2-(2,4-Dinitrobenzyl)pyridine

Product Name: 2-(2,4-Dinitrobenzyl)pyridine
CAS No.: 1151-97-9
Chemical Name: 2-(2,4-Dinitrobenzyl)pyridine
Synonyms: AKOS 92219;TIMTEC-BB SBB003093;2-(2,4-DINITROBENZYL)PYRIDINE;2-(2,4-BISNITROBENZYL)PYRIDINE;2-(2,4-Dinitrobenzyl)pyridine >2-(2,4-Dinitrobenzyl)pyridine,99%;2-[(2,4-dinitrophenyl)methyl]-pyridin;2-[(2,4-dinitrophenyl)methyl]pyridine;Pyridine, 2-[(2,4-dinitrophenyl)Methyl]-;2-ACETYL-5-CHLORO-167-METHYLTHIANAPHTHENE
CBNumber: CB2343620
Molecular Formula: C12H9N3O4
Formula Weight: 259.22
MOL File: 1151-97-9.mol

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2-(2,4-Dinitrobenzyl)pyridine Property

Melting point:: 92-94°C
Boiling point:: 402.47°C (rough estimate)
Density: 1.3450 (rough estimate)
refractive index: 1.5700 (estimate)
form: powder to crystal
pka: 4.42±0.12(Predicted)
color: White to Yellow to Green
BRN: 265115
Stability:: Stable. Combustible. Incompatible with strong oxidizing agents.
CAS DataBase Reference: 1151-97-9(CAS DataBase Reference)
EPA Substance Registry System: Pyridine, 2-[(2,4-dinitrophenyl)methyl]- (1151-97-9)

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36
TSCA: Yes
HS Code: 2933.39.9200

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: S765163
Product name: 2-(2,4-DINITROBENZYL)PYRIDINE
Purity: Aldrich
Packaging: 50mg
Price: $110
Updated: 2024/03/01

TCI Chemical

Product number: D1095
Product name: 2-(2,4-Dinitrobenzyl)pyridine
Purity: >98.0%(HPLC)
Packaging: 1g
Price: $47
Updated: 2024/03/01

TCI Chemical

Product number: D1095
Product name: 2-(2,4-Dinitrobenzyl)pyridine
Purity: >98.0%(HPLC)
Packaging: 5g
Price: $142
Updated: 2024/03/01

AK Scientific

Product number: 4976AL
Product name: 2-(2,4-Dinitrobenzyl)pyridine
Packaging: 1g
Price: $129
Updated: 2021/12/16

AK Scientific

Product number: 4976AL
Product name: 2-(2,4-Dinitrobenzyl)pyridine
Packaging: 5g
Price: $320
Updated: 2021/12/16

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2-(2,4-Dinitrobenzyl)pyridine Chemical Properties,Usage,Production

Chemical Properties

White to Yellow to Green powder to crystal.

Uses

2-(2,4-Dinitrobenzyl)pyridine can be used in organic synthesis and pharmaceutical intermediates.

Preparation

Synthesis of 2-(2,4-Dinitrobenzyl)pyridine
A solution of sulfuric acid (15 mL) is placed in an ice bath along with a magnetic stirrer.Benzylpyridine (2.4 mL) is added dropwise, maintaining a temperature below 10°C. This process is then repeated for fuming nitric acid (3.0 mL), once again maintaining the temperature. After addition mixture is allowed to stand at room temperature for 30minutes. Once completed reaction mixture is heated in an 80°C water bath for 20 minutes. Mixture is then poured into a conical flask containing crushed ice (50 cm3) which is stirred in an ice bath. Using a separating funnel aqueous ammonia is added (50 – 100 mL) until the pH rises to ~9 – 10 and filter using a Buchner funnel. Ethyl acetate (40mL) & sodium hydroxide (40mL) is added to the solid and stirred using a magnetic stirrer until dissolved.
Dry the organic layer using magnesium sulfate as the drying agent which is then followed by a rotary evaporator (40°C, vacuum). Product is then washed using cold methylated spirit and left to recrystalise.

2-(2,4-Dinitrobenzyl)pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-(2,4-Dinitrobenzyl)pyridine manufacturers

Henan Fengda Chemical Co., Ltd

Product: 2-(2,4-Dinitrobenzyl)pyridine 1151-97-9
Price: US $8.00-0.80/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-04-08

1151-97-9, 2-(2,4-Dinitrobenzyl)pyridineRelated Search:

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2-[(2,4-dinitrophenyl)methyl]-pyridin

TIMTEC-BB SBB003093

2-(2,4-DINITROBENZYL)PYRIDINE

2-(2,4-BISNITROBENZYL)PYRIDINE

2-[(2,4-dinitrophenyl)methyl]pyridine

2-(2,4-Dinitrobenzyl)pyridine,99%

AKOS 92219

Pyridine, 2-[(2,4-dinitrophenyl)Methyl]-

2-(2,4-Dinitrobenzyl)pyridine &gt

2-ACETYL-5-CHLORO-167-METHYLTHIANAPHTHENE

1151-97-9