2-IODO-5-METHOXYANILINE

Product Name: 2-IODO-5-METHOXYANILINE
CAS No.: 153898-63-6
Chemical Name: 2-IODO-5-METHOXYANILINE
Synonyms: 2-IODO-5-METHOXYANILINE;2-Iodo-5-methoxybenzenamine;2-Iodo-5-methoxy-phenylamine;BenzenaMine, 2-iodo-5-Methoxy-;1H-Pyrazol-5-amine,1-(3-methylethyl)-
CBNumber: CB4130950
Molecular Formula: C7H8INO
Formula Weight: 249.05
MOL File: 153898-63-6.mol

More

Less

2-IODO-5-METHOXYANILINE Property

Melting point:: 33-36 °C(Solv: ethyl acetate (141-78-6))
Boiling point:: 298.4±30.0 °C(Predicted)
Density: 1.807±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka: 2.11±0.10(Predicted)
Appearance: White to light brown Solid
InChI: InChI=1S/C7H8INO/c1-10-5-2-3-6(8)7(9)4-5/h2-4H,9H2,1H3
InChIKey: CYDBBGSUZRDOPE-UHFFFAOYSA-N
SMILES: C1(N)=CC(OC)=CC=C1I

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: I708655
Product name: 2-Iodo-5-methoxyaniline
Packaging: 50mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: W3349
Product name: 2-Iodo-5-methoxyaniline
Packaging: 5g
Price: $444
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049825
Product name: 2-IODO-5-METHOXYANILINE
Purity: 95.00%
Packaging: 1G
Price: $852.55
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049825
Product name: 2-IODO-5-METHOXYANILINE
Purity: 95.00%
Packaging: 2.5G
Price: $1227.82
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049825
Product name: 2-IODO-5-METHOXYANILINE
Purity: 95.00%
Packaging: 5G
Price: $1548.26
Updated: 2021/12/16

More

Less

2-IODO-5-METHOXYANILINE Chemical Properties,Usage,Production

Synthesis

58755-70-7

153898-63-6

General procedure for the synthesis of 2-iodo-5-methoxyaniline from 4-iodo-3-nitroanisole: To a 100 mL methanol solution of 4-iodo-3-nitroanisole (5 g, 17.9 mmol) was added FeCl3 (50 mg, 0.3 mmol) and activated carbon (40 mg). The mixture was heated to reflux and hydrazine hydrate (1.75 g, 35 mmol) was added slowly and dropwise. After keeping the reaction at reflux for 8 h, it was cooled to room temperature and the reaction mixture was filtered through diatomaceous earth. The filtrate was concentrated and purified by column chromatography (eluent: hexane solution of 10% ethyl acetate) to afford 4.05 g of the target product 2-iodo-5-methoxyaniline as a light yellow oil (91% yield).1H NMR (300 MHz, CDCl3) δ 7.47 (1H, d, J = 8.7 Hz), 6.31 (1H, d, J = 2.8 Hz), 6.13 (1H, d, J = 2.8 Hz) 6.13 (1H, dd, J = 2.8, 8.7 Hz), 3.73 (3H, s).

References

[1] Angewandte Chemie - International Edition, 2011, vol. 50, # 32, p. 7354 - 7358
[2] Journal of Organic Chemistry, 2001, vol. 66, # 13, p. 4525 - 4542
[3] Patent: WO2003/106462, 2003, A1. Location in patent: Page 110
[4] Tetrahedron Letters, 2008, vol. 49, # 2, p. 363 - 366
[5] Angewandte Chemie - International Edition, 2010, vol. 49, # 48, p. 9262 - 9265

2-IODO-5-METHOXYANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

2-IODO-5-METHOXYANILINE Suppliers

China 89 Germany 1 India 3 United States 7 Global 100

Shanghai Titan Enterprise Development Co., Ltd

Tel: 16621224781
Email: syy@titansci.com
Country: China
ProdList: 2896
Advantage: 58

Adamas Reagent, Ltd.

Tel: 400-6009262 16621234537
Fax: 021-64823266
Email: chenyj@titansci.com
Country: China
ProdList: 14101
Advantage: 59

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

Shanghai yirong biology science and technology co., ltd

Tel: 18049974220
Fax: +86 (21) 51062076
Email: 3060526242@qq.com
Country: China
ProdList: 995
Advantage: 60

Chengdu HappySyn Pharmaceutical Technology Co., Ltd.

Tel: 028-85114309 18982182443
Email: yangli@happysyn.com
Country: China
ProdList: 2150
Advantage: 55

Hangzhou Sage Chemical Co., Ltd.

Tel: +86057186818502 13588463833
Fax: Pls mail us for more information!
Email: info@sagechem.com
Country: China
ProdList: 10266
Advantage: 58

Nanjing JinruiJiuAn Biotechnology Co., Ltd.

Tel: 025-58196018 800028039
Fax: 025-83453306
Email: sales@fartop.net
Country: China
ProdList: 2229
Advantage: 55

NovoChemy Ltd.

Tel: 021-31261262/ 49 (0)17662837245
Fax: (0)21-33250524
Email: sales@novochemy.com
Country: Germany
ProdList: 6328
Advantage: 58

Shanghai Topbiochem Technology Co., Ltd

Tel: 021-58170097
Email: info@topbiochem.com
Country: China
ProdList: 9510
Advantage: 58

More

Less

View Lastest Price from 2-IODO-5-METHOXYANILINE manufacturers

Career Henan Chemical Co

Product: 2-IODO-5-METHOXYANILINE 153898-63-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 200kgs
Release date: 2020-01-28

153898-63-6, 2-IODO-5-METHOXYANILINERelated Search:

3-Methoxy-2-methylaniline Butanoic acid, 4-oxo-4-(propyl(2,4,6-triiodo-3-methoxyphenyl)amino)- ( 9CI) 2-NITRO-4-(TRIFLUOROMETHOXY)IODOBENZENE 2,2-DIFLUORO-5-AMINO-6-IODO-1,3-BENZODIOXOLE Iolixanic acid iopronic acid 5-IODO-6-NITRO-1,3-BENZODIOXOLE Butanoic acid, 4-(methyl(2,4,6-triiodo-3-propoxyphenyl)amino)-4-oxo- 4-IODO-3-NITROANISOLE 2-IODO-5-METHOXYANILINE

2-IODO-5-METHOXYANILINE

BenzenaMine, 2-iodo-5-Methoxy-

2-Iodo-5-methoxy-phenylamine

2-Iodo-5-methoxybenzenamine

1H-Pyrazol-5-amine,1-(3-methylethyl)-

153898-63-6