BOC,ET-N-ET-OH
- Product Name
- BOC,ET-N-ET-OH
- CAS No.
- 152192-95-5
- Chemical Name
- BOC,ET-N-ET-OH
- Synonyms
- BOC,ET-N-ET-OH;BOC-N-ET-AMINOETHANOL;N-BOC-N-ETHYL-ETHANOLAMINE;2-[Boc(ethyl)amino]ethanol;2-(N-BOC-ETHYLAMINO)ETHANOL;tert-Butyl ethyl(2-hydroxyethyl);N-T-BUTYLOXYCARBONYL-N-ETHYL-AMIN;tert-Butyl ethyl(2-hydroxyethyl)carbamate;N-T-BUTYLOXYCARBONYL-N-ETHYL-AMINOETHANOL;N-TERT-BUTYLOXYCARBONYL-N-ETHYL-AMINOETHANOL
- CBNumber
- CB2422277
- Molecular Formula
- C9H19NO3
- Formula Weight
- 189.25
- MOL File
- 152192-95-5.mol
BOC,ET-N-ET-OH Property
- Boiling point:
- 263.5±19.0 °C(Predicted)
- Density
- 1.020±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 14.67±0.10(Predicted)
- form
- liquid
- color
- Colourless
Safety
- HS Code
- 2924297099
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B433618
- Product name
- Ethyl-(2-hydroxy-ethyl)carbamicAcidtert-ButylEster
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 16215
- Product name
- N-Boc-N-ethyl-ethanolamine,≥99%(HPLC)
- Purity
- ≥99%(HPLC)
- Packaging
- 1G
- Price
- $34.94
- Updated
- 2021/12/16
- Product number
- BAL1000
- Product name
- Boc,Et-Glycinol
- Packaging
- 1g
- Price
- $60.75
- Updated
- 2021/12/16
- Product number
- FB50499
- Product name
- N-Boc-N-ethyl-ethanolamine
- Packaging
- 1g
- Price
- $65.2
- Updated
- 2021/12/16
- Product number
- FB50499
- Product name
- N-Boc-N-ethyl-ethanolamine
- Packaging
- 2g
- Price
- $104.3
- Updated
- 2021/12/16
BOC,ET-N-ET-OH Chemical Properties,Usage,Production
Synthesis
24424-99-5
110-73-6
152192-95-5
The general procedure for the synthesis of tert-butyl (2-hydroxyethyl)carbamate from di-tert-butyl dicarbonate and N-ethyl ethanolamine was as follows: to a mixed solution containing 2-(ethylamino)ethanol (8.91 g) and ethyl acetate (100 mL) was added di-tert-butyl dicarbonate (21.8 g) slowly under ice-bath cooling conditions. The reaction mixture was stirred continuously at room temperature for 3 days. Upon completion of the reaction, the mixture was washed with saturated brine (100 mL) and the organic phase was subsequently dried with anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure to give the title compound (19.0 g) as a colorless oil. The product was characterized by 1H-NMR (CDCl3): δ 1.11 (3H, t, J = 7.0 Hz), 1.47 (9H, s), 3.27 (2H, q, J = 7.0 Hz), 3.37 (2H, t, J = 5.2 Hz), 3.73 (2H, q, J = 5.2 Hz).
References
[1] Synthetic Communications, 1993, vol. 23, # 17, p. 2443 - 2449
[2] Chemical Communications, 2015, vol. 51, # 49, p. 9987 - 9990
[3] Bioorganic and Medicinal Chemistry Letters, 2005, vol. 15, # 6, p. 1547 - 1551
[4] Journal of the American Chemical Society, 2002, vol. 124, # 41, p. 12182 - 12191
[5] Patent: WO2005/80343, 2005, A2. Location in patent: Page/Page column 51-52
BOC,ET-N-ET-OH Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from BOC,ET-N-ET-OH manufacturers
- Product
- tert-butyl N-ethyl-N-(2-hydroxyethyl)carbamate 152192-95-5
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2020-01-10