ChemicalBook > CAS DataBase List > 2-IODO-5-METHOXYANILINE

2-IODO-5-METHOXYANILINE

Product Name
2-IODO-5-METHOXYANILINE
CAS No.
153898-63-6
Chemical Name
2-IODO-5-METHOXYANILINE
Synonyms
2-IODO-5-METHOXYANILINE;2-Iodo-5-methoxybenzenamine;2-Iodo-5-methoxy-phenylamine;BenzenaMine, 2-iodo-5-Methoxy-;1H-Pyrazol-5-amine,1-(3-methylethyl)-
CBNumber
CB4130950
Molecular Formula
C7H8INO
Formula Weight
249.05
MOL File
153898-63-6.mol
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2-IODO-5-METHOXYANILINE Property

Melting point:
33-36 °C(Solv: ethyl acetate (141-78-6))
Boiling point:
298.4±30.0 °C(Predicted)
Density 
1.807±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka
2.11±0.10(Predicted)
Appearance
White to light brown Solid
InChI
InChI=1S/C7H8INO/c1-10-5-2-3-6(8)7(9)4-5/h2-4H,9H2,1H3
InChIKey
CYDBBGSUZRDOPE-UHFFFAOYSA-N
SMILES
C1(N)=CC(OC)=CC=C1I
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
I708655
Product name
2-Iodo-5-methoxyaniline
Packaging
50mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
W3349
Product name
2-Iodo-5-methoxyaniline
Packaging
5g
Price
$444
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049825
Product name
2-IODO-5-METHOXYANILINE
Purity
95.00%
Packaging
1G
Price
$852.55
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049825
Product name
2-IODO-5-METHOXYANILINE
Purity
95.00%
Packaging
2.5G
Price
$1227.82
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0049825
Product name
2-IODO-5-METHOXYANILINE
Purity
95.00%
Packaging
5G
Price
$1548.26
Updated
2021/12/16
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2-IODO-5-METHOXYANILINE Chemical Properties,Usage,Production

Synthesis

58755-70-7

153898-63-6

General procedure for the synthesis of 2-iodo-5-methoxyaniline from 4-iodo-3-nitroanisole: To a 100 mL methanol solution of 4-iodo-3-nitroanisole (5 g, 17.9 mmol) was added FeCl3 (50 mg, 0.3 mmol) and activated carbon (40 mg). The mixture was heated to reflux and hydrazine hydrate (1.75 g, 35 mmol) was added slowly and dropwise. After keeping the reaction at reflux for 8 h, it was cooled to room temperature and the reaction mixture was filtered through diatomaceous earth. The filtrate was concentrated and purified by column chromatography (eluent: hexane solution of 10% ethyl acetate) to afford 4.05 g of the target product 2-iodo-5-methoxyaniline as a light yellow oil (91% yield).1H NMR (300 MHz, CDCl3) δ 7.47 (1H, d, J = 8.7 Hz), 6.31 (1H, d, J = 2.8 Hz), 6.13 (1H, d, J = 2.8 Hz) 6.13 (1H, dd, J = 2.8, 8.7 Hz), 3.73 (3H, s).

References

[1] Angewandte Chemie - International Edition, 2011, vol. 50, # 32, p. 7354 - 7358
[2] Journal of Organic Chemistry, 2001, vol. 66, # 13, p. 4525 - 4542
[3] Patent: WO2003/106462, 2003, A1. Location in patent: Page 110
[4] Tetrahedron Letters, 2008, vol. 49, # 2, p. 363 - 366
[5] Angewandte Chemie - International Edition, 2010, vol. 49, # 48, p. 9262 - 9265

2-IODO-5-METHOXYANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-IODO-5-METHOXYANILINE manufacturers

Career Henan Chemical Co
Product
2-IODO-5-METHOXYANILINE 153898-63-6
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
200kgs
Release date
2020-01-28

153898-63-6, 2-IODO-5-METHOXYANILINERelated Search:

3-Methoxy-2-methylaniline Butanoic acid, 4-oxo-4-(propyl(2,4,6-triiodo-3-methoxyphenyl)amino)- ( 9CI) 2-NITRO-4-(TRIFLUOROMETHOXY)IODOBENZENE 2,2-DIFLUORO-5-AMINO-6-IODO-1,3-BENZODIOXOLE Iolixanic acid iopronic acid 5-IODO-6-NITRO-1,3-BENZODIOXOLE Butanoic acid, 4-(methyl(2,4,6-triiodo-3-propoxyphenyl)amino)-4-oxo- 4-IODO-3-NITROANISOLE 2-IODO-5-METHOXYANILINE

  • 2-IODO-5-METHOXYANILINE
  • BenzenaMine, 2-iodo-5-Methoxy-
  • 2-Iodo-5-methoxy-phenylamine
  • 2-Iodo-5-methoxybenzenamine
  • 1H-Pyrazol-5-amine,1-(3-methylethyl)-
  • 153898-63-6