

Product: 4-Iodoanisole 696-62-8
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2024-11-01

R&D Scientific Inc.

Product: 4-Iodoanisole 696-62-8
Price: US $397.00/Kg
Min. Order: 1Kg
Purity: 98
Supply Ability: 500 Kg
Release date: 2024-05-12

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ETHER

Ethers

Organic Building Blocks

Oxygen Compounds

Building Blocks

Pyridines ,Halogenated Heterocycles

Building Blocks

C2 to C8

Chemical Synthesis

Ethers

Organic Building Blocks

Oxygen Compounds