4-CHLORO-3-IODOQUINOLINE
- Product Name
- 4-CHLORO-3-IODOQUINOLINE
- CAS No.
- 590371-90-7
- Chemical Name
- 4-CHLORO-3-IODOQUINOLINE
- Synonyms
- 4-CHLORO-3-IODOQUINOLINE;1,4-CHLORO-3-IODOQUINOLINE;Quinoline, 4-chloro-3-iodo-
- CBNumber
- CB2325143
- Molecular Formula
- C9H5ClIN
- Formula Weight
- 289.5
- MOL File
- 590371-90-7.mol
4-CHLORO-3-IODOQUINOLINE Property
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- solid
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- SYX00306
- Product name
- 4-Chloro-3-iodo-quinoline
- Packaging
- 1g
- Price
- $185
- Updated
- 2025/07/31
- Product number
- C367308
- Product name
- 4-Chloro-3-iodoquinoline
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C367308
- Product name
- 4-Chloro-3-iodoquinoline
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- Y1203
- Product name
- 4-Chloro-3-iodo-quinoline
- Packaging
- 1g
- Price
- $97
- Updated
- 2021/12/16
- Product number
- J96930
- Product name
- 4-Chloro-3-iodo-quinoline
- Packaging
- 5g
- Price
- $295
- Updated
- 2021/12/16
4-CHLORO-3-IODOQUINOLINE Chemical Properties,Usage,Production
Synthesis
64965-48-6
590371-90-7
Synthesis of 4-chloro-3-iodoquinoline (Compound 16): 4-hydroxy-3-iodoquinoline (Compound 15, 1000 mg, 3.69 mmol) was dissolved in 25 mL of phosphorus oxychloride (POCl3). The reaction mixture was stirred at 100°C for 2 hours. The reaction progress was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the solvent was removed by evaporation under reduced pressure, followed by the addition of ice water. The solid product was collected by filtration and dried under vacuum to give compound 16 as a white solid (900 mg, 85% yield).
References
[1] ChemMedChem, 2014, vol. 9, # 4, p. 719 - 723
[2] Patent: WO2015/95780, 2015, A1. Location in patent: Page/Page column 21; 35
[3] Journal of the American Chemical Society, 1946, vol. 68, p. 2570,2573
[4] Patent: WO2011/22216, 2011, A1. Location in patent: Page/Page column 30
4-CHLORO-3-IODOQUINOLINE Preparation Products And Raw materials
Raw materials
Preparation Products
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