ChemicalBook > CAS DataBase List > 3-HYDROXY-4-IODOBENZYL ALCOHOL

3-HYDROXY-4-IODOBENZYL ALCOHOL

Product Name: 3-HYDROXY-4-IODOBENZYL ALCOHOL
CAS No.: 773869-57-1
Chemical Name: 3-HYDROXY-4-IODOBENZYL ALCOHOL
Synonyms: RARECHEM AL BD 0964;3-Hydroxy-4-iodobenz;3-HYDROXY-4-IODOBENZYL ALCOHOL;5-(HYDROXYMETHYL)-2-IODOPHENOL;3-Hydroxy-4-iodobenzenemethanol;Benzenemethanol,3-hydroxy-4-iodo-;5-(Hydroxymethyl)-2-iodophenol 97%;3-Hydroxy-4-iodobenzyl alcohol, (3-Hydroxy-4-iodophenyl)methanol
CBNumber: CB2343332
Molecular Formula: C7H7IO2
Formula Weight: 250.03
MOL File: 773869-57-1.mol

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3-HYDROXY-4-IODOBENZYL ALCOHOL Property

Melting point:: 148 °C
Boiling point:: 273.9±25.0 °C(Predicted)
Density: 2.020±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 8.29±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

Hazard Note: Harmful
HS Code: 2909500090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: H973038
Product name: 5-(Hydroxymethyl)-2-iodophenol
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: OR8637
Product name: 5-(Hydroxymethyl)-2-iodophenol
Purity: 97%
Packaging: 5g
Price: $227
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2704-H-02
Product name: 5-(Hydroxymethyl)-2-iodophenol
Purity: 97%
Packaging: 1g
Price: $61
Updated: 2021/12/16

AK Scientific

Product number: 2103AC
Product name: 5-(Hydroxymethyl)-2-iodophenol
Packaging: 1g
Price: $151
Updated: 2021/12/16

Matrix Scientific

Product number: 084176
Product name: 5-(Hydroxymethyl)-2-iodophenol
Purity: 97%
Packaging: 1g
Price: $157
Updated: 2021/12/16

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3-HYDROXY-4-IODOBENZYL ALCOHOL Chemical Properties,Usage,Production

Synthesis

58123-77-6

773869-57-1

The general procedure for the synthesis of 3-hydroxy-4-iodobenzyl alcohol from 3-hydroxy-4-iodobenzoic acid was as follows: to a solution of 3-hydroxy-4-iodobenzoic acid (20.9 g, 79.3 mmol) in anhydrous THF (160 mL) was slowly added a 1 M borane-THF solution (240 mL, 240 mmol). The reaction mixture was stirred at 60 °C for 2 hours. Upon completion of the reaction, the reaction was quenched by careful addition of water and subsequently extracted twice with ethyl acetate. The organic phases were combined, washed with saturated brine and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure and the resulting residue was washed with diisopropyl ether and hexane to give 3-hydroxy-4-iodobenzenemethanol (17.4 g, 88% yield) as a white solid. The structure of the product was confirmed by 1H NMR (CDCl3): δ 1.69 (br, 1H), 4.64 (s, 2H), 5.33 (s, 1H), 6.70 (dd, J = 7.8, 1.5 Hz, 1H), 7.01 (d, J = 1.5 Hz, 1H), 7.63 (d, J = 7.8 Hz, 1H).

References

[1] Patent: EP2351743, 2011, A1. Location in patent: Page/Page column 117

3-HYDROXY-4-IODOBENZYL ALCOHOL Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-HYDROXY-4-IODOBENZYL ALCOHOL manufacturers

Career Henan Chemical Co

Product: 3-HYDROXY-4-IODOBENZYL ALCOHOL 773869-57-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-09

773869-57-1, 3-HYDROXY-4-IODOBENZYL ALCOHOLRelated Search:

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773869-57-1

242-71-6

C7H7IO2

Benzhydrols, Benzyl & Special Alcohols

Methyl Halides

Phenyls & Phenyl-Het

Methyl Halides

Phenyls & Phenyl-Het