3-HYDROXY-4-IODOBENZYL ALCOHOL
- Product Name
- 3-HYDROXY-4-IODOBENZYL ALCOHOL
- CAS No.
- 773869-57-1
- Chemical Name
- 3-HYDROXY-4-IODOBENZYL ALCOHOL
- Synonyms
- RARECHEM AL BD 0964;3-Hydroxy-4-iodobenz;3-HYDROXY-4-IODOBENZYL ALCOHOL;5-(HYDROXYMETHYL)-2-IODOPHENOL;3-Hydroxy-4-iodobenzenemethanol;Benzenemethanol,3-hydroxy-4-iodo-;5-(Hydroxymethyl)-2-iodophenol 97%;3-Hydroxy-4-iodobenzyl alcohol, (3-Hydroxy-4-iodophenyl)methanol
- CBNumber
- CB2343332
- Molecular Formula
- C7H7IO2
- Formula Weight
- 250.03
- MOL File
- 773869-57-1.mol
3-HYDROXY-4-IODOBENZYL ALCOHOL Property
- Melting point:
- 148 °C
- Boiling point:
- 273.9±25.0 °C(Predicted)
- Density
- 2.020±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 8.29±0.10(Predicted)
- Appearance
- White to off-white Solid
Safety
- Hazard Note
- Harmful
- HS Code
- 2909500090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- H973038
- Product name
- 5-(Hydroxymethyl)-2-iodophenol
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR8637
- Product name
- 5-(Hydroxymethyl)-2-iodophenol
- Purity
- 97%
- Packaging
- 5g
- Price
- $227
- Updated
- 2021/12/16
- Product number
- 2704-H-02
- Product name
- 5-(Hydroxymethyl)-2-iodophenol
- Purity
- 97%
- Packaging
- 1g
- Price
- $61
- Updated
- 2021/12/16
- Product number
- 2103AC
- Product name
- 5-(Hydroxymethyl)-2-iodophenol
- Packaging
- 1g
- Price
- $151
- Updated
- 2021/12/16
- Product number
- 084176
- Product name
- 5-(Hydroxymethyl)-2-iodophenol
- Purity
- 97%
- Packaging
- 1g
- Price
- $157
- Updated
- 2021/12/16
3-HYDROXY-4-IODOBENZYL ALCOHOL Chemical Properties,Usage,Production
Synthesis
58123-77-6
773869-57-1
The general procedure for the synthesis of 3-hydroxy-4-iodobenzyl alcohol from 3-hydroxy-4-iodobenzoic acid was as follows: to a solution of 3-hydroxy-4-iodobenzoic acid (20.9 g, 79.3 mmol) in anhydrous THF (160 mL) was slowly added a 1 M borane-THF solution (240 mL, 240 mmol). The reaction mixture was stirred at 60 °C for 2 hours. Upon completion of the reaction, the reaction was quenched by careful addition of water and subsequently extracted twice with ethyl acetate. The organic phases were combined, washed with saturated brine and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure and the resulting residue was washed with diisopropyl ether and hexane to give 3-hydroxy-4-iodobenzenemethanol (17.4 g, 88% yield) as a white solid. The structure of the product was confirmed by 1H NMR (CDCl3): δ 1.69 (br, 1H), 4.64 (s, 2H), 5.33 (s, 1H), 6.70 (dd, J = 7.8, 1.5 Hz, 1H), 7.01 (d, J = 1.5 Hz, 1H), 7.63 (d, J = 7.8 Hz, 1H).
References
[1] Patent: EP2351743, 2011, A1. Location in patent: Page/Page column 117
3-HYDROXY-4-IODOBENZYL ALCOHOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-HYDROXY-4-IODOBENZYL ALCOHOL manufacturers
- Product
- 3-HYDROXY-4-IODOBENZYL ALCOHOL 773869-57-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2020-01-09