2-Amino-6-methyl-5-nitropyridine
- Product Name
- 2-Amino-6-methyl-5-nitropyridine
- CAS No.
- 22280-62-2
- Chemical Name
- 2-Amino-6-methyl-5-nitropyridine
- Synonyms
- 6-Amino-3-Nitro-2-Picolin;6-AMINO-3-NITRO-2-PICOLINE;2-AMINO-5-NITRO-6-PICOLINE;2-Amino-5-nitro-6-methylpyridi;6-Amino-3-nitro-2-picoline,98%;6-Amino-3-nitro-2-picoline ,97%;6-Methyl-5-nitro-2-pyridinaMine;6-methyl-5-nitro-pyridin-2-amine;2-AMINO-6-METHYL-5-NITROPYRIDINE;6-AMINO-3-NITRO-2-METHYLPYRIDINE
- CBNumber
- CB2430160
- Molecular Formula
- C6H7N3O2
- Formula Weight
- 153.14
- MOL File
- 22280-62-2.mol
2-Amino-6-methyl-5-nitropyridine Property
- Melting point:
- 185-189 °C
- Boiling point:
- 276.04°C (rough estimate)
- Density
- 1.3682 (rough estimate)
- refractive index
- 1.6500 (estimate)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 2.97±0.37(Predicted)
- form
- Powder
- color
- Yellow
- InChIKey
- BGMZTBKXOFFTBJ-UHFFFAOYSA-N
- CAS DataBase Reference
- 22280-62-2(CAS DataBase Reference)
Safety
- Hazard Codes
- Xn,Xi
- Risk Statements
- 36/37/38-20/21/22
- Safety Statements
- 36/37/39-26-22-36
- HazardClass
- 6.1
- HS Code
- 29333999
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- A2326
- Product name
- 6-Amino-2-methyl-3-nitropyridine
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $63
- Updated
- 2025/07/31
- Product number
- A2326
- Product name
- 6-Amino-2-methyl-3-nitropyridine
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $212
- Updated
- 2025/07/31
- Product number
- A898138
- Product name
- 2-Amino-6-methyl-5-nitropyridine
- Packaging
- 1g
- Price
- $45
- Updated
- 2021/12/16
- Product number
- A898138
- Product name
- 2-Amino-6-methyl-5-nitropyridine
- Packaging
- 10g
- Price
- $140
- Updated
- 2021/12/16
- Product number
- A11777
- Product name
- 2-Amino-6-methyl-5-nitropyridine
- Purity
- 98%
- Packaging
- 1g
- Price
- $6
- Updated
- 2021/12/16
2-Amino-6-methyl-5-nitropyridine Chemical Properties,Usage,Production
Chemical Properties
Light yellow Cryst
Synthesis
1824-81-3
22280-62-2
General procedure for the synthesis of 2-amino-5-nitro-6-methylpyridine from 2-amino-6-methylpyridine: 10 mL of concentrated sulfuric acid was cooled to 0-1 °C and 2-amino-6-methylpyridine (20 g) was slowly added, keeping the temperature at 0 °C. Subsequently, 110 mL of nitric acid in the ratio of 1:1 by volume was slowly added, stirred at -1 °C and continued stirring at room temperature for 30 min. The reaction mixture was warmed up to 50 °C for 11 hours. After completion of the reaction, the reaction solution was extracted with ethyl acetate (EA). The ethyl acetate layer was washed with ammonia and then the ammonia layer was concentrated. Eventually, the solid product 2-amino-5-nitro-6-methylpyridine (18 g) was precipitated in 75% yield.
References
[1] Patent: CN105906621, 2016, A. Location in patent: Paragraph 0019
[2] Patent: WO2005/42464, 2005, A1. Location in patent: Page/Page column 32-33
[3] Bioorganic and Medicinal Chemistry, 2015, vol. 23, # 8, p. 1858 - 1868
[4] Patent: WO2009/30725, 2009, A2. Location in patent: Page/Page column 58
[5] Patent: EP1857444, 2007, A1. Location in patent: Page/Page column 20
2-Amino-6-methyl-5-nitropyridine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-Amino-6-methyl-5-nitropyridine manufacturers
- Product
- 2-Amino-6-methyl-5-nitropyridine 22280-62-2
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-05-29
- Product
- 2-Amino-6-methyl-5-nitropyridine 22280-62-2
- Price
- US $0.00/Kg/Drum
- Min. Order
- 1KG
- Purity
- 98%min HPLC
- Supply Ability
- 500KGS
- Release date
- 2021-08-09
- Product
- 2-Amino-6-methyl-5-nitropyridine 22280-62-2
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-18